Method for manufacturing a parasiticidal composition

Patent metadata

Field	Value
Publication number	US-9918476-B2
Application number	US-201214366083-A
Country	US
Kind code	B2
Filing date	Dec 19, 2012
Priority date	Dec 19, 2011
Publication date	Mar 20, 2018
Grant date	Mar 20, 2018

Abstract

A method for manufacturing a parasiticidal composition comprising at least 40% of alkali metal bicarbonate and at least 1% of silica, wherein: at least 35% of the alkali metal bicarbonate of the composition is milled in the presence of silica in order to form a mixture of particles, and if necessary, the remainder of the alkali metal bicarbonate is added to the mixture of particles to form the parasiticidal composition, and wherein said parasiticidal composition has a particle size distribution such that at least 50% by weight of the particles have a diameter of less than 100 μm. A parasiticidal composition obtained by the present method and the use of the parasiticidal composition obtained by the present method in the form of a powder, a suspension or a gel.

First claim

The invention claimed is:

1. A method for manufacturing a parasiticidal composition consisting essentially of:
at least 40% by weight of alkali metal bicarbonate, and
at least 1% of silica,
said method comprising:
milling at least 35% of the alkali metal bicarbonate of the composition in the presence of said silica in order to form a mixture of particles, and
if necessary, adding the remainder of the alkali metal bicarbonate to said mixture of particles to form the parasiticidal composition,
wherein said parasiticidal composition has a particle size distribution such that at least 50% by weight of the particles have a diameter of less than 100 μm.

2. The method according to claim 1 , wherein the content of said alkali metal bicarbonate in the parasiticidal composition is at least 70% by weight.

3. The method according to claim 1 , wherein the content of said silica in the parasiticidal composition is at least 5% by weight.

4. The method according to claim 1 , wherein said milling is carried out with an alkali metal bicarbonate:silica weight ratio which is at most equal to: 100:1 and at least equal to 1:1.

5. The method according to claim 1 , wherein at least 50% of said alkali metal bicarbonate of the composition is milled in the presence of said silica.

6. The method according to claim 1 , wherein said milling is carried out with an alkali metal bicarbonate:silica weight ratio which is at most equal to: 100:1.

7. The method according to claim 6 , wherein said alkali metal bicarbonate:silica weight ratio is at least equal to 1.

8. The method according to claim 1 , wherein said silica has a specific surface area of at least 5 m 2 /g.

9. The method according to claim 1 , wherein said silica consists of silica grains having a weight-average diameter at most equal to 20 μm.

10. The method according to claim 1 , wherein said alkali metal bicarbonate of the composition milled in the presence of said silica consists of bicarbonate grains before milling that have a weight-average diameter of at least 100 μm.

11. The method according to claim 1 , wherein said alkali metal bicarbonate is sodium bicarbonate.

12. The method according to claim 1 , wherein said milling of the at least 35% of the alkali metal bicarbonate of the composition milled in the presence of said silica is carried out with an impact mill.

13. The method according to claim 1 , wherein said parasiticidal composition is used for protecting cereal plants or for controlling development of parasites in an environment of animals.

14. The method according to claim 13 , wherein the parasiticidal composition in a powder form is used in an amount of at least 1% by weight relative to the total weight of said material.

15. The method according to claim 1 , further comprising dispersing said parasiticidal composition in a liquid to form a suspension or a gel.

16. The method according to claim 15 , wherein said liquid is a solvent of the alkali metal bicarbonate.

17. The method according to claim 1 , wherein said parasiticidal composition is in form of a powder.

18. The method according to claim 1 , wherein said parasiticidal composition is free of silica agglomerates of greater than 1000 μm.

Assignees

• Solvay

Inventors

• Pascal Jean-Philippe

Classifications

• A01N25/04 Primary

  Dispersions, {emulsions, suspoemulsions, suspension concentrates} or gels (foams A01N25/16) · CPC title

• A01N25/08

  containing solids as carriers or diluents · CPC title

• A01N59/00 Primary

  Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds · CPC title

• A01N25/12

  Powders or granules (A01N25/26 takes precedence) · CPC title

• A01N2300/00

  Combinations or mixtures of active ingredients covered by classes A01N27/00 - A01N65/48 with other active or formulation relevant ingredients, e.g. specific carrier materials or surfactants, covered by classes A01N25/00 - A01N65/48 · CPC title