Concentration control in filtration systems, and associated methods

Patent metadata

Field	Value
Publication number	US-10561987-B2
Application number	US-201815892012-A
Country	US
Kind code	B2
Filing date	Feb 8, 2018
Priority date	Nov 17, 2014
Publication date	Feb 18, 2020
Grant date	Feb 18, 2020

Abstract

Concentration control in filtration systems and associated methods are generally described. Streams originating from upstream filters and having similar concentrations of a target minor component and/or similar osmotic pressures can be mixed and subsequently filtered within additional filters. Certain embodiments comprise recycling an output stream produced by a filter to a filter feed stream, wherein the output stream and the filter feed stream have similar concentrations of a target minor component and/or similar osmotic pressures. Such strategic mixing and/or recycling can reduce the amount of energy and/or the amount of filtration medium surface area required to achieve a desired concentration of the target minor component in a final product stream.

First claim

What is claimed is:

1. A reverse osmosis separation system for enriching a minor component of a liquid feed, the liquid feed having concentrations of a major component and the minor component, the minor component being non-ionic and having a molecular weight less than about 150 g/mole, wherein the concentration of the minor component in the liquid feed is at least about 0.00001% to less than 50% by weight, the system comprising:
a plurality of passes in a first grouping, including a first pass, wherein (i) each pass has at least one reverse osmosis membrane filtration unit, each membrane filtration unit having at least one membrane that at least partially rejects ethanol, (ii) each pass has a feed stream inlet for a feed stream, a permeate stream outlet for a permeate stream, and a retentate stream outlet for a retentate stream, (iii) the feed stream inlet of each pass, other than the first pass, is coupled to the permeate stream outlet of a preceding pass, and (iv) the retentate stream outlet, of a selected pass, after the first pass, is coupled to the feed stream inlet of the first pass;
a retentate side of a particular one of the reverse osmosis membrane filtration units of the first grouping coupled to a reverse osmosis membrane filtration unit, distinct from the particular one, such that (a) a first fluid on the retentate side of the particular one is configured to be coupled to the second fluid in the distinct one and (b) the distinct one receives second fluid from the first grouping; and
a feedback control system comprising one or more pumps and one or more sensors configured to control the concentration of the minor component in the one of the first and second fluids having a lesser concentration thereof to match within 50% the concentration of the minor component of the other of the first and second fluids.

2. A system according to claim 1 , further comprising:
a set of reverse osmosis membrane filtration units in a second grouping to provide second stage filtration, the set having at least one member, wherein each filtration unit in the set has a feed stream inlet coupled to a retentate stream outlet of a selected pass in the first grouping and a permeate stream outlet coupled to a retentate stream outlet of a pass subsequent to the selected pass in the first grouping, and wherein the distinct reverse osmosis membrane filtration unit is in the second grouping,
the first fluid corresponding to the retentate stream outlet of the pass subsequent to the selected pass in the first grouping, and
the second fluid corresponding to the permeate stream outlet of the distinct reverse osmosis membrane filtration unit in the second grouping.

3. A system according to claim 2 , wherein the system is configured to recycle retentate from the retentate stream outlet, of a selected pass of the second grouping, to the feed stream inlet of a pass of the first grouping.

4. A system according to claim 1 , further comprising:
a set of reverse osmosis membrane filtration units in a second grouping to provide second stage filtration, the set having at least one member, and
wherein the system is configured to recycle retentate from the retentate stream outlet, of a selected pass of the second grouping, to the feed stream inlet of a pass of the first grouping, wherein the first fluid corresponds to fluid in the feed stream inlet of the pass of the first grouping and the second fluid corresponds to the retentate from the retentate stream outlet of the selected pass of the second grouping.

5. A system according to claim 1 , wherein the at least one membrane has a rejection percentage of the minor component between about 10% and about 99%.

6. A system according to claim 1 , wherein the at least one membrane has a rejection percentage of the minor component between about 35% and about 90%.

7. A system according to claim 1 , wherein the at least one membrane has a rejection percentage of the minor component between about 60% and about 90%.

8. A reverse osmosis separation system for enriching a minor component of a liquid feed, the liquid feed having concentrations of a major component and the minor component, the minor component being non-ionic and having a molecular weight less than about 150 g/mole, wherein the concentration of the minor component in the liquid feed is at least about 0.00001% to less than 50% by weight, the system comprising:
a first filter comprising a first filtration medium defining a permeate side and a retentate side of the first filter;
a second filter comprising a second filtration medium defining a permeate side and a retentate side of the second filter;
a third filter comprising a third filtration medium defining a permeate side and a retentate side of the third filter;
a fluidic connection between:
(a) the liquid feed and the retentate side of the first filter;
(b) the permeate side of the first filter and the retentate side of the second filter;
(c) the retentate side of the first filter and the retentate side of the third filter; and
(d) the retentate side of the second filter and the retentate side of the third filter or the retentate side of the second filter and the permeate side of the third filter, wherein each of the fluidic connections is configured to convey a liquid stream; and

a feedback control system comprising one or more pumps and one or more sensors configured to control:
a lesser of the concentration of the minor component (1) in the liquid stream within the fluidic connection between the retentate side of the third filter and the retentate side of the first filter and (2) in the liquid feed to match within 50% a greater of the concentration of the minor component (1) in the liquid stream within the fluidic connection between the retentate side of the third filter and the retentate side of the first filter and (2) in the liquid feed; and/or
the concentration of the minor component in the liquid stream within the fluidic connection between the retentate side of the second filter and the permeate side of the third filter, such that a lesser of the concentration of the minor component (1) in the liquid stream leaving the permeate side of the third filter and (2) in the liquid stream leaving the retentate side of the second filter matches within 50% a greater of the concentration of the minor component (1) in the liquid stream leaving the permeate side of the third filter and (2) in the liquid stream leaving the retentate side of the second filter.

9. The system of claim 8 , further comprising:
a fourth filter comprising a fourth filtration medium defining a permeate side and a retentate side of the fourth filter; and
a fluidic connection between the retentate side of the fourth filter, the retentate side of the second filter and the permeate side of the third filter.

10. The system of claim 9 , further comprising a fluidic connection between the retentate side of the fourth filter and the retentate side of the first filter.

11. The system of claim 9 , wherein the fourth filtration medium comprises a filtration membrane.

12. The system of claim 8 , wherein the first filter, the second filter, and/or the third filter includes a vessel within which the corresponding filtration medium is housed, and the vessel is configured to withstand an internal hydraulic pressure of at least about 3900 psi gauge without rupturing.

13. The system of claim 8 , further comprising a pump connected to the second filter and configured to transport liquid from the second filter to the third filter.

14. The system of claim 8 , wherein the first filter and the second filter are directly fluidically connected.

Assignees

• Massachusetts Inst Technology

Inventors

• Mcgovern Ronan K
• Lienhard V John H

Classifications

• B01D61/22

  Controlling or regulating · CPC title

• C12C11/11

  Post fermentation treatments, e.g. carbonation, or concentration (methods for reducing the alcohol content after fermentation C12H3/00; methods for increasing the alcohol content after fermentation C12H6/00) · CPC title

• B01D61/12 Primary

  Controlling or regulating · CPC title

• B01D61/18

  Apparatus therefor · CPC title

• B01D2311/08

  Specific process operations in the concentrate stream · CPC title