Systems and methods for analyzing the characteristics and compositions of cement additives

Patent metadata

Field	Value
Publication number	US-10344197-B2
Application number	US-201415313283-A
Country	US
Kind code	B2
Filing date	Aug 26, 2014
Priority date	Aug 26, 2014
Publication date	Jul 9, 2019
Grant date	Jul 9, 2019

Abstract

Optical analysis systems and methods may be used for analyzing the characteristics, including compositions, of cement additives, which may be used in formulating a cement slurry. For example, a cement additive may be optically interacting with an integrated computational element (“ICE”) configured to detect a characteristic of the cement additive. An output signal may then be generated corresponding to the characteristic of the cement additive detected by the ICE, which may be received and processed with a signal processor to yield a value for the characteristic of the cement additive. The value of the characteristic of the cement additive may then be used to determine an amount of the cement additive for use in producing a cement slurry.

First claim

The invention claimed is:

1. A method comprising:
optically interacting a cement additive with a first integrated computational element (“ICE”) configured to detect a first characteristic of the cement additive, wherein the cement additive includes two or more active components, and wherein the first characteristic is a relative concentration of the two or more active components in the cement additive;
generating an output signal corresponding to the first characteristic of the cement additive detected by the first ICE;
receiving and processing the output signal with a signal processor to yield a value for the first characteristic of the cement additive; and
determining an amount of the cement additive for use in producing a cement slurry based, at least in part, on the value of the first characteristic of the cement additive.

2. The method of claim 1 , wherein the first ICE or a second ICE is configured to detect a second characteristic which is a concentration of a degradation product of the cement additive.

3. The method of claim 1 , wherein the first ICE or a second ICE is configured to detect a second characteristic which is a concentration of a contaminant of the cement additive.

4. The method of claim 1 , wherein the cement additive is a liquid concentrate with an active component of the cement additive dispersed in a fluid, wherein the first ICE or a second ICE is configured to detect a second characteristic which is a concentration of the active component in the fluid.

5. The method of claim 1 , wherein the first ICE is configured to detect a relative concentration of a first active component of the two or more active components in the cement additive and a second ICE is configured to detect a relative concentration of a second active component of the two or more active components in the cement additive.

6. The method of claim 1 , wherein optically interacting the cement additive with the first ICE is performed at a well site.

7. The method of claim 1 , further comprising:
optically interacting the cement additive with a second ICE configured to detect a second characteristic of the cement additive that is different than the first characteristic of the cement additive;
generating a second output signal corresponding to the second characteristic of the cement additive detected by the second ICE; and
receiving and processing the second output signal with the signal processor to yield a value for the second characteristic of the cement additive, wherein determining the amount of the cement additive for use in producing the cement slurry is based on the values for the first and second characteristics of the cement additive.

8. The method of claim 7 , wherein the cement additive is produced water, seawater, or saltwater, and wherein the first characteristic is magnesium salt concentration and the second characteristic is pH.

9. The method of claim 7 , wherein the cement additive is produced water, seawater, or saltwater, and wherein the first characteristic is magnesium salt concentration and the second characteristic is total salt concentration.

10. The method of claim 1 , further comprising:
preparing the cement slurry; and
introducing the cement slurry into a wellbore penetrating a subterranean formation.

11. A method comprising:
optically interacting a first cement additive with a first integrated computational element (“ICE”) configured to detect a first characteristic of the first cement additive, wherein the first characteristic is at least one of magnesium salt concentration, clay concentration, salt concentration, and organic matter;
generating an output signal corresponding to the first characteristic of the first cement additive detected by the first ICE;
receiving and processing the output signal with a signal processor to yield a value for the first characteristic of the first cement additive; and
determining a concentration of a second cement additive for use in producing a cement slurry based on the value of the first characteristic of the first cement additive, wherein the second cement additive is at least one of water, a gelling agent, a set accelerator, and a set retarder.

12. The method of claim 11 , wherein the first cement additive is produced water, seawater, or saltwater, wherein the second cement additive is another water source.

13. The method of claim 11 , wherein the first cement additive is water and the method further comprises calculating an estimated salt concentration in the cement slurry based at least in part on the salt concentration in the water.

14. The method of claim 13 , wherein the estimated salt concentration in the cement slurry is greater than 8% and the second cement additive is a set accelerator.

15. The method of claim 13 , wherein the estimated salt concentration in the cement slurry is less than 8% and the second cement additive is a set retarder.

16. The method of claim 11 , further comprising:
preparing the cement slurry; and
introducing the cement slurry into a wellbore penetrating a subterranean formation.

17. An apparatus comprising:
a first integrated computational element configured to optically interact with a cement additive to detect a first characteristic of the cement additive, wherein the cement additive is a liquid concentrate with a first active component of the cement additive dispersed in a fluid, wherein the first characteristic is a concentration of the first active component in the fluid;
a processor;
a computer-readable medium with instructions executable by the processor to cause the apparatus to,
receive and process an output signal corresponding to the first characteristic of the cement additive detected by the first integrated computational element to yield a value for the first characteristic of the cement additive; and
determine an amount of the cement additive for use in producing a cement slurry based on the value of the first characteristic of the cement additive.

18. The apparatus of claim 17 further comprising a second integrated computational element configured to optically interact with the cement additive to detect a second characteristic of the cement additive.

19. The apparatus of claim 18 , wherein the cement additive comprises a second active component, wherein the second characteristic is a concentration of the second active component.

Assignees

• Halliburton Energy Services Inc

Inventors

• Pearl Jr William C
• Pearl Megan Renee

Classifications

• G01N21/85

  Investigating moving fluids or granular solids · CPC title

• G01N21/76

  Chemiluminescence; Bioluminescence · CPC title

• G01N21/31

  Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry {(G01N21/72 takes precedence)} · CPC title

• G01N21/00 Primary

  Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light (G01N3/00 - G01N19/00 take precedence) · CPC title

• G01J2003/1282

  Spectrum tailoring · CPC title