Method of sterilizing preform and method of sterilizing container made of resin

Patent metadata

Field	Value
Publication number	US-9988170-B2
Application number	US-201515329328-A
Country	US
Kind code	B2
Filing date	Sep 18, 2015
Priority date	Sep 25, 2014
Publication date	Jun 5, 2018
Grant date	Jun 5, 2018

Abstract

A sterilization process is performed on a preform or container made of resin after a corona discharge treatment is performed on an inner surface of the preform or container, the corona discharge treatment including applying a voltage produced in a corona discharge to an electrode that passes through an opening part of the preform or container, an insertion step of inserting the electrode to which the voltage is applied into the preform or container through the opening part, and a bottom part treatment step of treating an inner surface of a bottom part of the preform or container by bringing the electrode close to the bottom part until the corona discharge from the electrode changes discharge mode, and the sterilization process including a hydrogen peroxide supplying step of blasting a mist or gas of hydrogen peroxide solution or a mixture thereof to the preform or container.

First claim

The invention claimed is:

1. A method of sterilizing a preform, wherein a sterilization process is performed on a preform that is made primarily of polyethylene terephthalate after a corona discharge treatment is performed on an inner surface of the preform, the corona discharge treatment including a voltage application step of applying a voltage produced in a corona discharge to an electrode that is capable of passing through an opening part of the preform, an insertion step of inserting the electrode to which the voltage is applied into the preform through the opening part, and a bottom part treatment step of treating an inner surface of a bottom part of the preform by bringing the electrode close to the bottom part until the corona discharge from the electrode changes discharge mode, and the sterilization process including a hydrogen peroxide supplying step of blasting a mist or gas of hydrogen peroxide solution or a mixture thereof to the preform.

2. The method of sterilizing a preform according to claim 1 , wherein the corona discharge treatment is performed with a grounded conductor being provided around at least a part of the outside of the preform.

3. The method of sterilizing a preform according to claim 2 , wherein the corona discharge treatment is performed with an insulator being provided between the preform and the conductor.

4. The method of sterilizing a preform according to claim 3 , wherein the corona discharge treatment is performed with the insulator protruding beyond the conductor in a direction toward the opening part of the preform.

5. The method of sterilizing a preform according to claim 1 , wherein the corona discharge treatment is performed by bringing the electrode close to the inner surface of the bottom part of the preform while rotating the electrode and the preform with respect to each other about a central axis in the direction toward the opening part of the preform.

6. The method of sterilizing a preform according to claim 1 , wherein the corona discharge treatment is performed so that a contact angle with water of the surface of the preform is equal to or less than 75 degrees.

7. The method of sterilizing a preform according to claim 1 , wherein the mist or gas of hydrogen peroxide or mixture thereof is blasted to the preform after the preform is preliminarily heated by blasting heated air into the preform and blasting heated air to a thick part of the preform from outside of the preform.

8. The method of sterilizing a preform according to claim 1 , wherein the mist or gas of hydrogen peroxide or mixture thereof is produced by injecting a hydrogen peroxide solution and aseptic air into an evaporator from a twin fluid nozzle.

9. A method of sterilizing a container made of resin, wherein a sterilization process is performed on a container made of resin after a corona discharge treatment is performed on an inner surface of the container made of resin, the corona discharge treatment including a voltage application step of applying a voltage produced in a corona discharge to an electrode that is capable of passing through an opening part of the container made of resin, an insertion step of inserting the electrode to which the voltage is applied into the container made of resin through the opening part, and a bottom part treatment step of treating an inner surface of a bottom part of the container made of resin by bringing the electrode close to the bottom part until the corona discharge from the electrode changes discharge mode, and the sterilization process including a hydrogen peroxide supplying step of blasting a mist or gas of hydrogen peroxide solution or a mixture thereof to the container made of resin.

10. The method of sterilizing a container made of resin according to claim 9 , wherein the opening part of the container made of resin is narrow, and the corona discharge treatment is performed on the inner surface of the container made of resin by an electrode that is expanded after the electrode enters the container made of resin through the opening part.

11. The method of sterilizing a container made of resin according to claim 9 , wherein the corona discharge treatment is performed with a grounded conductor being provided around at least a part of the outside of the container made of resin.

12. The method of sterilizing a container made of resin according to claim 11 , wherein the corona discharge treatment is performed with an insulator being provided between the container made of resin and the conductor.

13. The method of sterilizing a container made of resin according to claim 12 , wherein the corona discharge treatment is performed with the insulator protruding beyond the conductor in a direction toward the opening part of the container made of resin.

14. The method of sterilizing a container made of resin according to claim 9 , wherein the corona discharge treatment is performed by bringing the electrode close to the inner surface of the bottom part of the container made of resin while rotating the electrode and the container made of resin with respect to each other about a central axis in the direction toward the opening part of the container made of resin.

15. The method of sterilizing a container made of resin according to claim 9 , wherein at least the inner surface of the container made of resin is made of polyolefin or polyethylene terephthalate.

16. The method of sterilizing a container made of resin according to claim 9 , wherein the corona discharge treatment is performed so that a contact angle with water of the surface of the container made of resin is equal to or less than 75 degrees.

17. The method of sterilizing a container made of resin according to claim 9 , wherein the mist or gas of hydrogen peroxide or mixture thereof is blasted to the container made of resin after the container made of resin is preliminarily heated by blasting heated air into the container made of resin and blasting heated air to a thick part of the container made of resin from outside of the container made of resin.

18. The method of sterilizing a container made of resin according to claim 9 , wherein the mist or gas of hydrogen peroxide or mixture thereof is produced by injecting a hydrogen peroxide solution and aseptic air into an evaporator from a twin fluid nozzle.

19. The method of sterilizing a container made of resin according to claim 9 , wherein the sterilization process includes an air rinsing step performed after the hydrogen peroxide supplying step.

20. The method of sterilizing a container made of resin according to claim 9 , wherein the sterilization process includes a water rinsing step performed after the hydrogen peroxide supplying step.

Assignees

• Dainippon Printing Co Ltd

Inventors

• Sato Yoshinori
• Tsuchiya Hirotaka

Classifications

• A61L2103/23

  Containers other than laboratory or medical, e.g. bottles or mail · CPC title

• B65B31/025

  specially adapted for rigid or semi-rigid containers (B65B31/021, B65B31/022 take precedence) · CPC title

• A61L2/186

  Peroxide solutions · CPC title

• B65B7/2835

  applying and rotating preformed threaded caps (for bottles or jars B67B3/20) · CPC title

• B65B55/10 Primary

  by liquids or gases · CPC title