Annular divided wall column for an air separation unit

Patent metadata

Field	Value
Publication number	US-10684071-B2
Application number	US-201816042189-A
Country	US
Kind code	B2
Filing date	Jul 23, 2018
Priority date	Aug 25, 2017
Publication date	Jun 16, 2020
Grant date	Jun 16, 2020

Abstract

An annular divided wall column for the cryogenic rectification of air or constituents of air is provided. The annular divided wall column includes a first annular column wall and a second annular column wall disposed within the first annular column wall and radially spaced therefrom to define an annulus column region as the space between the first annular column wall and the second annular column wall. An interior core column region is also defined by the interior space of the second annular column wall. The present annular divided wall column further includes a plurality of packing elements, plurality of trays or a heat exchange device disposed within the interior core column region; and a plurality of packing elements disposed within the annulus column region.

First claim

We claim:

1. An annular column for cryogenic rectification of air or constituents of air, said column comprising:
a first annular column wall;
a second annular column wall radially spaced from the first annular column wall and disposed within a first interior space of the first annular column wall to define an annulus column region between the first annular column wall and the second annular column wall and to define an interior core column region as part or all of a second interior space of the second annular column wall;
a plurality of structured packing elements of a first type disposed within the annulus column region; and
a plurality of structured packing elements of a second type disposed within the interior core column region;
wherein the first type of structured packing elements and the second type of structured packing elements have different surface area densities and the surface area densities of the first type of structured packing elements are between about 100 m 2 /m 3 to 1200 m 2 /m 3 and the second type of structured packing elements are between about 100 m 2 /m 3 to 1200 m 2 /m 3 ; and
wherein the first type of structured packing elements have a first nominal inclination angle of corrugations to the horizontal axis of between about 35° to 70° and the second type of structured packing elements have a second nominal inclination angle of corrugations to the horizontal axis of between about 35° to 70° and wherein the first nominal inclination angle of corrugations to the horizontal axis of the first type of structured packing elements is different than the second nominal inclination angle of corrugations to the horizontal axis of the second type of structured packing elements.

2. The annular column of claim 1 , wherein the first annular column wall and the second annular column wall are concentrically disposed relative to one another.

3. The annular column of claim 1 , wherein the first annular column wall is cylindrical and the second annular column wall is cylindrical.

4. The annular column of claim 1 , wherein a vertical height of the first annular column wall is greater than a vertical height of the second annular column wall.

5. The annular column of claim 1 , further comprising a cap or header extending from the top of the second annular column wall to an intermediate location of the first annular column wall to partially enclose the annulus column region.

6. The annular column of claim 1 , further comprising a cap or header attached to the top of the second annular column wall to partially enclose the interior core column region.

7. The annular column of claim 1 , wherein the annulus column region is configured for rectification of an argon-oxygen containing stream to separate it into an argon-rich overhead stream and an oxygen-rich stream.

8. The annular column of claim 1 , wherein the annulus column region is configured for rectification of a nitrogen-oxygen containing stream to separate it into a nitrogen rich overhead stream and an oxygen-rich stream.

9. The annular column of claim 1 , wherein the interior core column region is configured for rectification of an argon-oxygen containing stream to separate it into an argon-rich overhead stream and an oxygen-rich stream.

10. The annular column of claim 1 , wherein the interior core column region is configured for rectification of a nitrogen-oxygen containing stream to separate it into a nitrogen rich overhead stream and an oxygen-rich stream.

11. The annular column of claim 1 , wherein the annulus column region is configured for rectification of a nitrogen-oxygen containing stream to separate it into a first nitrogen rich overhead stream and a first oxygen-rich stream of a first purity and the interior core column region is configured for rectification of the nitrogen-oxygen containing stream to separate it into a second nitrogen rich overhead stream and a second oxygen-rich stream of a second purity.

12. The annular column of claim 1 , wherein the annulus column region is configured for rectification of a nitrogen-oxygen containing stream to separate it into a first nitrogen rich overhead stream of a first purity and a first oxygen-rich stream and the interior core column region is configured for rectification of the nitrogen-oxygen containing stream to separate it into a second nitrogen rich overhead stream of a second purity and a second oxygen-rich stream.

13. The annular column of claim 1 , wherein the plurality of structured packing elements of the first type and of the second type are constructed of aluminum sheet metal or stainless steel sheet metal.

14. The annular column of claim 1 , wherein the first type of structured packing elements and the second type of structured packing elements have different surface area densities and the surface area densities of the first type of structured packing elements and the second type of structured packing elements are selected from a group consisting of: 110 m 2 /m 3 ; 220 m 2 /m 3 ; 250 m 2 /m 3 ; 350 m 2 /m 3 ; 430 m 2 /m 3 ; 500 m 2 /m 3 ; 730 m 2 /m 3 ; 950 m 2 /m 3 ; and 1200 m 2 /m 3 .

15. The annular column of claim 1 , wherein the first and second nominal inclination angle of corrugations to the horizontal axis selected from a group consisting of: 40°; 45°; and 60°.

16. The annular column of claim 1 , wherein the structured packing elements of the first type and of the second type are configured as rectangular bricks or arcuate bricks.

17. The annular column of claim 1 , wherein the surface area density of the first type of structured packing elements is between 700 m 2 /m 3 and 1000 m 2 /m 3 and the surface area density of the second type of structured packing elements is between 400 m 2 /m 3 and 700 m 2 /m.

18. The annular column of claim 1 , wherein the first nominal inclination angle of corrugations to the horizontal axis is between about 55° to 70° and the second nominal inclination angle of corrugations to the horizontal axis is between about 45° to 55°.

Assignees

• Larson Kirk F
• Belanger Paul W
• Brown Steven C
• Ricotta John P
• Chen Guang X
• Lenz Richard D
• Praxair Technology Inc

Inventors

• Larson Kirk F
• Belanger Paul W
• Brown Steven C
• Ricotta John P
• Chen Guang X
• Lenz Richard D

Classifications

• B01J2219/32203

  Sheets · CPC title

• F25J3/04896

  Details of columns, e.g. internals, inlet/outlet devices · CPC title

• B01D3/141

  where at least one distillation column contains at least one dividing wall · CPC title

• B01J2219/185

  vertical · CPC title

• B01J2219/3085

  Ordered or stacked packing elements · CPC title