System and method for cryogenic purification of a feed stream comprising hydrogen, methane, nitrogen and argon
US-10088229-B2 · Oct 2, 2018 · US
US10012439B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10012439-B2 |
| Application number | US-201615285557-A |
| Country | US |
| Kind code | B2 |
| Filing date | Oct 5, 2016 |
| Priority date | Jan 29, 2014 |
| Publication date | Jul 3, 2018 |
| Grant date | Jul 3, 2018 |
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A system and method for the concurrent condensation of a nitrogen-rich vapor and vaporization of an oxygen-rich liquid in a distillation column based air separation unit is provided. The disclosed system includes a condenser-reboiler heat exchanger located between a lower pressure column and a higher pressure column and configured to condense a nitrogen-rich vapor from the higher pressure column and partially vaporize an oxygen-rich liquid from the lower pressure column. Within the condenser-reboiler heat exchanger, the nitrogen-rich vapor flows in an upward direction such that any non-condensables present in the nitrogen-rich vapor will accumulate proximate the upper portion or top of the condenser-reboiler modules where they can be easily removed through venting.
Opening claim text (preview).
What is claimed is: 1. A condensation and vaporization system for an air separation unit comprising: one or more condenser-reboiler modules having a housing defining a top, a bottom, one or more lateral sides, an upper portion, and a lower portion, the one or more condenser-reboiler modules disposed within a lower pressure column and configured to receive a condensing medium at a condensing inlet disposed at the top of the housing, an oxygen-rich liquid from the lower pressure column at an oxygen-rich liquid inlet disposed proximate the top or bottom of the housing, and further defining a condensate outlet proximate the bottom of the housing and an oxygen-rich effluent outlet disposed proximate the top or bottom of the housing; a shell and tube heat exchanger disposed in the one or more condenser-reboiler modules and comprising two opposed tube sheets, a cylindrical shell connecting the two opposed tube sheets, and a plurality of tubes extending between the two opposed tube sheets, the shell and tube heat exchanger configured to partially vaporize the oxygen-rich liquid flowing within the plurality of tubes thereby forming an oxygen-rich effluent and condense the condensing medium within the cylindrical shell forming a condensate; wherein the condensing medium enters the one or more condenser-reboiler modules at the condensing inlet, traverses through the inlet conduit and is released within the shell and tube heat exchanger in the condenser-reboiler modules at the bottom of the cylindrical shell and flows in an upward and radially outward direction within the cylindrical shell; wherein non-condensables present in the condensing medium accumulate at the outer surfaces of the plurality of tubes and proximate the upper portion; and one or more vents disposed proximate the upper portion or top of the housing for the one or more condenser-reboiler modules and configured to remove the accumulated non-condensables proximate the outer surfaces of the plurality of tubes. 2. The system of claim 1 wherein the heat exchanger is a downflow heat exchanger and the oxygen-rich liquid inlet is disposed proximate the top of the housing for the one or more condenser-reboiler modules and the oxygen-rich effluent outlet is disposed proximate the bottom of the condenser-reboiler module. 3. The system of claim 1 wherein the condensate outlet further comprises a plurality of condensate outlet that are disposed proximate the bottom of the housing for the one or more condenser-reboiler modules and concentrically around the condensing medium inlet. 4. The system of claim 1 wherein the condensate outlet is disposed proximate the bottom of the housing for the one or more condenser-reboiler modules and proximate the lateral side or peripheral edges of the housing. 5. The system of claim 1 further comprising a non-condensable recovery system coupled to the one or more vents and configured to purify and recover the removed non-condensables. 6. The system of claim 1 wherein the condensing medium is a nitrogen-rich vapor. 7. The system of claim 1 wherein the condensing medium is an air vapor.
in a reboiler-condenser, e.g. within a column · CPC title
Boiler-condenser with multiple exchanger cores in parallel or with multiple re-boiling or condensing streams · CPC title
Down-flowing type boiler-condenser, i.e. with evaporation of a falling liquid film · CPC title
Arrangement of reboiler-condensers · CPC title
Boiler-condenser with superposed stages · CPC title
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