Column for thermal treatment of a fluid

Patent metadata

Field	Value
Publication number	US-9958201-B2
Application number	US-201514817351-A
Country	US
Kind code	B2
Filing date	Aug 4, 2015
Priority date	Aug 5, 2014
Publication date	May 1, 2018
Grant date	May 1, 2018

Abstract

The present disclosure includes a column ( 1 ) having a cylindrical, vertical column body ( 2 ) forming a column cavity ( 3 ), and a mass transfer tray ( 4 ) disposed in the column cavity ( 3 ) and forming a collecting area ( 5 ). The column ( 1 ) is characterized by a circulation device ( 9 ) having at least one drain orifice ( 10 ) formed in the column body ( 2 ) above the collecting area ( 5 ), a circulation line ( 11 ) in fluid connection with the drain orifice ( 10 ) and at least one recycling orifice ( 14; 14 - 1 to 14 - 3 ) which is in fluid connection with the circulation line ( 11 ) and is formed in the column body ( 2 ) above the collecting area ( 5 ). Also disclosed herein is a thermal separating process in which a gas ascends within a column ( 1 ) of the present disclosure, and a liquid descends within the column ( 1 ), said gas and/or liquid containing (meth)acrylic monomers.

First claim

The invention claimed is:

1. A column for thermal treatment of a fluid, the column comprising:
a cylindrical, vertical column body which forms a column cavity;
a mass transfer tray which is disposed in the column cavity and forms a collecting area;
a circulation device having, at east one drain orifice formed in the column body above the collecting area;
a circulation line in fluid connection with the drain orifice; and
at least one recycling orifice which is in fluid connection with the circulation line and is formed in the column body above the collecting area,
wherein:
a plurality of mass transfer trays are arranged with vertical spacing in the column cavity, and the drain orifice and the recycling orifice are arranged vertically between two adjacent mass transfer trays with vertical spacing; and
the ratio of the vertical separation of the lowest region of the collecting area of the mass transfer tray from the lower edge of the drain orifice to the vertical separation of the lowest region of the collecting area of the mass transfer tray from the underside of the mass transfer tray disposed directly above is within a range from 0 to 0.3.

2. The column according to claim 1 , wherein the recycling orifice opens into the column cavity above the drain orifice.

3. The column according to claim 1 , wherein a nozzle for producing a liquid jet on entry of the liquid into the column cavity is disposed in the recycling orifice.

4. The column according to claim 1 , wherein the circulation line and the recycling orifice are arranged such that the liquid recycled enters the column cavity radially.

5. The column according to claim 1 , wherein a plurality of spaced-apart recycling orifices are formed in the column body, each of which is in fluid connection with the circulation line.

6. The column according to claim 1 , wherein the mass transfer tray has passage orifices for gas ascending from the bottom, and cylindrical bodies extend upward in the passage orifices.

7. The column according to claim 6 , wherein the recycling orifices are arranged relative to the cylindrical bodies so as to result in a meandering liquid flow on the collecting area of the mass transfer tray.

8. The column according to claim 6 , wherein the mass transfer tray is a chimney tray and the cylindrical body is a chimney body.

9. The column according to claim 1 , wherein the circulation line has an opening for supply of a further liquid.

10. The column according to claim 1 , wherein a pump arranged in the circulation line pumps away liquid that collects on the collecting area of the mass transfer tray and feeds it back to the column cavity through the recycling orifice.

11. A thermal separation process, comprising thermally separating at least one gas ascending within the column of claim 1 and at least one liquid descending within the column.

12. The process according to claim 11 , wherein liquid is introduced via the recycling orifice below the liquid level in the collecting area.

13. The process according to claim 11 , wherein the ascending gas, the descending liquid, or both, comprises at least one (meth)acrylic monomer.

14. The column according to claim 1 , wherein the drain orifice is disposed immediately above the lowermost region of the collecting area of the mass transfer tray.

15. A column for thermal treatment of a fluid, the column comprising:
a cylindrical, vertical column body which forms a column cavity;
a mass transfer tray which is disposed in the column cavity and forms a collecting area;
a circulation device having at least one drain orifice formed in the column body above the collecting area;
a circulation line in fluid connection with the drain orifice; and
at least one recycling orifice which is in fluid connection with the circulation line and is formed in the column body above the collecting area,
wherein the recycling orifice opens into the column cavity at the same height as the drain orifice.

16. A column for thermal treatment of a fluid, the column comprising:
a cylindrical, vertical column body which forms a column cavity;
a mass transfer tray which is disposed in the column cavity and forms a collecting area;
a circulation device having, at least one drain orifice formed in the column body above the collecting area;
a circulation line in fluid connection with the drain orifice;
at least one recycling orifice which is in fluid connection with the circulation line and is formed in the column body above the collecting area,
wherein:
a plurality of mass transfer trays are arranged with vertical spacing in the column cavity, and the drain orifice and the recycling orifice are arranged vertically between two adjacent mass transfer trays with vertical spacing; and
the ratio of the vertical separation of the lowest region of the collecting area of the mass transfer tray from the upper edge of the recycling orifice to the vertical separation of the lowest region of the collecting area of the mass transfer tray from the underside of the mass transfer tray disposed directly above is within a range from 0 to 0.3.

17. A column for thermal treatment of a fluid the column comprising:
a cylindrical, vertical column body which forms a column cavity;
a mass transfer tray which is disposed in the column cavity and forms a collecting area;
a circulation device having at least one drain orifice formed in the column body above the collecting area;
a circulation line in fluid connection with the drain orifice; and
at least one recycling orifice Which is in fluid connection with the circulation line and is formed in the column body above the collecting area,
wherein:
the mass transfer tray has passage orifices for gas ascending from the bottom, and cylindrical bodies extend upward in the passage orifices; and
the upper edges of the cylindrical body are overflow edges and the ratio of the vertical separation of the lowest region of the collecting area of the mass transfer tray from the lower edge of the drain orifice to the vertical separation of the lowest region of the collecting area of the mass transfer tray from the height of the lowermost overflow edge of the cylindrical bodies is within a range from 0 to 0.1.

18. A column for thermal treatment of a fluid, the column comprising:
a cylindrical, vertical column body which forms a column cavity;
a mass transfer tray which is disposed in the column cavity and forms a collecting area;
a circulation device having at least one drain orifice formed in the column body above the collecting area;
a circulation line in fluid connection with the drain orifice; and
at least one recycling orifice which is in fluid connection with the circulation line and is formed in the column body above the collecting area,
wherein:
the mass transfer tray has passage orifices for gas ascending from the bottom, and cylindrical bodies extend upward in the passage orifices; and
the upper edges of the cylindrical body are overflow edges and the ratio of the vertical separation of the lowest region of the collecting area of the mass transfer tray from the upper edge of the recycling orifice to the vertical separation of the lowest region of the collecting area of the mass transfer tray from the height of the lowermost overflow edge of the cylindrical bodies is within a range from 0 to 0.9.

Assignees

• Basf Se

Inventors

• Hammon Ulrich
• Walter Thomas

Classifications

• B01D3/32

  Other features of fractionating columns {; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30} · CPC title

• C07C45/82

  by distillation · CPC title

• C07C67/54 Primary

  by distillation · CPC title

• B01D3/4261

  Side stream · CPC title

• C07C45/80

  by liquid-liquid treatment · CPC title