Method for producing mixture

Patent metadata

Field	Value
Publication number	US-10428187-B2
Application number	US-201615559141-A
Country	US
Kind code	B2
Filing date	Mar 18, 2016
Priority date	Mar 19, 2015
Publication date	Oct 1, 2019
Grant date	Oct 1, 2019

Abstract

Provided is a method for producing a mixture, comprising a mixing step for mixing a slurry prepared by dispersing a filler containing carbon black and a rubber liquid prepared by dispersing or the like a rubber component. In the above producing method, the carbon black contained in the slurry has a surface average acidic functional group amount (μeq/m 2 ) of 0.40 or more and less than 3.00; a pH of the slurry is 8 or more; the sum total of the solid matter concentrations of the slurry and the rubber liquid is 20% by mass or less; a mixing equipment used has one or more rotors disposed rotatably in a rotation axis direction and one or more stators disposed unrotatably in the rotation axis direction; the rotors and the stators have plural projections which are arranged circularly with the rotation axis set as the center; rings are formed concentrically by the projections in a single stage or a multistage; and the slurry and the rubber liquid are allowed to pass through a space between the rotors and the stators while the rotors rotate, whereby the mixing is carried out to produce the mixture.

First claim

What is claimed is:

1. A method for producing a mixture, comprising a mixing step for mixing a slurry prepared by dispersing a filler containing carbon black and a rubber liquid prepared by dispersing or dissolving a rubber component, wherein the carbon black contained in the slurry prepared by dispersing the filler containing carbon black has a surface average acidic functional group amount (μeq/m 2 ) of 0.40 or more and less than 3.00; a pH of the slurry is 8 or more; the sum total of the solid matter concentrations of the slurry prepared by dispersing the filler containing carbon black and the rubber liquid prepared by dispersing or dissolving the rubber component is 20% by mass or less; a mixing equipment used in the mixing step has one or plural rotors disposed rotatably in a rotation axis direction and one or plural stators disposed unrotatably in the rotation axis direction; the rotors and the stators have plural projections which are arranged circularly with the rotation axis set as the center; rings are formed concentrically by the projections in a single stage or a multistage; the projections of the rotors and the stators are oppositely disposed so that they engage alternately; and the slurry and the rubber liquid in which the sum total of the solid matter concentrations thereof is 20% by mass or less are allowed to pass through a space between the rotors and the stators while the rotors rotate, whereby the mixing step is carried out.

2. The method for producing a mixture as described in claim 1 , wherein a peripheral speed of the rotors in the mixing step is 3 to 16 m/second.

3. The method for producing a mixture as described in claim 1 , wherein the mixture produced in the mixing step passes through a coagulating step in which the mixture produced in the mixing step is continuously coagulated by means of a static mixer.

4. The method for producing a mixture as described in claim 2 , wherein the mixture produced in the mixing step passes through a coagulating step in which the mixture produced in the mixing step is continuously coagulated by means of a static mixer.

Assignees

• Bridgestone Corp

Inventors

• Yanagisawa Yasuto
• Kanda Yukari
• WARAGAI Shigenobu
• MATSUO Osamaru

Classifications

• C08J2307/00

  Characterised by the use of natural rubber · CPC title

• C08J3/215 Primary

  at least one additive being also premixed with a liquid phase · CPC title

• C08J2309/00

  Characterised by the use of homopolymers or copolymers of conjugated diene hydrocarbons · CPC title

• C08K3/04

  Carbon · CPC title

• C08J3/22

  using masterbatch techniques · CPC title