Reverse filling carbon and temperature drop-in sensor

Patent metadata

Field	Value
Publication number	US-9958427-B2
Application number	US-201514942180-A
Country	US
Kind code	B2
Filing date	Nov 16, 2015
Priority date	Jan 21, 2015
Publication date	May 1, 2018
Grant date	May 1, 2018

Abstract

A drop-in probe for determining phase changes by thermal analysis of a sample of a molten metal includes a measurement head having a first end which is an immersion end and an opposing second end having an end face. A sample chamber is arranged within the measurement head. An opening, which is free of any restrictions and which is in communication with the sample chamber, is formed in the end face of the second end of the measurement head. The sample chamber includes a first thermocouple having a first thermocouple junction enclosed within a wall which has a uniform internal geometry. A ratio D/H of an internal diameter D of the sample chamber to a length H extending between the opening and the first thermocouple junction is between 0.1 and 1.2.

First claim

We claim:

1. A drop-in probe for determining phase changes by thermal analysis of a sample of a molten metal, the drop-in probe comprising:
a measurement head including a first end which is an immersion end and an opposing second end having an end face; and
a sample chamber arranged within the measurement head, an opening in communication with the sample chamber being formed in the end face of the second end of the measurement head, the opening being free of any restrictions, the sample chamber including a first thermocouple having a first thermocouple junction enclosed within a wall, the wall having a uniform internal geometry,
wherein, a ratio D/H of an internal diameter D of the sample chamber to a length H extending between the opening and the first thermocouple junction is between 0.1 and 1.2, and
wherein, when the sample chamber is filled with a sample of the molten metal, a ratio of a mass of the metal accommodated in the sample chamber to a mass of the wall of the sample chamber is between 0.25 and 1.25.

2. The drop-in probe according to claim 1 , wherein the ratio D/H is 0.3.

3. The drop-in probe according to claim 1 , further comprising a second thermocouple having a second thermocouple junction at the immersion end of the measurement head.

4. The drop-in probe according to claim 1 , further comprising an extension tube emerging from second end of the measurement head and a signal cable extending through the extension tube and exiting therefrom at an outlet opening.

5. The drop-in probe according to claim 4 , wherein the extension tube is made of a material selected from the group consisting of a metal, a plastic, a rubber, a paper material and a woven material.

6. The drop-in probe according to claim 1 , wherein an in-situ density of the measurement head, with the sample chamber being empty, is greater than 5 g/cm 3 .

7. The drop-in probe according to claim 1 , wherein an in-situ density of the measurement head, with the sample chamber being filled with the molten metal, is less than 6.5 g/cm 3 .

8. The drop-in probe according to claim 1 , further comprising a cushion cap attached to the immersion end.

9. The drop-in probe according to claim 1 , further comprising a protective cap covering the opening.

10. The drop-in probe according to claim 9 , wherein the cap is made of aluminum.

Assignees

• Heraeus Electro Nite Int

Inventors

• Turner Paul A
• Clauss Jr Harry G

Classifications

• G01N1/125

  adapted for sampling molten metals · CPC title

• G01N33/205 Primary

  in liquid state, e.g. molten metals · CPC title

• G01K7/02 Primary

  using thermoelectric elements, e.g. thermocouples · CPC title

• B22D2/006

  for the temperature of the molten metal (measuring temperature in general G01K) · CPC title

• B22D2/00

  Arrangement of indicating or measuring devices, e.g. for temperature or viscosity of the fused mass · CPC title