Sample testing apparatus and method

Patent metadata

Field	Value
Publication number	US-9927419-B2
Application number	US-201313919532-A
Country	US
Kind code	B2
Filing date	Jun 17, 2013
Priority date	Jun 26, 2012
Publication date	Mar 27, 2018
Grant date	Mar 27, 2018

Abstract

A test apparatus ( 12 ) and a method of testing a sample ( 30 ) are disclosed. The method comprises receiving a test sample ( 30 ) within a test chamber ( 14 ), the test chamber ( 14 ) containing two or more iron saturation elements ( 2 ) separated by a spacer ( 16 ); and filling the test chamber ( 14 ) with a test solution, the iron saturation elements ( 2 ) being arranged to saturate the test solution with iron. Each iron saturation element ( 2 ) is shaped such that it has a predetermined surface area such that the ratio of the volume of the test solution to the surface area of the iron saturation elements ( 2 ) and the test sample ( 30 ) exposed to the test solution can be calculated.

First claim

The invention claimed is:

1. A test apparatus comprising:
a test chamber arranged to be filled with a test solution and to receive a test sample;
two or more iron saturation elements located within the test chamber to saturate the test solution with iron; and
at least one spacer separating at least one pair of iron saturation elements;
wherein each iron saturation element is shaped such that it has a predetermined surface area such that the ratio of the volume of the test solution to the surface area of the iron saturation elements and the test sample exposed to the test solution can be calculated.

2. A test apparatus according to claim 1 , wherein at least some of the iron saturation elements are formed from sheet material having a thickness that is less than the minimum width of the element in a direction perpendicular to the thickness direction.

3. A test apparatus according to claim 1 , further comprising a loading mechanism for applying tensile stress to the test sample within the test chamber.

4. A test apparatus according to claim 1 , further comprising a first fluid inlet arranged to supply the test solution to the test chamber such that the volume of chamber surrounding the iron saturation elements and at least one spacer is substantially filled by the test solution.

5. A test apparatus according to claim 1 , wherein the iron saturation elements are formed from carbon steel.

6. A test apparatus according to claim 1 , further comprising a second fluid inlet arranged to supply a test fluid to the test chamber.

7. A test apparatus according to claim 6 , wherein the second fluid inlet is arranged to supply H 2 S or CO 2 to the test chamber.

8. A test apparatus according to claim 1 , further comprising a support structure arranged to support at least two iron saturation elements and at least one spacer to form an iron saturation module.

9. A test apparatus according to claim 8 , wherein the support structure is arranged to support a variable number of iron saturation elements and spacers so as to adjust the ratio of the volume of the test solution to the surface area of the iron saturation elements and the test sample exposed to the test solution.

10. A test apparatus according to claim 8 , wherein at least two iron saturation elements are formed from a sheet material and have corresponding holes arranged to receive a guide rod of the support structure, and wherein the at least one spacer also comprises a hole arranged to receive the guide rod such that the spacer and the iron saturation elements are supported by the guide rod with the spacer between the iron saturation elements such that the test solution is in contact with first and second sides of the iron saturation elements surrounding the holes.

11. A method of testing a sample, the method comprising:
receiving a test sample within a test chamber, the test chamber containing two or more iron saturation elements separated by a spacer; and
filling the test chamber with a test solution, the iron saturation elements being arranged to saturate the test solution with iron;
wherein each iron saturation element is shaped such that it has a predetermined surface area such that the ratio of the volume of the test solution to the surface area of the iron saturation elements and the test sample exposed to the test solution can be calculated.

Assignees

• Wellstream Int Ltd
• Ge Oil & Gas Uk Ltd

Inventors

• Pires Fabio De Souza
• Santos Fabio Pinheiro Dos

Classifications

• G01N2203/0464

  with provisions for testing more than one specimen at the time · CPC title

• G01N2203/024

  Corrosive · CPC title

• G01N3/32

  by applying repeated or pulsating forces · CPC title

• G01N2203/0023

  Bending · CPC title

• G01N33/20 Primary

  Metals · CPC title