Methods for manufacturing biocompatible cathode slurry for use in biocompatible batteries

Patent metadata

Field	Value
Publication number	US-9946092-B2
Application number	US-201514804606-A
Country	US
Kind code	B2
Filing date	Jul 21, 2015
Priority date	Aug 21, 2014
Publication date	Apr 17, 2018
Grant date	Apr 17, 2018

Abstract

Methods and apparatus to form biocompatible energization elements are described. In some examples, the methods and apparatus to form the biocompatible energization elements involve forming cavities comprising active cathode chemistry. The active elements of the cathode and anode are sealed with a biocompatible material. In some examples, a field of use for the methods and apparatus may include any biocompatible device or product that requires energization elements.

First claim

What is claimed is:

1. A method for manufacturing a biocompatible cathode for use in a biocompatible battery comprising the steps of:
obtaining toluene, manganese dioxide, carbon black, and polyisobutylene;
filtering toluene;
sieving manganese dioxide;
sieving carbon black;
sieving polyisobutylene;
mixing the toluene and the polyisobutylene into a liquid phase pre-mixture;
mixing the manganese dioxide and carbon black into a solid phase pre-mixture;
checking a quality of both the solid and liquid phase pre-mixtures
mixing the solid phase pre-mixture and liquid phase pre-mixture into a cathode slurry mixture;
filtering the cathode slurry mixture;
storing the cathode slurry mixture;
recirculating the cathode slurry mixture;
obtaining a laminar structure wherein the laminar structure has a volume removed to form a cavity, wherein the laminar structure comprises a first anode collector layer laminated to a first laminar construct core, wherein the first laminar construct core had the volume removed from its body before it was laminated to the first anode collector layer, and wherein the laminar structure comprises an electroplated anode film thereupon within the cavity;
depositing a hydrogel precursor solution upon the electroplated anode film, wherein the hydrogel precursor solution comprises a hydrogel precursor material and a solvent, wherein the hydrogel precursor material polymerizes and the solvent of the hydrogel precursor solution evaporates to form a separator;
filtering the stored cathode slurry mixture, wherein the filtering removes particles from the cathode slurry which may cause insufficient filling of the cavity;
distributing the filtered cathode slurry mixture into the cavity of the laminar structure, wherein the filtering occurs before the distributing of the cathode slurry; and
drying the cathode slurry mixture to form a biocompatible cathode for use in a biocompatible battery.

2. A method for manufacturing a cathode slurry for use in a biomedical device comprising the steps of:
mixing one or more of a liquid phase pre-mixture with one or more of a solid phase pre-mixture into a cathode slurry mixture;
obtaining a laminar structure wherein the laminar structure has a volume removed to form a cavity, wherein the laminar structure comprises a first anode collector layer laminated to a first laminar construct core, wherein the first laminar construct core had the volume removed from its body before it was laminated to the first anode collector layer, and wherein the laminar structure comprises an electroplated anode film thereupon within the cavity;
depositing a hydrogel precursor solution upon the electroplated anode film, wherein the hydrogel precursor solution comprises a hydrogel precursor material and a solvent, wherein the hydrogel precursor material polymerizes and the solvent of the hydrogel precursor solution evaporates to form a separator;
filtering the cathode slurry mixture, wherein the filtering removes particles from the cathode slurry which may cause insufficient filling of the cavity; and
distributing the cathode slurry mixture into the cavity of the laminar structure forming the cathode slurry for use in a biomedical device, wherein the filtering occurs before the distributing of the cathode slurry;
wherein the biomedical device comprises an insert device comprising:
an electroactive element responsive to a controlling voltage signal;
a biocompatible battery;
wherein the biocompatible battery comprises:
a first and second electrode;
an anode;
a separator;
a laminar structure, wherein at least one layer of the laminar structure has a volume removed to form a cavity; and
the cathode slurry wherein at least an average molecular size of one component of the cathode slurry is reduced in particle size by milling said component; and
wherein the cathode slurry is capable of filling the cavity, based on its rheology, while maintaining electroconductivity through the laminar structure in the cavity; and

a circuit electrically connected to a biocompatible battery, wherein the circuit provides the controlling voltage signal.

3. The method of claim 2 wherein the biomedical device is a contact lens.

4. A method of manufacturing a cathode slurry mixture for use in a biomedical device comprising the steps of:
mixing one or more of a liquid phase pre-mixture with one or more of a solid phase pre-mixture into a cathode slurry mixture;
obtaining a laminar structure wherein the laminar structure has a volume removed to form a cavity, wherein the laminar structure comprises a first anode collector layer laminated to a first laminar construct core, wherein the first laminar construct core had the volume removed from its body before it was laminated to the first anode collector layer, and wherein the laminar structure comprises an electroplated anode film thereupon within the cavity;
depositing a hydrogel precursor solution upon the electroplated anode film, wherein the hydrogel precursor solution comprises a hydrogel precursor material and a solvent, wherein the hydrogel precursor material polymerizes and the solvent of the hydrogel precursor solution evaporates to form a separator;
filtering the cathode slurry mixture, wherein the filtering removes particles from the cathode slurry which may cause insufficient filling of the cavity; and
distributing the cathode slurry mixture into the cavity of the laminar structure forming the cathode slurry mixture for use in a biomedical device, wherein the filtering occurs before the distributing of the cathode slurry;
wherein the biomedical device comprises:
an insert device comprising:
an electroactive element responsive to a controlling voltage signal;
a biocompatible battery;
wherein the biocompatible battery comprises:
a first and second electrode;
an anode;
a separator; and
the cavity for storing a cathode mixture;
wherein the cathode mixture is capable for storage, based on its rheology, while maintaining electroconductivity and biocompatibility;
 wherein the cathode slurry mixture comprises:
 manganese dioxide;
 graphite;
 polyisobutylene (PIB);
 Toluene; and
 wherein at least an average molecular size of one component of the cathode mixture is reduced in particle size by milling said component; and
 a circuit electrically connected to the biocompatible battery wherein the circuit provides the controlling voltage signal.

Assignees

• Johnson & Johnson Vision Care

Inventors

• Flitsch Frederick A
• Gonzalez Jorge
• Otts Daniel B
• Pugh Randall B
• Riall James Daniel
• Toner Adam

Classifications

• H01M10/0436

  Small-sized flat cells or batteries for portable equipment · CPC title

• H01M6/162

  characterised by the electrolyte · CPC title

• H01M10/052

  Li-accumulators · CPC title

• G02C7/04

  Contact lenses for the eyes (disinfection or sterilisation of contact lenses A61L12/00) · CPC title

• H01M4/625

  Carbon or graphite · CPC title