Apparatus and process for preparation of small water cluster and small molecular cluster water prepared therefrom

Patent metadata

Field	Value
Publication number	US-9907896-B2
Application number	US-201414309486-A
Country	US
Kind code	B2
Filing date	Jun 19, 2014
Priority date	Jun 21, 2013
Publication date	Mar 6, 2018
Grant date	Mar 6, 2018

Abstract

The invention provides an apparatus of treating water to obtain small water cluster, which comprises one or more illumination devices and one or more holders holding metal particles. The invention also provides a method of preparing the small water cluster and the small water cluster prepared from the apparatus or the method.

First claim

What is claimed is:

1. A small water cluster, which has one of the following characteristics:
(a) the central points of the Raman bands in the deconvoluted spectrum on OH vibration of water are at the positions of about 3018 cm −1 , about 3223 cm −1 , about 3393 cm −1 , about 3506 cm −1 , and 3624 cm −1 respectively, and the non-hydrogen bond level obtained by the integral area at the about 3506 cm −1 and about 3624 cm −1 positions divided by the sum of the integral areas of the five bands at about 3018 cm −1 , about 3223 cm −1 , about 3393 cm −1 , about 3506 cm −1 , and 3624 cm −1 positions is higher than about 22%;
(b) the characteristic peak of the triple hydrogen bond in the IR spectrum (about 3090 to about 3310 cm −1 ) and the non-hydrogen bond, single hydrogen bond and doublet hydrogen bond in the IR spectrum (about 3310 cm −1 to about 3640 cm −1 ) of the water molecule shift from about 3170 cm −1 to more higher than about 3175 cm −1 and from about 3449 cm −1 to more higher than about 3454 cm −1 , respectively;
(c) the evaporation rate of the small water cluster of the invention is more than 3%/hour higher than that of deionized water;
(d) the solubility of NaCl in the small water cluster at about 22.8° C. under about 1 atmosphere is more than about 37 g dL −1 ;
(e) the maximum amount of dissolved oxygen of the small water cluster at about 22.8° C. under about 1 atmosphere is more than about 21 mg L −1 ;
(f) the solubility of the small water cluster in PEG 400 is smaller than the preparation value by more than about 2%; and
(g) the saturated vapor pressure of the small water cluster at 25° C. is higher than that of the deionized water by more than about 3.0%.

2. The small water cluster of claim 1 , wherein the small water cluster has metal residue more than about 0.05 ppb measured by inductively coupled plasma-mass spectrometer (ICP-MS).

3. The small water cluster of claim 1 , wherein (a) the Raman spectrum further comprises the Raman shifts at the about 3506 cm −1 and 3624 cm −1 positions higher than 15.0% and 6%, respectively, wherein the percentage is calculated by the integral area of the band at about 3506 cm −1 or at about 3624 cm −1 divided by the sum of the integral areas of the five bands at about 3018 cm −1 , about 3223 cm −1 , about 3393 cm −1 , about 3506 cm −1 , and 3624 cm −1 positions; (b) the characteristic peak of the triple hydrogen bond in the IR spectrum (about 3090 to about 3310 cm −1 ) and the non-hydrogen bond, single hydrogen bond and doublet hydrogen bond in the IR spectrum (about 3310 cm −1 to about 3640 cm −1 ) of the water molecule shift from about 3170 cm −1 to about 3180 cm −1 and from about 3449 cm −1 to about 3461 cm −1 , respectively; (c) the evaporation rate of the small water cluster is more than 7.2%/hour higher than that of the deionized water; (d) the solubility of NaCl in the small water cluster of the invention at about 22.8° C. under about 1 atmosphere is more than about 41.3 g dL −1 ; or (e) the maximum amount of dissolved oxygen of the small water cluster at about 22.8° C. under about 1 atmosphere is more than about 23.8 mg L −1 .

4. The small water cluster of claim 1 , which can stably exist for at least three days.

Assignees

• Univ Taipei Medical

Inventors

• Liu Yu Chuan

Classifications

• A61P43/00

  Drugs for specific purposes, not provided for in groups A61P1/00-A61P41/00 · CPC title

• A61P39/02

  Antidotes · CPC title

• A61P3/00

  Drugs for disorders of the metabolism (of the blood or the extracellular fluid A61P7/00) · CPC title

• A61P29/00

  Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID] · CPC title

• A61M1/1656 Primary

  Apparatus for preparing dialysates · CPC title