Process for manufacturing a milk of slaked lime of great fineness and milk of great fineness thereby obtained

Patent metadata

Field	Value
Publication number	US-10138163-B2
Application number	US-201515323620-A
Country	US
Kind code	B2
Filing date	Sep 7, 2015
Priority date	Sep 8, 2014
Publication date	Nov 27, 2018
Grant date	Nov 27, 2018

Abstract

A process is shown for manufacturing a milk of lime of great fineness which includes at least the steps of providing one lime compound chosen in the group consisting of prehydrated lime, a paste of lime obtained by addition of water to quicklime instead of addition of quicklime to water and their mixture, and forming a milk of slaked lime of great fineness with the chosen lime compound. The paste of lime is obtained by progressive addition of water to quicklime under agitation conditions.

First claim

The invention claimed is:

1. Process for manufacturing a milk of lime of great fineness wherein said milk of lime comprises slaked lime particles in suspension into an aqueous phase, the slaked lime particles having a d 50 greater than or equal to 2 μm and lower than or equal to 6 μm, measured by means of a laser granulometer in methanol, comprising at least the steps of:
(a) adding water to quicklime instead of addition of quicklime to water to obtain a paste of lime and
(b) forming a milk of slaked lime of great fineness with said paste of lime.

2. Process for manufacturing a milk of lime of great fineness according to claim 1 , wherein said paste of lime is obtained by progressive addition of water to quicklime under agitation conditions.

3. Process for manufacturing a milk of lime of great fineness according to claim 2 , wherein said progressive addition of water to quicklime comprises presenting a pattern of addition of water for controlling water uptake by the quicklime when forming the paste of lime.

4. Process for manufacturing a milk of slaked lime of great fineness according to claim 2 , wherein said progressive addition to form the paste of lime is a continuous process during which progressive hydration of quicklime is performed by adjusting quicklime feeding rate into a hydrator wherein a predetermined atmosphere is fed containing a limited amount of water for addition of water to quicklime.

5. Process for manufacturing milk of slaked lime of great fineness according to claim 2 , wherein progressive addition to form the paste of lime is performed by spraying a mist of water into a hydrator.

6. Process for manufacturing milk of slaked lime of great fineness according to claim 5 , wherein said mist of water is a controlled size of droplets of addition of water.

7. Process for manufacturing a milk of lime of great fineness according to claim 1 , wherein water added to form said paste of lime comprises an additive selected from the group consisting of carbohydrates, sugars, alcohol sugars, sorbitol, phosphates, sulfates, bicarbonates, silicates, phosphonates, polyacrylates, polycarboxylic acids, low molecular weight organic acids, mixtures and derivatives thereof.

8. Process for manufacturing a milk of lime of great fineness according to claim 1 , wherein the slaked lime particles have a d 50 greater than or equal to 2.5 μm and lower than or equal to 5.5 μm, measured by means of a laser granulometer in methanol.

9. Process for manufacturing a milk of lime of great fineness according to claim 1 , wherein the step of forming a milk of slaked lime of great fineness with said paste of lime is a step of adding water to the paste of lime.

10. Process for manufacturing a milk of lime of great fineness according to claim 1 , wherein the step of forming a milk of slaked lime of great fineness with said paste of lime is a step of adding paste of lime to water.

11. Process for manufacturing milk of lime of great fineness according to claim 1 , wherein said step of forming a milk of slaked lime of great fineness is a batch step by addition of a predetermined amount of said paste of lime into a predetermined amount of water or by addition of a predetermined amount of water into a predetermined amount of said paste of lime to produce said milk of slaked lime of great fineness.

12. Process for manufacturing milk of lime of great fineness according to claim 1 , wherein said step of forming a milk of slaked lime of great fineness is a continuous step comprising the steps of feeding said paste of lime into a vessel provided with an exit of milk of slaked lime of great fineness and containing an aqueous suspension of lime and feeding said vessel with water and is followed by an exit of said milk of slaked lime of great fineness thereby obtained.

13. Process for manufacturing a milk of slaked lime of great fineness according to claim 1 , wherein the paste of lime is made by a progressive addition of water to quicklime, said progressive addition of water being pursued during the step of forming said milk of slaked lime of great fineness until said milk of slaked lime of great fineness is reached.

14. Process for manufacturing milk of lime of great fineness according to claim 13 , wherein said progressive addition of water is carried out by increasing the amount of water added until said predetermined amount of water of the step of forming said milk of slaked lime of great fineness has been added.

Assignees

• Lhoist Rech Et Developpement Sa

Inventors

• Kutlubay Galen
• Ballard Deborah
• Laurent Bernard
• Querton Augustin

Classifications

• C01P2004/61

  Micrometer sized, i.e. from 1-100 micrometer · CPC title

• C04B2/06 Primary

  with addition of substances, e.g. hydrophobic agents {; Slaking in the presence of other compounds} · CPC title

• C01P2004/03

  obtained by SEM · CPC title

• C01P2006/22

  Rheological behaviour as dispersion, e.g. viscosity, sedimentation stability · CPC title

• C04B28/10

  Lime cements or magnesium oxide cements · CPC title