Process and apparatus for production of a granular urea product

Patent metadata

Field	Value
Publication number	US-10166517-B2
Application number	US-201213984330-A
Country	US
Kind code	B2
Filing date	Feb 28, 2012
Priority date	Mar 10, 2011
Publication date	Jan 1, 2019
Grant date	Jan 1, 2019

Abstract

A process for production of a granular urea product in a fluidized-bed where: small droplets (10) of fresh urea melt are contacted with a cooling medium to form solid particles, said solid particles (11) are contacted with droplets of urea melt (12) which are larger than said germ particles, the solid particles and said droplets forming together larger solid particles (13), and said solid particles further increasing their size step by step and upon contact with droplets of urea melt, until the solid particles reaches a given size, and said solid particles are then subject to a further growing process by contact with liquid droplets now smaller than the solid particles, until a desired size of the granular product is reached.

First claim

The invention claimed is:

1. A process for production of a granular urea product comprising the steps of:
a) contacting droplets of fresh urea melt with a cooling medium to form solid starting particles,
b) contacting said solid starting particles with droplets of urea melt which are larger than said solid starting particles, the solid starting particles and said droplets forming together larger solid particles, and said larger solid particles further increasing their size step-by-step upon contact with larger droplets of urea melt, until the solid particles reach a given size, and
c) subjecting said solid particles to a further growing process by contact with liquid droplets now smaller than the solid particles, until a desired size of the granular product is reached;
wherein said droplets which form the starting particles have an average size equal to or less than 200 μm (0.2 mm).

2. The process according to claim 1 , said droplets which form the starting particles having an average size in a range 50-200 μm (0.05-0.2 mm).

3. The process according to claim 2 , the solid particles obtained after step b) having an average size of around 0.5 mm.

4. The process according to claim 2 , the solid particles obtained after step b) having an average size in the range 0.5 to 1 mm.

5. The process according to claim 1 , a fluidized-bed state being maintained at least in the stage c) of the process with air which also acts as the cooling medium.

6. The process according to claim 5 , the fluidized-bed in the stage c) being a longitudinal fluidized bed with a main flow direction and a double-vortex arrangement with two vortex formed in the fluidized bed having opposite sense of rotation around axes substantially parallel to said main flow direction.

7. Equipment for carrying out a process according to claim 1 , comprising at least:
a first environment;
means adapted to feed at least a first flow of droplets of fresh urea melt and cooling air to said first environment, to cause the formation of solid starting particles,
means to feed at least a second flow of larger droplets of urea melt to said first environment, the droplets of said second flow being larger than droplets of said first flow,
a second environment in communication with the first environment and means for feeding particles formed in the first environment and droplets of urea and fluidizing air to said second environment for granulation of said solid particles under a fluidized-bed state;
wherein the means feeding said first flow of droplets being adapted to deliver droplets with a diameter equal to or less than 200 μm.

8. The equipment according to claim 7 , comprising separate containers delimiting said first environment and second environment, or a single container comprising portions delimiting said first environment and second environment.

9. The equipment according to claim 7 , wherein said means to feed at least a second flow comprises a plurality of flows of larger droplets of urea melt to said first environment.

Assignees

• Bedetti Gianfranco
• Casale Sa

Inventors

• Bedetti Gianfranco

Classifications

• B01J2/16 Primary

  by suspending the powder material in a gas, e.g. in fluidised beds or as a falling curtain · CPC title

• C05C9/005

  Post-treatment · CPC title