Water soluble fluorescent or colored dyes and methods for their use
US-2016341736-A1 · Nov 24, 2016 · US
US10288554B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10288554-B2 |
| Application number | US-201615008302-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jan 27, 2016 |
| Priority date | Jan 27, 2016 |
| Publication date | May 14, 2019 |
| Grant date | May 14, 2019 |
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A moisture detecting bleeder material includes a fiberglass material and a moisture absorption indicator material. The moisture absorption indicator material is a component of the fiberglass material and undergoes a color change from a first color to a second color when exposed to moisture. The color change may be thermally irreversible below a threshold temperature (e.g., below a temperature of 450° F.).
Opening claim text (preview).
What is claimed is: 1. A method comprising: applying a plurality of layers to a composite repair area, the plurality of layers including a moisture detecting bleeder material that includes a moisture absorption indicator material, wherein an area of the moisture absorption indicator material is larger than or coextensive with the composite repair area, and wherein a color change of the moisture absorption indicator material from a first color to a second color is indicative of moisture absorption by the moisture absorption indicator material; applying a bagging film to the composite repair area, the bagging film including a fluid interface; performing a moisture removal operation that includes applying a pressure that is less than an ambient pressure to the fluid interface; removing the bagging film to expose the moisture detecting bleeder material; and evaluating the moisture detecting bleeder material to determine whether the color change occurred. 2. The method of claim 1 , wherein the moisture detecting bleeder material includes a bleeder cloth, a bleeder mat, or a combination thereof. 3. The method of claim 1 , wherein the plurality of layers includes a porous release film layer in contact with the moisture detecting bleeder material. 4. The method of claim 1 , wherein the plurality of layers further includes: a porous release film layer between the moisture detecting bleeder material and the composite repair area; and a breather layer overlying the moisture detecting bleeder material. 5. The method of claim 1 , wherein the color change is thermally irreversible below a temperature of 450° F. 6. The method of claim 1 , wherein the moisture absorption indicator material includes a metal halide material. 7. The method of claim 6 , wherein the metal halide material is a component of a silica gel. 8. The method of claim 6 , wherein the metal halide material includes a chloride material, a bromide material, or a combination thereof. 9. The method of claim 6 , wherein the metal halide material includes nickel, cobalt, or a combination thereof. 10. The method of claim 1 , further comprising after determining that the color change occurred: applying a composite repair formulation to the composite repair area; after applying the composite repair formulation, applying the plurality of layers to the composite repair area; applying the bagging film to the composite repair area; performing a curing operation that includes heating the composite repair formulation; removing the bagging film to expose the moisture detecting bleeder material; and evaluating the moisture detecting bleeder material to determine whether the color change occurred. 11. The method of claim 10 , further comprising determining that moisture incursion occurred during the curing operation when the color change occurred. 12. The method of claim 10 , wherein the composite repair formulation includes one or more volatile components, and wherein exposure of the moisture absorbing indicator material to the one or more volatile components does not result in the color change from the first color to the second color. 13. The method of claim 10 , wherein the plurality of layers further includes: a porous release film layer between the moisture detecting bleeder material and the composite repair area; a solid release film layer, wherein the moisture detecting bleeder material is between the porous release film layer and the solid release film layer; and a breather layer overlying the solid release film layer. 14. The method of claim 10 , wherein the color change is thermally irreversible below a threshold temperature of 450° F., and wherein the composite repair formulation is heated to a curing temperature that does not exceed the threshold temperature. 15. A method comprising: applying a composite repair formulation to a composite repair area; after applying the composite repair formulation, applying a plurality of layers to the composite repair area, the plurality of layers including a moisture detecting bleeder material that includes a moisture absorption indicator material and a porous release film layer between the moisture detecting bleeder material and the composite repair area, wherein the porous release film layer is directly coupled to the moisture detecting bleeder material, and wherein a color change of the moisture absorption indicator material from a first color to a second color is indicative of moisture absorption by the moisture absorption indicator material; applying a bagging film to the composite repair area; performing a curing operation that includes heating the composite repair formulation; removing the bagging film to expose the moisture detecting bleeder material; and evaluating the moisture detecting bleeder material to determine whether the color change occurred.
Fibre-reinforced materials (B29C66/729 takes precedence) · CPC title
involving the assembly of discrete sheets or panels only · CPC title
by measuring or controlling the humidity · CPC title
Heating, or preheating, e.g. drying (B29C66/3464 takes precedence) · CPC title
Heat-activated adhesive (B32B37/04 takes precedence) · CPC title
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