Measuring tensile strength of tight rock using electromagnetic heating

Patent metadata

Field	Value
Publication number	US-9970852-B2
Application number	US-201514920273-A
Country	US
Kind code	B2
Filing date	Oct 22, 2015
Priority date	Oct 23, 2014
Publication date	May 15, 2018
Grant date	May 15, 2018

Abstract

A method for determining the tensile strength of a rock sample comprising the steps of obtaining the rock sample, measuring a water content of the rock sample through a water measurement method, determining a matrix bulk modulus of the rock sample, wherein the matrix bulk modulus is determined through a matrix modulus method, heating the rock sample with electromagnetic energy such that the electromagnetic energy heats the water content in the rock sample from an initial temperature, wherein heating the water content causes a pore-water pressure of the rock sample to increase, detecting a break in the rock sample with a sensor, wherein the increase in the pore-water pressure causes the rock sample to break, wherein the break occurs at a break time, at a break temperature; and calculating the pore-water pressure through the water content, the matrix bulk modulus, and the break temperature of the water content.

First claim

We claim:

1. A method for determining the tensile strength of a rock sample, the method comprising the steps of:
obtaining the rock sample;
measuring a water content of the rock sample, wherein the water content is measured through a water measurement method , wherein the water measurement method is selected from the group consisting of NMR measurement, dielectric measurement, a gravimetric method, Dean-Stark analysis, and combinations thereof;
determining a matrix bulk modulus of the rock sample, wherein the matrix bulk modulus is determined through a matrix modulus method, wherein the matrix modulus method is selected from the group consisting of experimental methods, estimation methods based on individual components, and combinations thereof;
heating the rock sample with electromagnetic energy such that the electromagnetic energy heats the water content in the rock sample from an initial temperature, wherein heating the water content causes a pore-water pressure of the rock sample to increase, wherein the electromagnetic energy is produced by an electromagnetic wave source, wherein the electromagnetic wave source produces electromagnetic energy in the range between 1 kHz and 300 GHz;
detecting a break in the rock sample with a sensor while heating the rock sample with the electromagnetic energy, wherein the increase in the pore-water pressure causes the rock sample to break,
wherein the break occurs at a break time,
wherein the break occurs at a break temperature;

determining the break temperature; and
calculating the pore-water pressure at the break time from the water content, the matrix bulk modulus, and the break temperature of the water content, wherein the tensile strength of the rock sample is the pore-water pressure at which the break occurs.

2. The method of claim 1 , wherein the rock sample is selected from the group consisting of shale, tight shale, tight organic-rich shale, sandstone, tight sandstone, carbonate rock, tight carbonate rock, and cement.

3. The method of claim 1 , wherein the sensor is selected from the group consisting of acoustic sensors, temperature sensors, and strain gauges.

4. The method of claim 1 , wherein the rock sample is subjected to a confining stress, wherein the confining stress is selected from the group consisting of a vice and a clamp.

5. The method of claim 1 , wherein the electromagnetic wave source produces electromagnetic energy in the range between 1 GHz and 50 GHz.

6. The method of claim 1 , wherein the rock sample is saturated with saturation water, the saturation water operable to increase the water content of the rock sample.

7. The method of claim 1 , wherein the estimation method based on the individual component is selected from the group consisting of a Reuss approach and a Voigt approach.

8. A method for determining the tensile strength of a rock sample, the method comprising the steps of:
obtaining the rock sample;
heating the rock sample with electromagnetic energy such that the electromagnetic energy heats a water content in the rock sample from an initial temperature, wherein heating the water content causes a temperature-dependent pressure in the rock sample to increase, wherein the electromagnetic energy is produced by an electromagnetic wave source, wherein the electromagnetic wave source produces electromagnetic energy in the range between 1 kHz and 300 GHz;
detecting a break in the rock sample with a sensor while heating the rock sample with the electromagnetic energy, wherein the increase in the temperature-dependent pressure causes the rock sample to break,
wherein the break occurs at a break time,
wherein the break occurs at a break temperature;

determining the break temperature; and
calculating the temperature-dependent pressure at the break time, wherein the temperature -dependent pressure is calculated based on a difference between the break temperature and the initial temperature of the rock sample, wherein the tensile strength of the rock sample is the temperature-dependent pressure at which the break occurs.

9. The method of claim 8 , wherein the rock sample is selected from the group consisting of shale, tight shale, tight organic-rich shale, sandstone, tight sandstone, carbonate rock, tight carbonate rock, and cement.

10. The method of claim 8 , wherein the difference between the break temperature and the initial temperature of the rock sample is calculated based on the temperature change of a water content of the rock sample, wherein the water content is measured through a water measurement method, wherein the water measurement method is selected from the group consisting of NMR measurement, dielectric measurement, a gravimetric method, Dean-Stark analysis, and combinations thereof.

11. The method of claim 8 , wherein the temperature-dependent pressure is modified based on determining a matrix bulk modulus of the rock sample, wherein the matrix bulk modulus is determined through a matrix modulus method, wherein the matrix modulus method is selected from the group consisting of experimental methods, estimation methods based on individual components, and combinations thereof.

12. The method of claim 11 , wherein the estimation method based on the individual component is selected from the group consisting of a Reuss approach and a Voigt approach.

13. The method of claim 8 , wherein the sensor is selected from the group consisting of acoustic sensors, temperature sensors, and strain gauges.

14. The method of claim 8 , wherein the rock sample is subjected to a confining stress, wherein the confining stress is selected from the group consisting of a vice and a clamp.

15. The method of claim 8 , wherein the electromagnetic wave source produces electromagnetic energy in the range between 1 GHz and 50 GHz.

16. The method of claim 8 , wherein the rock sample is saturated with saturation water, the saturation water operable to increase the water content of the rock sample.

Assignees

• Aramco Services Co
• Saudi Arabian Oil Co

Inventors

• Chen Jinhong
• Georgi Daniel
• Davis Lorne
• Liu Hui-Hai

Classifications

• G01N33/24

  Earth materials (G01N33/42 takes precedence) · CPC title

• G01N3/18

  Performing tests at high or low temperatures · CPC title

• G01N33/246

  for water content · CPC title

• G01N3/60 Primary

  Investigating resistance of materials, e.g. refractory materials, to rapid heat changes {(thermal testing of structures or apparatus G01M99/002)} · CPC title

• G01N2203/0057

  using stresses due to heating, e.g. conductive heating, radiative heating · CPC title