Oscillating path length spectrometer

Patent metadata

Field	Value
Publication number	US-9952350-B1
Application number	US-201715495512-A
Country	US
Kind code	B1
Filing date	Apr 24, 2017
Priority date	Apr 24, 2017
Publication date	Apr 24, 2018
Grant date	Apr 24, 2018

Abstract

Evaluating a fluid, including transmitting a light beam through the fluid to a detector while oscillating a path length traveled through the fluid by the light beam at a first frequency of oscillation; measuring a time-dependent intensity of incident light at the detector responsive to an interaction of the light beam with the fluid to produce a time-dependent intensity signal; filtering the time-dependent intensity signal to recover a path-dependent signal oscillating at the first frequency and indicative of an absorbance property of the fluid; and estimating a parameter of interest of the fluid using the path-dependent signal. The time-dependent intensity may be indicative of the true absorbance at multiple wavelengths of the fluid or fluids over the maximum path length difference so as to permit quantification of the percentages of each of these fluids. Filtering may include frequency filtering alone or using a phase-sensitive lock-in amplifier.

First claim

What is claimed is:

1. A method of evaluating a fluid, the method comprising:
transmitting a light beam through the fluid to a detector while oscillating a path length traveled through the fluid by the light beam at a first frequency of oscillation;
measuring a time-dependent intensity of incident light at the detector responsive to an interaction of the light beam with the fluid to produce a time-dependent intensity signal;
filtering the time dependent intensity signal to recover a path-dependent signal oscillating at the first frequency and indicative of an absorbance property of the fluid; and
estimating a parameter of interest of the fluid using the path-dependent signal.

2. The method of claim 1 , wherein the time-dependent intensity is indicative of a decrease in intensity between the light beam and the incident light.

3. The method of claim 2 , wherein:
the time-dependent intensity is indicative of a difference in intensity caused by absorbance and a difference in intensity caused by non-absorbance related optical effects; and
the difference in intensity caused by absorbance is represented by the path-dependent signal.

4. The method of claim 1 , comprising filtering the time-dependent intensity signal using at least one of: i) a band-pass filter centered on a second frequency substantially the same as the first frequency; and ii) a phase-sensitive lock-in amplifier.

5. The method of claim 1 , wherein the parameter of interest comprises at least one of: i) an oil fraction of the fluid; ii) a water fraction of the fluid; iii) a gas fraction of the fluid; and iv) a composition of the fluid.

6. The method of claim 1 , wherein the path length is oscillated between a minimum path length and a maximum path length, the minimum path length corresponds to a maximum in the path-dependent signal, and the maximum path length corresponds to a minimum in the path-dependent signal.

7. The method of claim 6 , estimating the parameter of interest by using a ratio of a first intensity of the minimum in the path-dependent signal to a second intensity of the maximum in the path-dependent signal to estimate an absorbance of the fluid.

8. The method of claim 6 , wherein the difference between the minimum path length and the maximum path length is a non-zero value less than one millimeter.

9. The method of claim 1 , wherein at least one of i) transmitting the light beam through the fluid, and ii) measuring the time-dependent intensity of incident light at the detector, is carried out using an optical fiber immersed in the fluid.

10. The method of claim 1 , wherein oscillating the path length comprises moving at least one of a source of the light beam and the detector along a light beam axis with respect to the other of the source and the detector.

11. The method of claim 1 , comprising estimating the parameter of interest using spectral information from the incident light.

12. The method of claim 1 , wherein the downhole fluid is flowing.

13. The method of claim 1 , comprising estimating an absorbance from the path-dependent signal, and using the absorbance to estimate the parameter of interest.

14. The method of claim 1 , wherein the fluid is a highly scattering mixture.

15. An apparatus for evaluating a fluid, the apparatus comprising:
a spectral detector;
a light source configured to transmit a light beam through the fluid to the detector;
an actuator configured to oscillate a path length traveled through the fluid by the light beam at a first frequency of oscillation; and
at least one processor configured to:
measure a time-dependent intensity of incident light at the detector responsive to an interaction of the light beam with the fluid to produce a time-dependent intensity signal;
filter the time dependent intensity signal to recover a path-dependent signal oscillating at the first frequency and indicative of an absorbance property of the fluid; and
estimate a parameter of interest of the fluid using the path-dependent signal.

Assignees

• Baker Hughes Inc
• Baker Hughes A Ge Co Llc

Inventors

• Difoggio Rocco

Classifications

• G01N21/0303

  Optical path conditioning in cuvettes, e.g. windows; adapted optical elements or systems; path modifying or adjustment (G01N21/031 - G01N21/15 take precedence) · CPC title

• G01N2021/1759

  Jittering, dithering, optical path modulation · CPC title

• G01N21/534

  by measuring transmission alone, i.e. determining opacity · CPC title

• G01J3/0208

  using focussing or collimating elements, e.g. lenses or mirrors; performing aberration correction · CPC title

• G01J3/26 Primary

  using multiple reflection, e.g. Fabry-Perot interferometer, variable interference filters · CPC title