Extraction method

Patent metadata

Field	Value
Publication number	US-10252184-B2
Application number	US-201515325850-A
Country	US
Kind code	B2
Filing date	Jun 25, 2015
Priority date	Jul 14, 2014
Publication date	Apr 9, 2019
Grant date	Apr 9, 2019

Abstract

An extracting method includes: an extracting step of extracting a specific component from a material fluid to an extraction agent while allowing the material fluid and the extraction agent to flow in a channel of the extraction unit for each stage; an outflowing step of outflowing a mixture fluid from the channel of the extraction unit for each stage before the extraction of the specific component reaches an extraction equilibrium; and a pH regulating step of regulating the pH of the material fluid separated in a separating step after flowing out of the channel of the extraction unit for a predetermined stage so as to cause a reverse change from a change caused in the pH of the material fluid in the extracting step, before the material fluid is introduced into the channel of the extraction unit for a stage succeeding to the predetermined stage.

First claim

The invention claimed is:

1. An extracting method, comprising:
(I) extracting a specific component from a material fluid to an extraction agent by using an extracting system, which comprises a plurality of extraction units, wherein each extraction unit has a channel configured for extraction and connected with one another to allow the material fluid and the extraction agent to flow in the channel of each extraction unit;
(II) outflowing a mixture fluid containing the material fluid and the extraction agent from the channel of each extraction unit before extraction of the specific component from the material fluid reaches an extraction equilibrium in the channel of each extraction unit;
(III) separating the mixture fluid flown out of the channel of each extraction unit into the material fluid and the extraction agent;
(IV) conveying the material fluid separated in said separating (III) after flowing out of the channel of any one extraction unit to the channel of a subsequent extraction unit;
(V) regulating pH of the material fluid separated in said separating (III) after flowing out of the channel of a predetermined extraction unit so as to cause a reverse change from a change caused in the pH of the material fluid in accordance with the extraction of the specific component in said extracting before introducing the material fluid into the channel of a succeeding extraction unit;
(VI) conveying the extraction agent separated in said separating (III) after flowing out of the channel of any one extraction unit to the channel of a subsequent extraction unit; and
(VII) supplying another extraction agent to the channel of a certain extraction unit different from the subsequent extraction unit in said conveying (VI), wherein the another extraction agent is separately added to the extracting system and has a content of the specific component lower than that in the extraction agent separated in said separating (III).

2. The extracting method according to claim 1 , wherein,
said regulating (V) is performed on each material fluid separated after flowing out of the channel of each extraction unit.

3. The extracting method according to claim 1 , wherein,
each extraction unit comprises a structure comprising a plurality of channel layers,
each channel layer comprises a plurality of microchannels as the channel,
the plurality of channel layers are placed over one another in the structure, and
the plurality of microchannels are arrayed in each channel layer.

4. The extracting method according to claim 3 , wherein the plurality of microchannels include material introduction passages, extraction agent introduction passages, joining portions, and extraction passages.

5. The extracting method according to claim 4 , wherein each extraction unit comprises a material inflow header formed with openings of upstream ends of the material introductions passages, an extraction agent inflow header formed with openings of upstream ends of the extraction agent introduction passages, and an outflow header formed with openings of downstream ends of the extraction passages, where an upstream end and an downstream end refer to an end located on an upstream side and a downstream side in a flow direction of the material fluid, respectively.

Assignees

• Kobe Steel Ltd

Inventors

• Matsuoka Akira
• Noishiki Koji

Classifications

• B01J19/00

  Chemical, physical or physico-chemical processes in general; Their relevant apparatus · CPC title

• B01D11/0496 Primary

  by extraction in microfluidic devices · CPC title

• B01D11/04 Primary

  of solutions which are liquid · CPC title

• B01D11/0484

  Controlling means · CPC title

• B01D11/0492

  Applications, solvents used · CPC title