Method for producing a substrate tube of quartz glass

Patent metadata

Field	Value
Publication number	US-10322962-B2
Application number	US-201615197245-A
Country	US
Kind code	B2
Filing date	Jun 29, 2016
Priority date	Jul 3, 2015
Publication date	Jun 18, 2019
Grant date	Jun 18, 2019

Abstract

A method for producing substrate tubes of quartz glass includes continuously supplying a hollow cylinder of quartz glass to a heating zone, softening the hollow cylinder zonewise in the heating zone, and drawing off a tubular strand from the softened portion. The hollow cylinder has an outer diameter Ca, an inner diameter Ci and an inner bore. The tubular strand has an outer diameter Ta and an inner diameter Ti. The following parameters are applicable to the hollow cylinder and the tubular strand: Ca>180 mm, Cr>3 with Cr=Ca/Ci, Tr<1.6 with Tr=Ta/Ti and Ci/Ti<2.5. The blow pressure in an inner bore is adjusted to a value in the range of 4 to 10 mbar. Substrate tubes, obtained by cutting the tubular strand to the desired length, serve as semi-finished products for the manufacture of preforms for optical fibers.

First claim

We claim:

1. A method for producing a substrate tube of quartz glass, comprising:
continuously supplying a hollow cylinder of quartz glass to a heating zone ( 3 ), the hollow cylinder having an outer diameter C a , an inner diameter C i , an inner bore and a wall thickness of at least 62.5 mm;
zonewise softening the hollow cylinder in the heating zone ( 3 ); and
drawing off a tubular strand ( 12 ) from a softened portion of the hollow cylinder, the tubular strand ( 12 ) having an outer diameter T a and an inner diameter T i ,
wherein a blow pressure is produced in an inner bore ( 13 ) is in the range of 4 to 10 mbar, and
wherein the following parameters are applicable to the hollow cylinder ( 4 ) and the tubular strand ( 12 ):
C a >180 mm,
C r >3 with C r =C a /C i ,
T r <1.6 with T r =T a /T i ,
C i /T i <2.5, and
C r /T r >1.88.

2. The method according to claim 1 , wherein the blow pressure is in the range of 6 to 8 mbar, and wherein the following parameters are applicable to the hollow cylinder:
Ca< 300 mm, and
C i /T i <2.

3. The method according to claim 1 , wherein the following parameters are applicable to the tubular strand:
28 mm< Ta< 50 mm, and
T r <1.3.

4. The method according to claim 1 , wherein the following parameters are applicable to the hollow cylinder and the tubular strand:
3.5< Cr< 4.5, and
C r >T r +2.4.

5. The method according to claim 1 , wherein the inner bore of the hollow cylinder has an inner wall that has a surface roughness defined by a roughness value R z >1 μm.

6. The method according to claim 1 , wherein the hollow cylinder has an outer wall that has a surface roughness defined by a roughness value R z >4 μm.

7. The method according to claim 1 , wherein a heating tube ( 1 ) is used that comprises a circular heating space ( 3 ) which is bounded by an inner wall and which defines a heating space volume V Heiz within which the hollow cylinder ( 4 ), a drawing bulb ( 11 ) and the tubular strand ( 12 ) occupy a cylinder space volume V c , where V Heiz >2.5×V c .

8. The method according to claim 7 , wherein an annular gap with a mean gap width in the range of 15 mm and 25 mm remains between the inner wall of the heating zone and the hollow cylinder ( 4 ).

9. The method according to claim 7 , wherein the heating tube ( 1 ) has a length L between 150 mm and 200 mm.

10. The method according to claim 1 , wherein the outer diameter T a of the tubular strand is in the range of 28 mm to not more than 35 mm and a throughput volume is in the range of 10 to 20 kg/h.

11. The method according to claim 1 , wherein the outer diameter T a of the tubular strand is in the range of 35 mm to 50 mm and a throughput volume is in the range of 20 to 30 kg/h.

12. The method according to claim 1 , wherein the tubular strand is drawn off at an elongation ratio of less than 150.

13. The method according to claim 1 , wherein the tubular strand is drawn off at an elongation ratio in the range between 50 and 130.

Assignees

• Heraeus Quarzglas

Inventors

• Ganz Oliver
• Hain Harald

Classifications

• C03B23/047 Primary

  by drawing ({C03B23/091} , C03B37/025 takes precedence) · CPC title

• C03B2205/40

  Monitoring or regulating the draw tension or draw rate · CPC title

• C03B37/01245

  by drawing and collapsing · CPC title

• C03B37/01242 Primary

  Controlling or regulating the down-draw process · CPC title

• Y02P40/50

  Glass production, e.g. reusing waste heat during processing or shaping · CPC title