Process for recovery of waste gel-mass from softgel manufacturing process

Patent metadata

Field	Value
Publication number	US-10465143-B2
Application number	US-201615345669-A
Country	US
Kind code	B2
Filing date	Nov 8, 2016
Priority date	Nov 9, 2015
Publication date	Nov 5, 2019
Grant date	Nov 5, 2019

Abstract

A process and system for recovering gel-mass from a gel-mass-containing waste material. The process comprises retrieving the gel-mass-containing waste material from an encapsulation process; melting the retrieved waste material to provide an oil phase and a non-oil phase; retrieving the non-oil phase to produce a recovered gel-mass; and recycling the recovered gel-mass for combination with fresh encapsulating material to provide a combined encapsulating material for use in encapsulating a same lot of the same product which was being encapsulated in the step that produced the gel-mass-containing waste material from which the gel-mass was obtained. The system comprises a heated accumulator for receiving and melting the gel-mass-containing waste material to provide an oil phase and a non-oil phase; a pumping system; an optional mixer; and a control system.

First claim

What is claimed is:

1. An encapsulation process including recovery of gel-mass from a gel-mass-containing waste material, comprising the steps of:
(a) encapsulating a product thereby producing an encapsulated product and a gel-mass-containing waste material;
(b) retrieving the gel-mass-containing waste material after said encapsulating step with sanitary mangle rolls;
c) introducing the gel-mass-containing waste material into a displacement liquid which is an oil-miscible liquid heated to a temperature in a range of from 50° C. to 90° C. to facilitate melting the gel-mass-containing waste material to produce an oil phase and a non-oil phase;
(d) separating the non-oil phase to provide a recovered gel-mass;
(e) combining the recovered gel-mass with fresh encapsulating material to provide a combined encapsulating material; and
(f) feeding the combined encapsulating material to step (a) for encapsulation of an additional product from a same lot of the product which was encapsulated in the step (a) that produced the gel-mass-containing waste material from which the recovered gel-mass of step (d) was obtained.

2. The process of claim 1 , further comprising the step of mixing the recovered gel-mass prior to combining it with fresh encapsulating material to provide a mixed recovered gel-mass.

3. The process of claim 2 , further comprising the step of detecting a water content of the mixed recovered gel-mass.

4. The process of claim 3 , further comprising the step of adding water to the mixed recovered gel-mass to adjust the water content of the mixed recovered gel-mass.

5. The process of claim 1 , wherein the melting step is carried out at a reduced pressure lower than one atmosphere.

6. The process of claim 1 , wherein the displacement liquid is heated to a temperature in a range of from 60° C. to 80° C.

7. The process of claim 1 , further comprising the step of detecting a presence of the oil phase and non-oil phase interface.

8. The process of claim 7 , wherein the detecting step is carried out using at least one sensor selected from capacitance sensors, pressure sensors, buoyancy sensors, differential temperature sensors, and conductivity sensors.

9. The process of claim 1 , further comprising the step of recovering lubricating oil from the oil phase using a technique selected from fractional distillation, short path distillation and reverse osmosis.

10. The process of claim 1 , further comprising the step of filtering the gel-mass using a filtration technique selected from pressure filtration, hot filtration or diafiltration.

11. The process of claim 1 , wherein the mangle rolls comprise a pair of knurled cylinders.

12. The process of claim 1 , wherein the mangle rolls employ sealed bearings.

13. The process of claim 1 , wherein the gel mass-containing waste material is recovered by a single pair of mangle rolls.

14. The process of claim 1 , wherein the gel mass-containing waste material is recovered by more than one pair of mangle rolls.

15. The process of claim 1 , wherein the mangle rolls include meshing curvilinear and elongated teeth configured to engage one another to grasp the gel mass-containing waste material therebetween.

Assignees

• Scherer Technologies Llc R P

Inventors

• Fulper Lester David
• Stange Werner
• Hart Norton Richard
• Mckee Shawn P
• Tosado Neftali

Classifications

• B01J13/0069 Primary

  Post treatment · CPC title

• C10M175/06

  by ultrafiltration or osmosis · CPC title

• C10M175/0033 Primary

  using distillation processes; devices therefor · CPC title

• B01D36/003

  Filters in combination with devices for the removal of liquids (B01D35/185 takes precedence) · CPC title

• B01D17/042

  by changing the temperature · CPC title