Method for producing surface-modified fluororesin film/thermoplastic resin composite
US-9410021-B2 · Aug 9, 2016 · US
US9962676B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9962676-B2 |
| Application number | US-201514674183-A |
| Country | US |
| Kind code | B2 |
| Filing date | Mar 31, 2015 |
| Priority date | Nov 17, 2009 |
| Publication date | May 8, 2018 |
| Grant date | May 8, 2018 |
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Disclosed herein is a method of: treating an organic polymer with an electron beam-generated plasma; exposing the treated polymer to air or an oxygen- and hydrogen-containing gas, generating hydroxyl groups on the surface of the polymer; reacting the surface with an organosilane compound having a chloro, fluoro, or alkoxy group and a functional or reactive group that is less reactive with the surface than the chloro, fluoro, or alkoxy group; and covalently immobilizing a biomolecule to the functional or reactive group or a reaction product thereof.
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What is claimed is: 1. A method comprising: treating an organic polymer microtitre plate with an electron beam-generated plasma; exposing the treated plate to air or an oxygen- and hydrogen-containing gas; wherein the treating and exposing generates hydroxyl groups on the surface of the plate. 2. The method of claim 1 ; wherein the plasma is generated in argon; wherein the argon gas pressure is 90 mTorr+/10%; wherein the treatment time is 2 min+/10%; wherein the electron beam is pulsed at 50 Hz+/−10%; and wherein the electron beam is operated with pulse width of 2 ms+/−10%.
Treatment by wave energy or particle radiation (C08J7/18 takes precedence) · CPC title
by plasma treatment {(plasma tubes per se H01J)} · CPC title
Light-directed synthesis · CPC title
with ligand attached to the carrier via a chemical coupling agent (coatings G01N33/54393) · CPC title
Polystyrene · CPC title
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