Concentration control in filtration systems, and associated methods

Patent metadata

Field	Value
Publication number	US-9925494-B2
Application number	US-201514943905-A
Country	US
Kind code	B2
Filing date	Nov 17, 2015
Priority date	Nov 17, 2014
Publication date	Mar 27, 2018
Grant date	Mar 27, 2018

Abstract

Concentration control in filtration systems and associated methods are generally described. Streams originating from upstream filters and having similar concentrations of a target minor component and/or similar osmotic pressures can be mixed and subsequently filtered within additional filters. Certain embodiments comprise recycling an output stream produced by a filter to a filter feed stream, wherein the output stream and the filter feed stream have similar concentrations of a target minor component and/or similar osmotic pressures. Such strategic mixing and/or recycling can reduce the amount of energy and/or the amount of filtration medium surface area required to achieve a desired concentration of the target minor component in a final product stream.

First claim

What is claimed is:

1. In a liquid feed having concentrations of a major component and of a minor component, the minor component being non-ionic and having a molecular weight less than about 150 g/mole, wherein the concentration of the minor component in the liquid feed is at least about 0.1% to less than 50% by weight, a method of enriching the minor component, the method comprising:
providing a reverse osmosis separation system having a plurality of passes in a first grouping, including a first pass, wherein (i) each pass has at least one reverse osmosis membrane filtration unit, each membrane filtration unit having at least one membrane that at least partially rejects ethanol, (ii) each pass has a feed stream inlet for a feed stream, a permeate stream outlet for a permeate stream, and a retentate stream outlet for a retentate stream, (iii) the feed stream inlet of each pass, other than the first pass, is coupled to the permeate stream outlet of a preceding pass; and
coupling first fluid on a retentate side of a particular one of the reverse osmosis membrane filtration units of the first grouping to second fluid from a reverse osmosis membrane filtration unit, distinct from the particular one, that receives second fluid from the first grouping, under operating conditions wherein the concentration of the minor component in one of the first and second fluids having a lesser concentration thereof matches within 50% the concentration of the minor component of the other of the first and second fluids.

2. A method according to claim 1 , further comprising supplying the liquid feed to the feed stream inlet of the first pass.

3. A method according to claim 1 , further comprising obtaining retentate, from the retentate stream outlet of the first pass, that is enriched with the minor component.

4. A method according to claim 1 , wherein providing a reverse osmosis separation system further includes providing:
a set of reverse osmosis membrane filtration units in a second grouping to provide second stage filtration, the set having at least one member, wherein each filtration unit in the set has a feed stream inlet coupled to a retentate stream outlet of a selected pass in the first grouping and a permeate stream outlet coupled to a retentate stream outlet of a pass subsequent to the selected pass in the first grouping, and wherein the distinct reverse osmosis membrane filtration unit is in the second grouping,
the first fluid corresponding to the retentate stream outlet of the pass subsequent to the selected pass in the first grouping, and
the second fluid corresponding to the permeate stream outlet of the distinct reverse osmosis membrane filtration unit in the second grouping.

5. A method according to claim 4 , further comprising:
recycling retentate from the retentate stream outlet, of a selected pass of the second grouping, to the feed stream inlet of a pass of the first grouping.

6. A method according to claim 4 , further comprising mixing the first fluid and second fluid prior to subsequent filtration in a reverse osmosis filtration unit of the second grouping.

7. A method according to claim 1 , wherein providing a reverse osmosis separation system further includes providing:
a set of reverse osmosis membrane filtration units in a second grouping to provide second stage filtration, the set having at least one member, and wherein the method further comprises:
recycling retentate from the retentate stream outlet, of a selected pass of the second grouping, to the feed stream inlet of a pass of the first grouping, wherein the first fluid corresponds to fluid in the feed stream inlet of the pass of the first grouping and the second fluid corresponds to the retentate from the retentate stream outlet of the selected pass of the second grouping.

8. A method according to claim 1 , wherein each membrane filtration unit having at least one membrane rejects ethanol with an ethanol rejection percentage between about 10% and about 99%.

9. A method according to claim 1 , wherein the ethanol rejection percentage is between about 35% and about 90%.

10. A method according to claim 1 , wherein the ethanol rejection percentage is between about 60% and about 90%.

11. A method according to claim 1 , wherein the liquid feed is an alcoholic beverage.

12. A method according to claim 1 , wherein the liquid feed is a beer.

13. A method according to claim 1 , wherein the major component is water and the minor component is ethanol.

14. A method according to claim 1 , wherein the concentration of the minor component in the liquid feed is at least about 1% to less than 50% by weight.

15. A method according to claim 1 , further comprising maintaining temperature of liquid in the at least one filtration unit between 0° C. and 8° C.

16. A method according to claim 1 , wherein preceding the feed stream inlet of the first pass is at least one reverse osmosis membrane filtration unit.

Assignees

• Massachusetts Inst Technology

Inventors

• Mcgovern Ronan K
• Lienhard V John H

Classifications

• C12H3/04

  using semi-permeable membranes · CPC title

• B01D2311/08

  Specific process operations in the concentrate stream · CPC title

• B01D61/22

  Controlling or regulating · CPC title

• B01D61/18

  Apparatus therefor · CPC title

• B01D2317/027

  Christmas tree arrangements · CPC title