Method of fabricating a composite material part with improved intra-yarn densification

Patent metadata

Field	Value
Publication number	US-9988750-B2
Application number	US-201314395118-A
Country	US
Kind code	B2
Filing date	Apr 11, 2013
Priority date	Apr 17, 2012
Publication date	Jun 5, 2018
Grant date	Jun 5, 2018

Abstract

A method of fabricating a composite material part comprises fiber reinforcement densified by a matrix. The method comprises the following steps: making a fiber fabric by weaving yarns having an initial mean fiber percentage; and densifying the fiber fabric with a matrix. The fiber fabric is subjected, prior to densification, to one or more jets of water under pressure so as to reduce the mean fiber percentage in the fabric to a value lying in the range 20% to 45%.

First claim

The invention claimed is:

1. A method of fabricating a thermostructural composite material part comprising fiber reinforcement densified by a matrix, said method comprising the following steps:
providing a fiber fabric of three-dimensionally woven warp yarns and weft yarns in which at least some of the warp yarns interlink weft yarns over a plurality of weft layers, said fiber fabric having a determined initial mean fiber percentage;
reducing a mean fiber percentage in the fiber fabric to a value lying in the range 20% to 45% by subjecting said fiber fabric to one or more water jets under pressure, each of the one or more water jets being delivered from a corresponding nozzle;
densifying the fiber fabric with a matrix;
wherein the step of reducing the mean fiber percentage in the fiber fabric is performed prior to densifying the fiber fabric,
wherein, in the step of reducing the mean fiber percentage, the pressure of each of the one or more water jets at the outlet from each of the one or more nozzles is less than or equal to 100 bars,
wherein each of the one or more nozzles is at a distance from the surface of the fiber fabric that is greater than or equal to 50 mm, and
wherein densification of the fiber fabric includes chemical vapor infiltration (CVI) of the matrix into said fiber fabric.

2. A method according to claim 1 , wherein the fiber fabric is a multilayer fabric made by three-dimensional weaving of continuous yarns of carbon fibers, of silicon carbide fibers, or of oxide fibers.

3. A method according to claim 1 , wherein it comprises, prior to densifying the fiber fabric, depositing an interphase on the fibers of said fiber fabric.

4. A method according to claim 1 , wherein densifying the fiber fabric comprises using a liquid technique to infiltrate a matrix into said fiber fabric.

5. A method according to claim 1 , wherein the matrix is a ceramic matrix selected from the group consisting: an oxide; a nitride; a carbide; and a silicide.

6. A method according to claim 5 , wherein the ceramic matrix comprises at least silicon carbide and boron or a boron compound.

7. A method according to claim 1 , further comprising a step of shaping and consolidating the fiber fabric after the step of reducing the mean fiber percentage in the fiber fabric and before the step of densifying said fiber fabric.

8. A method according to claim 1 , wherein the pressure of the water jet at the outlet of each of the one or more nozzles is about 80 bars.

9. A method according to claim 1 , wherein the nozzle have an outlet diameter of about 0.127 mm.

10. A method according to claim 1 , wherein the fiber fabric has a thickness in the range of 1 mm to 2 mm before treating the fiber fabric by subjecting the fiber fabric to the one or more jets of water under pressure.

11. A method according to claim 1 , further comprising a step of impregnating the fiber fabric with a liquid consolidation composition.

12. A method according to claim 11 , wherein the liquid consolidation composition is a resin that is a precursor for silicon carbide.

13. A method according to claim 11 , further comprising a step of shaping the impregnated fiber fabric by molding.

14. A method according to claim 13 , further comprising a step of subjecting the shaped the fiber fabric to a heat treatment, after the fiber fabric has been shaped.

15. A method according to claim 14 , wherein the step of densifying the fiber fabric is performed by chemical vapor infiltration, after the fiber fabric has been shaped.

16. The method according to claim 1 , wherein the mean fiber percentage in the fiber fabric is calculated on a basis of a weight per unit area of the fiber fabric, a density of the fibers of the fiber fabric, and a thickness of the fiber fabric, based on the formula:

Fiber
⁢

⁢
percentage

=

weight
⁢

⁢
per
⁢

⁢
unit
⁢

⁢
area

fiber
⁢

⁢
density
×
fabric
⁢

⁢
thickness

.

17. The method according to claim 1 , wherein the step of reducing the mean fiber percentage in the fiber fabric includes subjecting a first face of said fiber fabric with water under said pressure, and subjecting a second face of said fiber fabric with water under said pressure.

18. The method according to claim 1 , wherein the step of reducing the mean fiber percentage in the fiber fabric includes subjecting said fiber fabric with said one or more jets of water under pressure in a first pass, and subsequently subjecting said fiber fabric with said one or more jets of water under pressure in a second pass.

19. The method according to claim 1 , wherein the step of densifying the fiber fabric includes depositing the matrix in both inter-yarn pores present between the woven yarns of the fiber fabric and within intra-yarn pores formed between filaments of each of the woven yards, the intra-yarn pores being made available for deposition of the matrix within the intra-yarn pores by the step of reducing the mean fiber percentage in the fiber fabric.

20. The method according to claim 1 , wherein, in the step of reducing mean fiber percentage in the fiber fabric, yarns present at a surface of the fiber fabric subjected to the one or more jets of fluid are essentially preserved without breaking.

21. The method according to claim 1 , wherein the water pressure at each of the one or more nozzles is less than 100 bars.

22. A method of fabricating a thermostructural composite material, said method comprising the steps:
providing a fiber fabric with three-dimensionally woven warp yarns and weft yarns in which at least some of the warp yarns interlink weft yarns over a plurality of weft layers, said fiber fabric having a determined initial mean fiber percentage;
reducing the mean fiber percentage in the fiber fabric to a value lying in a range of 20% to 45%; and
densifying the fiber fabric with a matrix,
wherein said step of reducing the mean fiber percentage is performed before the step of densifying the fiber fabric with the matrix,
wherein, in the step of reducing the mean fiber percentage in the fiber fabric, a first face of the fiber fabric is subjected to one or more jets of water under pressure, each of the one or more jets of water being delivered from a corresponding nozzle, and a second face of the fiber fabric is subjected to said one or more jets of water under pressure, and
wherein densificat

Assignees

• Herakles

Inventors

• Fillion Arnaud
• Philippe Eric
• Charleux Francois
• Bouillon Eric

Classifications

• D06C29/00

  Finishing or dressing, of textile fabrics, not provided for in the preceding groups · CPC title

• C04B2235/5268

  Orientation of the fibers · CPC title

• C04B2237/365

  Silicon carbide · CPC title

• C04B2235/614

  Gas infiltration of green bodies or pre-forms · CPC title

• C04B2237/38

  Fiber or whisker reinforced · CPC title