Liquid compositions used as insulating and heat transfer means, electrical devices containing said compositions and preparation method for such compositions
US-9240259-B2 · Jan 19, 2016 · US
US9997273B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9997273-B2 |
| Application number | US-201314654167-A |
| Country | US |
| Kind code | B2 |
| Filing date | Dec 20, 2013 |
| Priority date | Dec 20, 2012 |
| Publication date | Jun 12, 2018 |
| Grant date | Jun 12, 2018 |
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An electrical device containing an enzymatically-degummed vegetable oil is disclosed. Also disclosed are methods for insulating and cooling a transformer using enzymatically-degummed vegetable oils, and methods for adding an enzymatically-degummed vegetable oil to an enclosure of an electrical device. Further disclosed are processes for making dielectric fluids using enzyme-degumming of vegetable oils or using enzyme-degummed vegetable oils as the starting material for the process.
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What is claimed is: 1. A process for manufacturing a dielectric fluid, the process comprising: (a) obtaining an enzymatically-degummed vegetable oil exhibiting a dielectric breakdown of less than 35 kilovolts (kV); and (b) filtering the enzymatically-degummed vegetable oil to produce the dielectric fluid exhibiting an IFT of at least 20 dynes/cm at 25° C., a Dissipation Factor of less than 0.20% at 25° C., an acid value (AV) of less than 0.09 milligrams KOH/gram, and a dielectric breakdown of at least 35 kilovolts (kV). 2. The process of claim 1 , wherein the enzymatically-degummed vegetable oil obtained for step (a) is a refined, bleached and deodorized vegetable oil. 3. The process of claim 1 , wherein dielectric fluid exhibits a Dissipation Factor of less than 0.15% at 25° C. 4. The process of claim 1 , wherein the process further includes a step (c) dewatering the enzymatically-degummed vegetable oil to reduce the water content of the dielectric fluid to 200 milligrams per kilogram of oil or less. 5. The process of claim 1 , wherein the water content of the dielectric fluid is 50 milligrams per kilogram oil or less. 6. The process of claim 1 , wherein the process further includes (d) degassing the enzymatically-degummed vegetable oil. 7. The process of claim 1 , wherein the dielectric fluid exhibits a dielectric breakdown of at least 50 kilovolts (kV). 8. The process of claim 1 , wherein the dielectric fluid exhibits an acid value (AV) of 0.06 milligrams KOH/gram or less. 9. The process of claim 1 , wherein the enzyme-degummed oil of step (a) exhibits a Dissipation Factor of greater than 0.20 percent at 25° C. 10. The process of claim 1 , wherein the vegetable oil is selected from the group consisting of at least one of a rapeseed oil, a corn oil, a mustard oil, an olive oil, a palm oil, a palm kernel oil, a peanut oil, a safflower oil, a sesame oil, a soybean oil, a nut oil, a cottonseed oil, a crambe oil, a coconut oil, a meadowfoam oil, a vernonia oil, a lesquerella oil, a jatropha oil, a jojoba oil, a grape seed oil, a sunflower oil, and mixtures thereof. 11. A process for manufacturing a dielectric fluid, the process comprising: (a) obtaining an enzymatically-degummed vegetable oil exhibiting a dielectric breakdown of less than 35 kilovolts (kV); and (b) filtering the enzymatically-degummed vegetable oil to produce the dielectric fluid exhibiting an IFT of at least 20 dynes/cm at 25° C., a Dissipation Factor of less than 0.20% at 25° C., an acid value (AV) of less than 0.09 milligrams KOH/gram, and a dielectric breakdown of at least 35 kilovolts (kV), wherein the dielectric fluid consists essentially of the enzymatically-degummed vegetable oil. 12. The process of claim 11 , wherein the dielectric fluid comprises an additive selected from the group consisting of antioxidants, pour point depressants, antimicrobial agents, dyes, and mixtures thereof.
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