Method for producing a ceramic component composed of a plurality of joined preforms and component obtained by the method

Patent metadata

Field	Value
Publication number	US-10696600-B2
Application number	US-201715497422-A
Country	US
Kind code	B2
Filing date	Apr 26, 2017
Priority date	Apr 20, 2011
Publication date	Jun 30, 2020
Grant date	Jun 30, 2020

Abstract

A method for producing a component includes a) providing at least two preforms each made of a carbon composite material, b) joining the at least two preforms at least at one respective connecting surface to form a composite, in which a joining compound is introduced between the joining surfaces of the preforms and then cured and the joining compound contains silicon carbide and at least one polymer adhesive, and c) siliconizing the composite to form the component. A component, such as an optical component produced thereby, is also provided.

First claim

The invention claimed is:

1. A method for manufacturing a component, the method comprising the following steps:
a) providing each of at least two preforms from a carbon composite material;
b) providing a joining compound containing silicon carbide and at least one polymer adhesive and connecting the at least two preforms at least at one joining surface of each of the at least two preforms to form a composite by introducing the joining compound between the joining surfaces of the at least two preforms and then curing the joining compound, the joining compound containing:
15 to 25% by weight of water,
45 to 55% by weight of silicon carbide, and
27 to 33% by weight of polymer adhesive; and

c) siliconizing the composite to produce the component.

2. The method according to claim 1 , wherein the component is a ceramic component.

3. The method according to claim 1 , which further comprises carrying out step b) by applying the joining compound to a joining surface of a preform to coat the joining surface, pressing the coated joining surface against the joining surface of another preform, and then curing the joining compound.

4. The method according to claim 1 , which further comprises carrying out step b) by aligning the at least two preforms to be connected relative to each other to form a bonding gap between the joining surfaces, then filling the bonding gap with the joining compound, and then curing the joining compound.

5. The method according to claim 4 , which further comprises carrying out the step of aligning the at least two preforms with a joining device.

6. The method according to claim 1 , which further comprises providing the at least one polymer adhesive in step b) by using a joining material including at least one of a phenolic resin or at least one of a carbon-free polymer, a polysiloxane or a polysilazane.

7. The method according to claim 1 , wherein the at least one polymer adhesive in step b) includes a polysilane carbon-free polymer.

8. The method according to claim 1 , which further comprises carrying out step b) by using a joining compound containing a curing agent for the at least one polymer adhesive.

9. The method according to claim 8 , wherein the curing agent contains a base or an acid or p-toluenesulfonic acid.

10. The method according to claim 1 , which further comprises carrying out step b) by curing the joining compound at one of the following temperature ranges:
10° C. to 100° C., or
15° C. to 80° C., or
18° C. to 30° C.

11. The method according to claim 10 , which further comprises carrying out the curing step for a period of 5 to 30 hours.

12. The method according to claim 1 , which further comprises carrying out step b) by using a joining compound containing silicon carbide in powder form and having an average particle diameter in one of the following ranges:
1 to 50 μm, or
3 to 20 μm, or
5 to 10 μm.

13. The method according to claim 1 , which further comprises carrying out step a) by providing the at least two preforms from a composite material including a matrix of amorphous and porous carbon.

14. The method according to claim 13 , which further comprises carrying out step a) by providing two preforms containing at least one of carbon particles or carbon fibers embedded in the matrix, and providing the carbon particles with a particle diameter or providing the carbon fibers with an average length, not exceeding 75 μm.

15. The method according to claim 14 , wherein the particle diameter or the average length does not exceed 50 μm.

16. A method for manufacturing a component, the method comprising the following steps:
a) providing each of at least two preforms from a composite material including a matrix of amorphous and porous carbon by molding the at least two preforms from a mixture containing a carbon precursor and an organic binder, subsequently carbonizing the at least two preforms, and using cellulose flour as the carbon precursor;
b) providing a joining compound containing silicon carbide and at least one polymer adhesive and connecting the at least two preforms at least at one joining surface of each of the at least two preforms to form a composite by introducing the joining compound between the joining surfaces of the at least two preforms and then curing the joining compound; and
c) siliconizing the composite to produce the component.

17. The method according to claim 1 , which further comprises carrying out step b) by applying a pretreatment compound to the joining surfaces of the at least two preforms before applying the joining compound.

18. The method according to claim 17 , wherein the pretreatment compound includes silicon.

19. The method according to claim 18 , wherein the pretreatment compound is composed of the same components as the joining compound.

20. The method according to claim 1 , which further comprises carrying out the siliconizing in step c) by infiltrating the composite with liquid silicon or a liquid silicon alloy and subsequently heat treating at a temperature in one of the following ranges:
1,100 to 2000° C., or
1,350 to 2000° C., or
1,500° C. to 1,700° C.

Assignees

• Sgl Carbon Se

Inventors

• Polster Peter
• Kienzle Andreas
• Putz Thomas
• Von Ganski Albin
• Hell Blasius
• Haeusler Alfred

Classifications

• C04B35/573

  obtained by reaction sintering {or recrystallisation} · CPC title

• C04B37/00 Primary

  Joining burned ceramic articles with other burned ceramic articles or other articles by heating {(soldering and welding materials B23K35/24; laminated products B32B, E04C)} · CPC title

• G03F7/20

  Exposure; Apparatus therefor (photographic printing apparatus for making copies G03B27/00) · CPC title

• C04B35/83

  Carbon fibres in a carbon matrix · CPC title

• C04B35/522 Primary

  Graphite (C04B35/536 takes precedence) · CPC title