Method for ultra-dehydrating thickened or pasty biomass products, and equipment for implementing the method

Patent metadata

Field	Value
Publication number	US-10239777-B2
Application number	US-201815891753-A
Country	US
Kind code	B2
Filing date	Feb 8, 2018
Priority date	May 3, 2013
Publication date	Mar 26, 2019
Grant date	Mar 26, 2019

Abstract

The invention relates to a method for ultra-dehydrating thickened or pasty biomass products, in particular sludge from wastewater treatment plants, according to which the products, in particular products having a dryness of 4% to 25%, are subjected to the following steps: hydrothermal carbonization treatment, including pressurization (1, 2) and thermal conditioning (30) for a duration in a closed reactor (4); followed by dehydration of the products by a ram press (12), obtaining a dryness of more than 50%; the temperature of the product upstream from the ram press dehydration being regulated by cooling between 40° C. and 90° C., advantageously to around 70° C., in order to optimize the filterability in the piston press; the steps of the method being performed in a confined space making it possible to prevent the release of smells into the atmosphere.

First claim

The invention claimed is:

1. A method for ultra-dehydrating thickened or pasty products, forming a biomass, wherein the products are subjected to the following steps:
hydrothermal carbonization treatment, comprising a pressurization and a thermal conditioning for a residence time in a closed reactor, followed by a decompression,
then dehydration of the products by a ram press, obtaining a dryness of greater than 50%,
the temperature of the product upstream of the dehydration by the ram press being regulated by cooling between 40° C. and 90° C. in order to optimize the filterability in the ram press,
the steps of the method being carried out in a confined space that makes it possible to prevent the diffusion of odors into the atmosphere,
wherein the ram press is provided in order to carry out a pressing of the products through flexible drains that form filters, which are permeable to the liquid that passes from the outside to the inside of the drains under the effect of the pressure between two plates between which the drains extend, which drains deform when the plates approach one another, whilst the solid materials are retained on the outside of the drains in order to be discharged during the disassembling.

2. The method as claimed in claim 1 , wherein, for the hydrothermal carbonization treatment, the pressurization in the reactor is between 10 and 30 bar and the thermal conditioning is carried out by heating the products between 150° C. and 250° C. in the reactor.

3. The method as claimed in claim 1 , further comprising a preheating of the product before the hydrothermal carbonization treatment.

4. The method as claimed in claim 1 , wherein the hydrothermal carbonization treatment comprises the following additional steps:
an injection of reactant upstream of or into the reactor in order to promote the reaction,
a heating in order to supplement the temperature in the reactor.

5. The method as claimed in claim 1 , wherein the regulation of the temperature of the product upstream of the dehydration is carried out with the aid of a chiller heat exchanger.

6. The method as claimed in claim 1 , wherein a conditioning of the product exiting the ram press is carried out using a crusher or a grinder.

7. The method as claimed in claim 1 , wherein a dedicated cooling of the product exiting the ram press is carried out in order to reduce a temperature of the product.

8. The method as claimed in claim 7 , wherein the temperature of the product is reduced to a value below 40° C.

9. The method as claimed in claim 7 , wherein the dedicated cooling is of indirect type and that it is carried out under vacuum.

10. The method as claimed in claim 1 , wherein a covered and deodorized store of product is created between the hydrothermal carbonization treatment and the ram press.

11. The method as claimed in claim 10 , wherein the automatic start-up of the dehydration phase by the ram press is carried out as a function of the level of product in the store.

12. The method as claimed in claim 1 , wherein a regulated deodorization is carried out during the disassembling phase by a vacuum application enabling a bleeding of the gases or vapors that generate the odors.

13. The method as claimed in claim 12 , wherein the non-condensable gases are subjected to a cooling.

14. The method as claimed in claim 13 , further comprising using the non-condensable gases in a boiler for thermal and odor-treatment purposes.

15. The method as claimed in claim 1 , wherein the temperature of the product upstream of the dehydration by the ram press is regulated by cooling at around 70° C.

16. The method as claimed in claim 1 , wherein the products have a dryness of between 4% to 25% before hydrothermal carbonization treatment.

17. The method as claimed in claim 2 , wherein the pressurization in the reactor is about 20 bar.

Assignees

• Degremont
• Suez Int
• Terranova Energy Gmbh

Inventors

• Pardo Pierre Emmanuel
• Judenne Eric

Classifications

• Y02W10/40

  Valorisation of by-products of wastewater, sewage or sludge processing · CPC title

• C02F2301/063

  Underpressure, vacuum · CPC title

• C02F2301/066

  Overpressure, high pressure · CPC title

• C02F9/00

  Multistage treatment of water, waste water or sewage · CPC title

• C02F2209/42

  Liquid level · CPC title