Liquid redistributor

Patent metadata

Field	Value
Publication number	US-10357740-B2
Application number	US-201414903851-A
Country	US
Kind code	B2
Filing date	Jul 7, 2014
Priority date	Jul 11, 2013
Publication date	Jul 23, 2019
Grant date	Jul 23, 2019

Abstract

A liquid redistributor, arranged in a packing column between two packings, wherein in the column a liquid phase is guided from top to bottom and against the same a gas phase from bottom to top, comprising a liquid distributor tray and a droplet damping tray, which attenuates the fluidization of the liquid layer on the liquid distributor tray as caused by the droplets falling down.

First claim

The invention claimed is:

1. A liquid redistributor, configured for use in a packing column for a thermal separation process between two packings, wherein in the column a liquid phase is guided from top to bottom and against the same a gas phase is guided from bottom to top, the liquid redistributor comprising:
a liquid distributor tray;
a droplet damping tray which is arranged above the liquid distributor tray and is aligned parallel to the same,
wherein the droplet damping tray covers the column cross-section to the same extent as the liquid distributor tray and wherein the droplet damping tray is configured such that on an upper side of the droplet damping tray no liquid layer is formed by the liquid dripping down from the packing disposed above and that, driven by gravity, the liquid moves through the droplet damping tray and again exits from a bottom side of the droplet damping tray,
wherein the droplet damping tray comprises a random packed bed or stacked packing arranged between a supporting grid and a hold-down grid,
wherein the liquid distributor tray comprises at least one gas chimney for the flux of the gas phase through the liquid distributor tray and the droplet damping tray,
wherein the droplet damping tray is disposed below an upper point of the at least one gas chimney.

2. The liquid redistributor according to claim 1 , wherein the void volume of the random packed bed or the stacked packing is at least 50 vol-%.

3. The liquid redistributor according to claim 1 , wherein a layer height of the random packed bed or the stacked packing lies between 10 and 800 mm.

4. The liquid redistributor according to claim 1 , wherein the distance between the liquid distributor tray and the droplet damping tray lies between 0 and 500 mm.

5. The liquid redistributor according to claim 1 , wherein the droplet damping tray is disposed below one of the two packings.

6. The liquid redistributor according to claim 1 , wherein the droplet damping tray is located below a point where the flux of the gas phase exits the at least one gas chimney, such that no flux of the gas phase is directed upwards into the droplet damping tray.

7. A packing column for carrying out a thermal separation process, wherein the packing column comprises at least one liquid redistributor according to claim 1 .

8. A method for carrying out a thermal separation process using a packing column as claimed in claim 7 , wherein the thermal separation process is selected from the group consisting of distillation, rectification, extractive distillation, and absorption.

9. The method as claimed in claim 8 , wherein the thermal separation process is absorption, wherein the absorption comprises a method for the absorption of 1,3-butadiene from a C 4 hydrocarbon mixture by a liquid mixture of N-methylpyrrolidone and up to 15 wt-% of water as selective solvent, wherein the packing column is equipped with a reflux and in a lower part of the packing column is designed as packing column and in its upper part as tray column, wherein below the packings a gas phase consisting of the C 4 -hydrocarbon mixture, and directly above the packings a liquid phase consisting of the solvent is introduced into the column, wherein the gas phase rises in the column and the 1,3-butadiene contained therein is absorbed by the liquid phase flowing down through the packings and wherein the gas phase is loaded with solvent, wherein the solvent in the upper part of the column equipped with trays is washed out from the gas phase by the reflux, wherein as top product a C 4 hydrocarbon mixture containing only traces of 1,3-butadiene and as bottom product the solvent loaded with 1,3-butadiene is obtained, wherein the packing column further comprises the liquid redistributor according to claim 1 .

Assignees

• Air Liquide

Inventors

• Eck Thomas
• Kirsten Klaus

Classifications

• B01D53/1487

  Removing organic compounds · CPC title

• B01D3/008 Primary

  Liquid distribution · CPC title

• B01D53/185 Primary

  Liquid distributors · CPC title

• B01J19/32

  Packing elements in the form of grids or built-up elements for forming a unit or module inside the apparatus for mass or heat transfer · CPC title