Apparatus for measuring rheological parameters and methods for its operation

Patent metadata

Field	Value
Publication number	US-9958367-B2
Application number	US-201414783811-A
Country	US
Kind code	B2
Filing date	Apr 9, 2014
Priority date	Apr 9, 2013
Publication date	May 1, 2018
Grant date	May 1, 2018

Abstract

An apparatus for measuring rheological parameters of a multi-phase fluid is provided. The apparatus includes a static chamber containing a multi-phase fluid having at least a first phase and a second phase. The apparatus also includes a rotor member submersed in the multiphase fluid in the static chamber. The rotor member includes a first set of threads formed on a first portion of the rotor member submersed in the first phase of the multi-phase fluid and a second set of threads formed on a second portion of the rotor member submersed in the second phase of the multi-phase fluid.

First claim

We claim:

1. An apparatus for measuring rheological parameters of a multi-phase fluid, the apparatus comprising:
a static chamber containing a multi-phase fluid having at least a first phase and a second phase; and
a rotor member submersed in the multi-phase fluid in the static chamber and rotatable about a rotational axis within the static chamber, wherein the rotor member comprises a first set of threads formed on a first portion of the rotor member submersed in the first phase of the multi-phase fluid and a second set of threads formed on a second portion of the rotor member submersed in the second phase of the multi-phase fluid, wherein the first phase of the multi-phase fluid is disposed above the second phase of the multi-phase fluid, wherein the first set of threads is disposed above the second set of threads, and wherein a pitch and a depth of the first set of threads and the second set of threads are selected based upon a density and viscosity of each of the first phase and the second phase of the multi-phase fluid, a required degree of mixing, or combinations thereof.

2. The apparatus of claim 1 , wherein the static chamber and the rotor member are coaxial.

3. The apparatus of claim 1 , wherein the static chamber is formed of stainless steel, hastelloy, or combinations thereof.

4. The apparatus of claim 1 , wherein the rotor member is formed of stainless steel, hastelloy, or combinations thereof.

5. The apparatus of claim 1 , wherein at least one of the first set of threads and the second set of threads comprises acme threads, buttress threads, whitworth threads, V-threads, or combinations thereof.

6. The apparatus of claim 1 , wherein the first phase of the multi-phase fluid is a liquid and the second phase of the multi-phase fluid is a gas.

7. The apparatus of claim 1 , wherein the first phase of the multi-phase fluid is a solid and the second phase of the multi-phase fluid is a liquid.

8. The apparatus of claim 1 , wherein the first phase of the multi-phase fluid is a liquid, second phase of the multi-phase fluid is a solid and a third phase of the multi-phase fluid is a gas.

9. The apparatus of claim 1 , wherein the static chamber and the rotor member define a shear zone containing the multi-phase fluid, wherein a shear stress is applied to the multi-phase fluid by rotating the rotor member.

10. The apparatus of claim 1 , wherein a pitch of the first set of threads and the second set of threads is about 0.1 mm to about 25 mm.

11. The apparatus of claim 1 , wherein a ratio of pitch to a length of the first set of threads and the second set of threads is about 0.01 to 0.5.

12. The apparatus of claim 1 , wherein a depth of the first set of threads and the second set of threads is about 0.1 mm to about 25 mm.

13. The apparatus of claim 1 , wherein the ratio of depth to the diameter of the first set of threads and second set of threads is about 0.01 to 0.5.

14. The apparatus of claim 1 , wherein a degree of mixing of the first phase and the second phase is about 1% to about 99%.

15. The apparatus of claim 1 , wherein the multi-phase fluid comprises at least two immiscible fluids.

16. The apparatus of claim 15 , wherein the multi-phase fluid comprises oil and water.

17. The apparatus of claim 1 , further comprising a processing circuitry configured to estimate the rheological parameters of the multi-phase fluid based on an applied shear rate, a temperature of the multi-phase fluid, a pressure of the multi-phase fluid, or combinations thereof.

18. The apparatus of claim 17 , wherein the rheological parameters of the multi-phase fluid comprise a viscosity, a shear storage modulus, a shear loss modulus, or combinations thereof.

19. The apparatus of claim 1 , wherein the first set of threads and the second set of threads are oppositely angled.

20. The apparatus of claim 10 , wherein a thread angle of the first set of threads is about 5 degrees to about 70 degrees.

21. The apparatus of claim 10 , wherein a thread angle of the second set of threads is between 5 degrees and 70 degrees.

22. The apparatus of claim 1 , further comprising a motor configured to rotate the rotor member about the rotational axis.

23. The apparatus of claim 22 , wherein a speed of rotation of the rotor member is about 0.01 rpm to about 10000 rpm.

24. The apparatus of claim 22 , wherein an applied shear rate is about 10 −5 S −1 to about 10 7 S −1 .

25. An apparatus for measuring rheological parameters of a multi-phase fluid, the apparatus comprising:
a static chamber containing a multi-phase fluid having at least a first phase and a second phase;
a rotor member submersed in the multi-phase fluid in the static chamber and rotatable about a rotational axis within the static chamber to apply a shear stress to the multi-phase fluid, wherein the rotor member comprises a first portion having a first set of threads formed thereon in a first direction and a second portion having a second set of threads formed thereon in a second direction that is opposite to the first direction; and
a processing circuitry configured to estimate the rheological parameters of the multi-phase fluid as the rotor member is rotated within the static chamber,
wherein the first phase of the multi-phase fluid is disposed above the second phase of the multi-phase fluid, and wherein the first set of threads is disposed above the second set of threads,
and wherein a height of the first portion and a height of the second portion of the rotor member are determined based upon a volume of the first phase and a volume of the second phase respectively.

26. The apparatus of claim 25 , wherein the first portion and the second portion of the rotor member are substantially submersed in the first phase and the second phase of the multi-phase fluid respectively.

27. The apparatus of claim 25 , wherein the multi-phase fluid comprises a third phase.

28. The apparatus of claim 27 , wherein the rotor member comprises a third un-threaded portion disposed between the first portion and the second portion, wherein the third un-threaded portion is substantially submersed in the third phase of the multi-phase fluid.

29. A method for measuring rheological parameters of a multi-phase fluid, the method comprising:
providing a static chamber having a rotor member, wherein the rotor member comprises a first portion having a first set of threads formed thereon in a first direction and a second portion having a second set of threads formed thereon in a second direction that is opposite to the first direction;
placing a multi-phase fluid having a first phase and a second phase within the static chamber such that the first portion and the second portion of the rotor member are substantially submersed in the first phase and the second phase of the multi-phase fluid respectively; and
rotating the rotor member about a rotational axis to apply shear stress to the first phase and the second phase of the multi-phase fluid through the first set of threads and the second set of threads respectively,
wherein the first phase of the multi-phase fluid is disposed above the second phase of the multi-phase fluid, and wherein the first set of threads is disposed above the second set of threads,
and wherein a height of the first portion and a height of the second portion of the rotor member are determined based upon a volume of the first p

Assignees

• Indian Institute Of Tech Madras

Inventors

• Sangwai Jitendra
• Khalde Chirag

Classifications

• F04C2/22

  of internal-axis type with equidirectional movement of co-operating members at the points of engagement, or with one of the co-operating members being stationary, the inner member having more teeth or tooth-equivalents than the outer member · CPC title

• G01N11/00 Primary

  Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties · CPC title

• G01N2011/0033

  Yield stress; Residual stress at zero shear rate · CPC title

• F04C18/16

  with helical teeth, e.g. chevron-shaped, screw type {(for non-parallel axes of movement F04C18/48)} · CPC title

• G01N11/14 Primary

  by using rotary bodies, e.g. vane (G01N11/16 takes precedence) · CPC title