Hydrogel encapsulations and methods of making the same
US-2024180220-A1 · Jun 6, 2024 · US
US9974720B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9974720-B2 |
| Application number | US-201615381145-A |
| Country | US |
| Kind code | B2 |
| Filing date | Dec 16, 2016 |
| Priority date | Dec 30, 2015 |
| Publication date | May 22, 2018 |
| Grant date | May 22, 2018 |
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A microcapsule composition containing microcapsules coated with a deposition protein, e.g., a protein-silanol copolymer, a protein-silane copolymer, a protein-siloxane copolymer, or a cationically modified protein, is provided as is a method for making the microcapsule composition and using the microcapsule composition in consumer products, in particular rinse-off consumer product.
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What is claimed is: 1. A method for preparing a microcapsule composition comprising: (a) providing a microcapsule slurry having a plurality of microcapsules each containing a polymeric wall and an active material encapsulated within the polymeric wall; (b) curing the microcapsules; and (c) coating each of the microcapsules with a deposition protein, wherein the deposition protein is cross-linked on the surface of the microcapsules (i) at a temperature between 35 to 75° C. after curing the microcapsules or (ii) by adding an alkoxysilane after step (b); and the active material contains a fragrance, pro-fragrance, flavor, malodor counteractive agent, anti-inflammatory agent, anesthetic, analgesic, anti-viral agent, anti-infectious agent, anti-acne agent, skin lightening agent, insect repellant, emollient, skin moisturizing agent, vitamin or derivative thereof, or any combination thereof. 2. The method of claim 1 , wherein the microcapsules are coated with the deposition protein at a temperature between 35 to 75° C. 3. The method of claim 1 , further comprising step (d) adding a second deposition aid after step (b). 4. The method of claim 1 , wherein the deposition protein is a cationically modified protein. 5. The method of claim 4 , wherein the cationically modified protein is a protein-acrylate copolymer having a nitrogen-containing acrylic moiety. 6. The method of claim 5 , wherein the nitrogen-containing acrylic moiety comprises a tertiary or quaternary amine group. 7. The method of claim 1 , wherein the deposition protein is cross-linked on the surface of the microcapsules using the alkoxysilane. 8. The method of claim 1 , wherein the plurality of microcapsules are prepared by cross-linking a polyisocyanate with an activation agent selected from the group consisting of an amine cross-linker, an alcohol cross-linker, an epoxy cross-linker, an acrylate cross-linker, a hybrid cross-linker, and a combination thereof. 9. The method of claim 1 , wherein the deposition protein is a modified vegetable protein, wheat protein, marine collagen protein, keratin protein, silk protein, or milk protein. 10. The method of claim 1 , wherein the deposition protein has a molecular weight in the range of 1000 to 500,000. 11. The method of claim 1 , wherein the microcapsule composition comprising a second deposition aid selected from the group consisting of anionically, cationically, nonionically, or amphoteric water-soluble polymers. 12. A microcapsule composition prepared by the method of claim 1 . 13. A consumer product comprising the microcapsule composition of claim 12 . 14. The consumer product of claim 13 , further comprising one or more different microcapsules, free active material, or a combination thereof. 15. The consumer product of claim 13 , wherein the consumer product is a shampoo, hair conditioner, body wash, detergent, softener, bar soap, scent booster, or hard surface cleaner.
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