Lubricant for metal powder metallurgy, method of producing same, metal powder composition, and method of producing metal powder metallurgy product

Patent metadata

Field	Value
Publication number	US-10259040-B2
Application number	US-201414764603-A
Country	US
Kind code	B2
Filing date	Feb 4, 2014
Priority date	Feb 5, 2013
Publication date	Apr 16, 2019
Grant date	Apr 16, 2019

Abstract

The lubricant for metal powder metallurgy of the present invention realizes low rattler values and low densities without inhibition of the lubricity, and can provide green bodies and sintered bodies free of cracking, chipping, and density imbalances.

First claim

The invention claimed is:

1. A lubricant for metal powder metallurgy, consisting of particulates that contain (A) an amide compound represented by formula (3) below, (B) an amide compound represented by formula (4) below, and (C) an amide compound represented by formula (5) below or formula (6) below, wherein particulates with a particle diameter larger than 198 μm are less than 1 mass % and particulates with a diameter of 10 μm or less are not more than 10 mass %,
R 4 —CONH CH 2 q NHCO—R 5   (3)

wherein, R 4 and R 5 each independently represent a C 13-27 straight-chain alkyl group and q represents a number from 1 to 6,
R 6 —CONH 2   (4)

wherein, R 6 represents a C 13-27 straight-chain alkyl group,
R 7 —CONH CH 2 r NHCO—R 8   (5)

wherein, R 7 and R 8 each independently represent a C 13-27 alkenyl group or branched alkyl group and n represents a number from 1 to 6,
R 9 —CONH 2   (6)

wherein, R 9 represents a C 13-27 alkenyl group.

2. The lubricant for metal powder metallurgy according to claim 1 , wherein the maximum particle diameter is not more than 100 μm and particulates with a particle diameter of 10 μm or less are not more than 1 mass %.

3. The lubricant for metal powder metallurgy according to claim 2 , wherein an amount of component (B) is 3 to 20 mass parts and an amount of component (C) is 0.3 to 5 mass parts with reference to 10 mass parts of component (A).

4. A method of producing the lubricant for metal powder metallurgy according to claim 3 , the method comprising: melt-mixing the amide compound, and then spraying the mixture to form particulates.

5. A metal powder composition comprising 0.01 to 10 mass parts of the lubricant for metal powder metallurgy according to claim 3 , added to 100 mass parts of metal particles having a median diameter of 5 to 300 μm.

6. A method of producing a metal powder metallurgy product, the method comprising: mixing 0.01 to 10 mass parts of the lubricant for metal powder metallurgy according to claim 3 , with 100 mass parts of metal particles having a median diameter of 5 to 300 μm; press molding the mixture to obtain a green body having a relative density, with respect to an ingot material having the same component composition as the metal particles, of not more than 90%; and sintering the green body to obtain a sintered body.

7. A method of producing the lubricant for metal powder metallurgy according to claim 2 , the method comprising: melt-mixing the amide compound, and then spraying the mixture to form particulates.

8. A metal powder composition comprising 0.01 to 10 mass parts of the lubricant for metal powder metallurgy according to claim 2 , added to 100 mass parts of metal particles having a median diameter of 5 to 300 μm.

9. A method of producing a metal powder metallurgy product, the method comprising: mixing 0.01 to 10 mass parts of the lubricant for metal powder metallurgy according to claim 2 , with 100 mass parts of metal particles having a median diameter of 5 to 300 μm; press molding the mixture to obtain a green body having a relative density, with respect to an ingot material having the same component composition as the metal particles, of not more than 90%; and sintering the green body to obtain a sintered body.

10. A method of producing the lubricant for metal powder metallurgy according to claim 1 , the method comprising: melt-mixing the amide compound, and then spraying the mixture to form particulates.

11. A metal powder composition comprising 0.01 to 10 mass parts of the lubricant for metal powder metallurgy according to claim 1 , added to 100 mass parts of metal particles having a median diameter of 5 to 300 μm.

12. A method of producing a metal powder metallurgy product, the method comprising: mixing 0.01 to 10 mass parts of the lubricant for metal powder metallurgy according to claim 1 , with 100 mass parts of metal particles having a median diameter of 5 to 300 μm; press molding the mixture to obtain a green body having a relative density, with respect to an ingot material having the same component composition as the metal particles, of not more than 90%; and sintering the green body to obtain a sintered body.

Assignees

• Adeka Corp
• Adeka Chemical Supply Corp

Inventors

• Mizuno Yukou
• Adachi Kyoushi

Classifications

• C10N2040/00

  Specified use or application for which the lubricating composition is intended · CPC title

• B22F2998/10

  Processes characterised by the sequence of their steps · CPC title

• C10N2030/06

  Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure · CPC title

• C10M2215/0806

  used as base material · CPC title

• C10N2020/06

  Particles of special shape or size · CPC title