Sintered body, sputtering target and molding die, and process for producing sintered body employing the same

Patent metadata

Field	Value
Publication number	US-9920420-B2
Application number	US-201514805107-A
Country	US
Kind code	B2
Filing date	Jul 21, 2015
Priority date	Feb 1, 2005
Publication date	Mar 20, 2018
Grant date	Mar 20, 2018

Abstract

Provided is an apparatus that includes a molding die for producing a sintered body. The molding die is configured for cold isostatic pressing and includes a knockdown mold frame comprised of plural frame members and a bottom plate provided in contact with the knockdown mold frame. An upper punch is provided to be movable along the inner surface of the knockdown mold frame. The frame members configured to be movable relative to each other to accommodate an expansion of a green body which takes place at the time of reducing the pressure after the completion of pressing.

First claim

The invention claimed is:

1. A process for producing an ITO sintered body, which comprises:
providing a raw material powder which lacks a molding aid containing an organic substance;
pressing the raw material powder in only a uniaxial direction to form a compressed green body;
releasing the pressure on said compressed green body isotropically; and
firing the green body to form the ITO sintered body.

2. The process for producing the ITO sintered body according to claim 1 , wherein the raw material powder is molded directly by a cold isostatic press to obtain the green body.

3. The process for producing the ITO sintered body according to claim 2 , wherein a molding die, for compression molding is used, wherein said molding die is a molding die for producing said compressed green body by filling and compressing a raw material powder in the molding die and which is characterized by having such a construction that at the time of pressure compression, pressing is applied to the filled raw material powder in only the uniaxial direction, and at the time of reducing the pressure after the completion of pressing, the pressure can be released isotropically with respect to said compressed green body.

4. A process for producing an ITO sintered body, which comprises:
providing a raw material powder which lacks a molding aid containing an organic substance;
pressing the raw material powder in only a uniaxial direction to form a compressed green body; and
releasing the pressure on said compressed green body isotropically;
wherein the process lacks a firing step intended to remove the organic substance from said compressed green body.

5. The process for producing the ITO sintered body according to claim 4 , wherein a raw material powder having an organic substance content of 0.6 wt % or less, is used.

6. The process for producing the ITO sintered body according to claim 4 , wherein a molding die, for compression molding is used, wherein said molding die is a molding die for producing said compressed green body by filling and compressing a raw material powder in the molding die and which is characterized by having such a construction that at the time of pressure compression, pressing is applied to the filled raw material powder in only the uniaxial direction, and at the time of reducing the pressure after the completion of pressing, the pressure can be released isotropically with respect to said compressed green body.

Assignees

• Itoh Kenichi
• Mesuda Masami
• Nagayama Hitoshi
• Shibutami Tetsuo
• Yatsunami Shunsuke
• Tosoh Corp

Inventors

• Itoh Kenichi
• Mesuda Masami
• Nagayama Hitoshi
• Shibutami Tetsuo
• Yatsunami Shunsuke

Classifications

• C23C14/086

  of zinc, germanium, cadmium, indium, tin, thallium or bismuth · CPC title

• C04B2235/6562

  Heating rate · CPC title

• C04B2235/77

  Density · CPC title

• B30B15/024

  using elastic mould parts · CPC title

• C04B2235/3217

  Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina · CPC title