Dissolution of oxidized cellulose and particle preparation by solvent and non-solvent precipitation
US-9447196-B2 · Sep 20, 2016 · US
US10287404B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10287404-B2 |
| Application number | US-201514915545-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jun 15, 2015 |
| Priority date | Jun 13, 2014 |
| Publication date | May 14, 2019 |
| Grant date | May 14, 2019 |
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The present application relates to a polymer particle manufacturing method, and according to an example of the manufacturing method and a manufacturing apparatus therefor, a reduction in energy can be achieved by simplifying a manufacturing process thereof.
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The invention claimed is: 1. A polymer particle manufacturing method, comprising: manufacturing a first polymer solution including a polymer dissolved in a first solvent; heating a manufactured first polymer solution to (T m +5) ° C. or above, wherein T m is a melting point (° C.) of the polymer; and mixing a second solvent with a heated first polymer solution, wherein the temperature of the second solvent to be mixed with the first polymer solution is adjusted to at or below a crystallization temperature of the polymer, and wherein the crystallization temperature of the polymer is lower than the T m , and wherein a mixture solution of the first polymer solution and the second solvent is a non-emulsion. 2. The polymer particle manufacturing method of claim 1 , wherein the first solvent is a good solvent with respect to the polymer. 3. The polymer particle manufacturing method of claim 1 , wherein the first solvent has a Hansen relative energy difference of 0.6 or more and less than 2, with respect to the polymer at room temperature. 4. The polymer particle manufacturing method of claim 1 , wherein the first solvent is a monovalent alcohol having 6 or more carbons. 5. The polymer particle manufacturing method of claim 1 , wherein the second solvent has a Hansen relative energy difference of more than 2 and less than 5 with respect to the polymer at room temperature. 6. The polymer particle manufacturing method of claim 1 , wherein the second solvent is a monovalent alcohol having 5 or less carbons, or ketone. 7. The polymer particle manufacturing method of claim 1 , wherein the first solvent is a monovalent alcohol and the second solvent is a monovalent alcohol or ketone. 8. The polymer particle manufacturing method of claim 1 , wherein the polymer is a polyolefin. 9. The polymer particle manufacturing method of claim 1 , wherein the temperature of the second solvent to be mixed with the first polymer solution is adjusted to a range of (T b -70) ° C. to T b ° C., wherein T b is a boiling point (° C.) of the second solvent. 10. The polymer particle manufacturing method of claim 1 , further comprising adjusting a temperature of the mixture solution of the first polymer solution and the second solvent to a range of (T b -35) ° C. to T b ° C., wherein T b is a boiling point (° C.) of the second solvent. 11. The polymer particle manufacturing method of claim 1 , further comprising cooling the mixture solution of the first polymer solution and the second solvent.
Polyolefins · CPC title
Porosity · CPC title
Polyethene · CPC title
Use of anti-solvent · CPC title
Powdering or granulating · CPC title
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