Sample vaporization unit and gas chromatograph

Patent metadata

Field	Value
Publication number	US-10551359-B2
Application number	US-201515550435-A
Country	US
Kind code	B2
Filing date	Feb 16, 2015
Priority date	Feb 16, 2015
Publication date	Feb 4, 2020
Grant date	Feb 4, 2020

Abstract

A housing is provided with an internal space for accommodating an insert and a cylindrical cap attachment part provided, at the distal end surface thereof, with an opening part communicating with the internal space. An inclined groove that is inclined from the distal end side to the proximal end side of the cap attachment part along the circumferential direction of the cap attachment part is provided on the outer circumferential surface of the cap attachment part. A cap fixing part for attaching a seal cap to the cap attachment part has a cap holding part for holding the outer peripheral surface of the seal cap and an elastic part connected to the cap holding part. The elastic part is provided with a protrusion that is fit into the inclined groove of the outer peripheral surface of the cap attachment part.

First claim

The invention claimed is:

1. A sample vaporization unit comprising:
a tubular insert;
a housing having an internal space which accommodates the insert, and a cylindrical cap attachment part provided with an opening part communicating with the internal space on a distal end side thereof, at least one inclined groove being formed on an outer peripheral surface of the cap attachment part, the at least one inclined groove being inclined from the distal end side toward a proximal end side of the cap attachment part along a circumferential direction, and having a start point at a position closest to the distal end side of the cap attachment part, and an end point at a position closest to the proximal end side of the cap attachment part;
a seal cap detachably attached to the cap attachment part of the housing to seal the opening part; and
a cap fixing part which has a cap holding part engaged with the seal cap to be movable in the circumferential direction of the outer peripheral surface, and an elastic part connected to the cap holding part, the elastic part having a protrusion fitted into the at least one inclined groove of the cap attachment part, the cap fixing part being rotatably attached to the cap attachment part so that the protrusion slides along the at least one inclined groove inside the at least one inclined groove, the elastic part having a spring property for generating an elastic force of pressing the cap holding part toward the opening part so that the seal cap seals the opening part when the protrusion approaches the end point of the at least one inclined groove.

2. The sample vaporization unit according to claim 1 , wherein a hollow is provided at a position of the end point of the inner surface of the at least one inclined groove that slides with the protrusion when the protrusion moves from the start point to the end point side of the at least one inclined groove, the hollow fitting the protrusion to the distal end side of the cap holding part to prevent movement of the protrusion toward the start point side.

3. The sample vaporization unit according to claim 1 , wherein the at least one inclined groove comprises multiple inclined grooves that are uniformly provided on the outer peripheral surface of the cap attachment part in the circumferential direction of the cap attachment part.

4. The sample vaporization unit according to claim 1 , wherein the cap holding part and the elastic part of the cap fixing part are integrally formed.

5. The sample vaporization unit according to claim 1 , wherein the cap holding part and the elastic part of the cap fixing part are formed as separate bodies and connected to each other.

6. The sample vaporization unit according to claim 1 , wherein an annular elastic seal member which surrounds the outer circumference of the opening part side of the insert is provided in the vicinity of the opening part in the internal space,
an annular pedestal which supports the elastic seal member inserted from the opening part to surround the periphery of the insert is provided on the opening part side of the inner wall surface of the internal space,
a pressing part which is inserted from the opening part into the internal space to press the elastic seal member toward the pedestal side is provided on the opening part side of the seal cap, and
when the protrusion of the cap fixing part reaches the end point of the at least one inclined groove, the elastic seal member pressed to the pedestal side by the pressing part of the seal cap deforms to seal a gap between the outer peripheral surface of the insert and the inner wall surface of the internal space.

7. The sample vaporization unit according to claim 1 , wherein a lever for driving the cap fixing part in a rotation direction is provided in the cap fixing part.

8. The sample vaporization unit according to claim 1 , wherein a flange part protruding in a flange shape in a circumferential direction is provided on an outer peripheral surface of the seal cap, and
the cap holding part of the cap fixing part has an annular shape having an inner diameter smaller than the outer diameter of the flange part, and a surface of the opening part side engages with the flange part to press the seal cap toward the opening part.

9. The sample vaporization unit according to claim 1 , wherein the seal cap has a needle insertion part which inserts a sample injection needle toward the internal space on a surface of an opposite side to the opening part, and the seal cap includes a septum on a side closer to the opening part than the needle insertion part, the septum allowing the needle inserted from the needle insertion part to penetrate, and being made of an elastic material having elasticity to close the hole after extraction of the needle.

10. The sample vaporization unit according to claim 1 , wherein the protrusion is provided in the elastic part so as to be perpendicular to the outer peripheral surface of the cap attachment part when the relative displacement amount of the protrusion from the seal holding part becomes maximum.

11. A gas chromatograph comprising:
the sample vaporization unit according to claim 1 ;
an analysis column which is connected to an outlet part of the sample vaporization unit to separate a sample having passed through the sample vaporization unit; and
a detector which detects the sample separated by the analysis column.

Assignees

• Shimadzu Corp

Inventors

• Takemoto Hajime
• Ide Yoshihiko
• Saeki Takahiro
• Takechi Ryo
• Komori Yuki

Classifications

• G01N2030/126

  evaporating sample · CPC title

• G01N30/12 Primary

  by evaporation · CPC title

• B65D41/28

  Caps combined with stoppers · CPC title

• G01N30/16

  Injection (G01N30/24 takes precedence) · CPC title

• B05C17/00516

  Shape or geometry of the outlet orifice or the outlet element · CPC title