Experimental device for simulating exploitation of natural gas hydrate in permeable boundary layer

Patent metadata

Field	Value
Publication number	US-9970267-B2
Application number	US-201414765475-A
Country	US
Kind code	B2
Filing date	Nov 5, 2014
Priority date	Oct 20, 2014
Publication date	May 15, 2018
Grant date	May 15, 2018

Abstract

A device for simulating exploitation of a natural gas hydrate in a permeable boundary layer includes a high pressure reaction kettle, a formation simulation unit and an aquifer maintaining unit. A water bath jacket externally connected with constant temperature water bath is arranged on the outer wall of the high pressure reaction kettle for providing a necessary temperature condition for the high pressure reaction kettle. A simulative well at the center of the top of the high pressure reaction kettle is connected with liquid injection, gas injection, gas production and water production equipment. An aquifer interface at the bottom of the high pressure reaction kettle is connected to the aquifer maintaining unit through a pipeline. The simulation device simulates the geological environment of a hydrate reservoir, allowing comprehensive evaluation of hydrate exploitation under different formation permeability and different formation pressure gradients.

First claim

The invention claimed is:

1. A device for simulating exploitation of a natural gas hydrate in a permeable boundary layer, comprising:
a high pressure reaction kettle;
a formation simulation unit;
an aquifer maintaining unit;
a water bath jacket externally connected with a constant temperature water bath and arranged on the outer wall of the high pressure reaction kettle for providing a necessary temperature condition for the high pressure reaction kettle;
a simulative well externally connected with a liquid injection, a gas injection, a gas production and a water production equipment and arranged at a center of a top of the high pressure reaction kettle; and
an aquifer interface arranged at the bottom of the high pressure reaction kettle, the formation simulation unit being arranged in the high pressure reaction kettle, and the aquifer maintaining unit is connected with the aquifer interface through a pipeline,
wherein the aquifer maintaining unit comprises:
a nitrogen cylinder;
a pressure reducing valve;
a gas booster pump;
a high pressure gas storage tank;
a first pressure control valve;
a low pressure gas storage tank;
a second pressure control valve;
a liquid storage container;
an electronic balance;
a constant-flux pump; and
a liquid storage tank,

wherein the bottom of the liquid storage tank is connected with the aquifer interface through a pipeline so as to be connected with the aquifer for supplementing water in the aquifer and maintaining the pressure of the aquifer,
wherein the nitrogen cylinder is connected with the high pressure gas storage tank through the pressure reducing valve and the gas booster pump in sequence,
wherein the high pressure gas storage tank is connected with the liquid storage tank through the first pressure control valve, and high pressure nitrogen is injected from the high pressure gas storage tank into the liquid storage tank through the first pressure control valve to maintain the pressure of the aquifer and simulate the pressure difference of the aquifer and the hydrate layer,
wherein the liquid storage container is placed on the electronic balance, and the liquid storage container is connected with the liquid storage tank through the constant-flux pump for supplementing water to the liquid storage tank, and
wherein the top of the liquid storage tank is connected with the low pressure gas storage tank through the second pressure control valve.

2. The device for simulating exploitation of the natural gas hydrate in the permeable boundary layer of claim 1 ,
wherein an interior of the high pressure reaction kettle is cylindrical, and
further comprising a confining pressure jacket arranged in the high pressure reaction kettle, the confining pressure jacket being connected with a confining pressure pump through a confining pressure interface to control a confining pressure through the confining pressure pump.

3. The device for simulating exploitation of the natural gas hydrate in the permeable boundary layer of claim 2 , wherein the formation simulation unit comprises:
a hydrate layer;
a low permeability layer; and
an aquifer,
the hydrate layer, the low permeability layer and the aquifer being arranged in the confining pressure jacket from top to bottom, and the confining pressure is loaded to avoid gas and water streaming between different simulative formations.

4. The device for simulating exploitation of the natural gas hydrate in the permeable boundary layer of claim 3 , wherein quartz sand is filled in the hydrate layer, and a necessary solution and a necessary gas are injected through the simulative well to form the hydrate.

5. The device for simulating exploitation of the natural gas hydrate in the permeable boundary layer of claim 3 , wherein the low permeability layer is a ceramic plate, and a permeability and a thickness of the ceramic plate are prepared according to experimental requirements.

6. The device for simulating exploitation of the natural gas hydrate in the permeable boundary layer of claim 3 , wherein the aquifer is a porous conglomerate.

7. The device for simulating exploitation of the natural gas hydrate in the permeable boundary layer of claim 3 , wherein a liquid level meter is arranged in the liquid storage tank for measuring the residual water amount in the liquid storage tank.

8. The device for simulating exploitation of the natural gas hydrate in the permeable boundary layer of claim 7 , wherein when the residual water amount in the liquid storage tank is smaller than ⅓, water in the liquid storage container is injected into the liquid storage tank through the constant-flux pump for supplementing water to the liquid storage tank.

9. The device for simulating exploitation of the natural gas hydrate in the permeable boundary layer of claim 8 , wherein when supplementing water to the liquid storage tank, the first pressure control valve is closed, meanwhile the second pressure control valve is opened to inject the gas exhausted by the water into the low pressure gas storage tank to maintain the stable pressure of the liquid storage tank and the aquifer,
wherein a seepage quantity from the aquifer to the hydrate layer is calculated according to a pressure change and a water injection amount measured by the liquid level meter, using the following formula:
Q=W 1 −W 2 +W i

where:
Q: seepage quantity from the aquifer to the hydrate layer;
W1: initial water amount of the liquid storage tank;
W2: real-time water amount of the liquid storage tank; and
Wi: water injection amount of the liquid storage tank in the experiment process.

Assignees

• Guangzhou Inst Energy Conversion Cas

Inventors

• Li Xiaosen
• Zhang Yu
• Wang Yi
• Li Gang
• Chen Zhaoyang
• Xu Chungang

Classifications

• G01N33/24

  Earth materials (G01N33/42 takes precedence) · CPC title

• G01N15/0826

  and measuring fluid flow rate, i.e. permeation rate or pressure change · CPC title

• E21B41/0099

  specially adapted for drilling for or production of natural hydrate or clathrate gas reservoirs; Drilling through or monitoring of formations containing gas hydrates or clathrates · CPC title

• E21B43/01 Primary

  specially adapted for obtaining from underwater installations · CPC title

• C10L2290/60

  Measuring or analysing fractions, components or impurities or process conditions during preparation or upgrading of a fuel · CPC title