Apparatus and method for coating specimens

Patent metadata

Field	Value
Publication number	US-10731252-B2
Application number	US-201815989697-A
Country	US
Kind code	B2
Filing date	May 25, 2018
Priority date	May 25, 2018
Publication date	Aug 4, 2020
Grant date	Aug 4, 2020

Abstract

An apparatus for coating specimens includes a reaction chamber and a plurality of reaction modules in the reaction chamber for containing specimens to be coated, where each reaction module includes a module inlet and a module outlet. A plurality of conduits are configured to be in fluid communication with at least one gas source external to the reaction chamber, and each of the conduits terminates in one of the reaction modules for delivery of gaseous reagents to the specimens to be coated. The module outlets are in fluid communication with the reaction chamber for expulsion of gaseous reaction products from the reaction modules.

First claim

The invention claimed is:

1. A method for coating specimens, the method comprising:
heating a reaction chamber containing a plurality of reaction modules and a plurality of specimens to be coated, each of the reaction modules including a module inlet and a module outlet and containing at least one of the specimens;
flowing gaseous reagents through the module inlets and into the reaction modules, the gaseous reagents chemically reacting to form coatings on the specimens; and
maintaining a pressure in each of the reaction modules higher than a pressure in the reaction chamber, gaseous reaction products thereby being expelled from the reaction modules through the module outlets,
wherein the gaseous reagents are flowed into the reaction modules through a plurality of conduits in fluid communication with one or more gas sources, each of the conduits including a single inlet and single outlet for flow of the gaseous reagents therethrough, and each of the conduits terminating within a volume defined by a different reaction module.

2. The method of claim 1 , wherein the reaction chamber comprises one or more outlet ports, and wherein the gaseous reaction products are removed from the reaction chamber through the one or more outlet ports.

3. The method of claim 2 , wherein the one or more outlet ports are in fluid communication with a vacuum pump.

4. The method of claim 1 , wherein the conduits pass through and/or are connected to one or more inlet ports in the reaction chamber.

5. The method of claim 1 , wherein the pressure in each of the reaction modules is from about one to about five orders of magnitude higher than that in the reaction chamber.

6. The method of claim 1 , wherein the pressure in each of the reaction modules is in a range from about 1 Torr to about 50 Torr, and the pressure in the reaction chamber is in a range from about 1 mTorr to about 50 mTorr.

7. The method of claim 1 , wherein the reaction chamber is heated to an elevated temperature in a range from about 700° C. to about 1800° C.

8. The method of claim 1 , wherein the specimens comprise porous specimens, and wherein the gaseous reagents flowed through the module inlets infiltrate the porous specimens.

9. The method of claim 8 , wherein the porous specimens comprise silicon carbide fiber preforms, and wherein the coatings comprise silicon carbide, boron nitride, or carbon.

10. The method of claim 1 , wherein the reaction chamber includes a single inlet port through which the plurality of conduits pass.

11. The method of claim 1 , wherein the plurality of reaction modules are stacked within the reaction chamber.

12. The method of claim 1 , wherein at least one of the conduits passes through at least one of the reaction modules prior to terminating in the volume defined by the different reaction module.

13. The method of claim 1 , wherein a first of the reaction modules is stacked on a sample support plate, and wherein a second of the reaction modules is stacked on the first of the reaction modules, such that a top surface of the first of the reaction modules functions as a sample support plate for the second of the reaction modules.

14. The method of claim 1 , comprising from three to six reaction modules.

15. The method of claim 1 , wherein the reaction chamber and/or each of the reaction modules comprise graphite or a carbon composite.

16. The method of claim 1 , further comprising a removable lid secured to an end of the reaction chamber.

Assignees

• Rolls Royce High Temperature Composites Inc
• Rolls Royce High Temperature Composites

Inventors

• Harris Stephen

Classifications

• C23C16/45559 Primary

  Diffusion of reactive gas to substrate · CPC title

• C04B35/565 Primary

  based on silicon carbide · CPC title

• C04B35/80

  Fibres, filaments, whiskers, platelets, or the like · CPC title

• C04B41/455

  the coating or impregnating process including a chemical conversion or reaction · CPC title

• C04B41/87

  Ceramics · CPC title