Preparation method of titanium alloy powders
US-12083602-B2 · Sep 10, 2024 · US
US9994947B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9994947-B2 |
| Application number | US-201514711291-A |
| Country | US |
| Kind code | B2 |
| Filing date | May 13, 2015 |
| Priority date | Jul 16, 2014 |
| Publication date | Jun 12, 2018 |
| Grant date | Jun 12, 2018 |
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A method for producing a Ti-6Al-4V article, includes providing a work piece of a Ti-6Al-4V alloy having a beta-transus temperature; subjecting the work piece to a beta solution heat treatment process in a furnace with a vacuum at a temperature above the beta transus; quenching the work piece in the furnace using high pressure inert gas following the subjecting of the work piece in the beta solution heat treatment process; and subjecting the work piece to an overage heat treatment process in the furnace with a vacuum to overage the work piece following the quenching of the work piece. The work piece can be a bolt blank that is further manufactured into a titanium bolt with pre-machined wave form threads and wave form rolling process utilized to manufacture threads into the bolt blank.
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What is claimed is: 1. A method for producing an alpha-beta titanium alloy article, comprising: providing a work piece of an alpha-beta titanium alloy having a beta transus; subjecting the work piece to a beta solution heat treatment process in a furnace with a vacuum at a temperature above the beta transus; quenching the work piece in the furnace using pressurized inert gas following the subjecting of the work piece in the beta solution heat treatment process; subjecting the work piece to an overage heat treatment process in the furnace with a vacuum to overage the work piece following the quenching of the work piece; cooling the work piece in a pressurized inert gas following the subjecting of the overage heat treatment process; wherein the work piece is processed during each of the beta solution heat treatment process, pressurized inert gas quenching, overage heat treatment process, and pressurized inert gas cooling without removal from the furnace; and manufacturing threads into the work piece using a pre-machined wave formed thread pattern prior to thread rolling. 2. The method of claim 1 , further comprising surface cleaning the work piece using one of abrasive media blasting, acid etching, or solvent emulsion cleaning prior to the beta solution heat treatment process. 3. The method of claim 1 or 2 , further comprising beta solution heat treating the work piece at a temperature in a range of about 50 degrees Fahrenheit to about 100 degrees Fahrenheit above the beta transus generally greater than 1875 degrees Fahrenheit for a time period between 30 and 60 minutes. 4. The method of claim 1 , further comprising quenching the work piece in one of a pressurized helium or argon inert gas that is configured to maintain a cooling rate of at least 280 degrees Fahrenheit per minute. 5. The method of claim 1 or 4 , further comprising quenching the work piece using the pressurized inert gas at a pressure in a range of about 200 kilopascals to about 400 kilopascals that is configured to lower a temperature of the work piece to below 600 degrees Fahrenheit. 6. The method of claim 1 , wherein the cooling includes cooling the work piece in one of a pressurized helium or argon inert gas that is configured to lower a temperature of the work piece to below 175 degrees Fahrenheit. 7. The method of claim 1 or 6 , further comprising pressurizing the furnace at a pressure in a range of about 200 kilopascals to about 400 kilopascals during the cooling of the work piece. 8. The method of claim 1 , wherein subjecting the work piece to an overage heat treatment process includes subjecting the work piece to a temperature in a range of about 1100 degrees Fahrenheit to about 1400 degrees Fahrenheit in a vacuum for about 2.5 hours to about 3 hours. 9. The method of claim 1 , wherein the manufacturing of the threads further comprises creating the threads using one of a conventional thread rolling process or a wave form thread rolling process. 10. The method of claim 1 , 2 , 4 , 6 , or 8 , where the alpha-beta titanium alloy is a Ti-6Al-4V alloy. 11. The method of claim 1 , wherein the article is a bolt. 12. The method of claim 1 , wherein the work piece is upset forged from a bar or rod to form a bolt head prior to subjecting the work piece to the beta solution heat treatment process.
by rapid cooling or quenching; cooling agents used therefor · CPC title
of titanium or alloys based thereon · CPC title
Alloys based on titanium · CPC title
in inert or controlled atmosphere or vacuum (adjusting the composition of the atmosphere C21D1/76) · CPC title
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