Manufacturing method of common grain-oriented silicon steel with high magnetic induction

Patent metadata

Field	Value
Publication number	US-9905361-B2
Application number	US-201214430463-A
Country	US
Kind code	B2
Filing date	Dec 11, 2012
Priority date	Sep 27, 2012
Publication date	Feb 27, 2018
Grant date	Feb 27, 2018

Abstract

A manufacturing method of oriented silicon steel with magnetic induction B8 of not less than 1.88 T, comprising the following steps: 1) smelting and continuous casting to obtain a slab, wherein the content of N is controlled at 0.002-0.014 wt % in the smelting stage; 2) hot-rolling; 3) cold-rolling; 4) decarbonizing and annealing; 5) nitriding treatment, wherein infiltrated nitrogen content [N] D is controlled to satisfy the formula: 328−0.14a−0.85b−2.33c≦[N] D ≦362−0.16a−0.94b−2.57c, wherein a is the content of Als in the smelting step, with the unit of ppm; b is the content of N element, with the unit of ppm; and c is primary grains size, with the unit of μm; 6) coating a steel's surfaces with a magnesium oxide layer and annealing; and 7) applying an insulating coating.

First claim

The invention claimed is:

1. A manufacturing method of common oriented silicon steel having high magnetic induction, comprising the following steps:
(1) smelting and continuous casting to obtain a slab, wherein the content of N is controlled in a range of 0.002-0.014 wt % in the smelting stage;
(2) hot-rolling, wherein a heating temperature is 1090-1200° C.;
(3) cold-rolling, wherein a primary aging-free rolling is performed;
(4) decarbonizing and annealing;
(5) nitriding treatment, wherein infiltrated nitrogen content [N] D satisfies the following formula: 328−0.14a−0.85b−2.33c≦[N] D ≦362−0.16a−0.94b−2.57c, wherein a is the content of Als in the smelting step, with a unit of ppm; b is the content of N element in the smelting step, with a unit of ppm; and c is the size of primary grains, with a unit of μm;
(6) coating a magnesium oxide layer on a steel plate's surfaces, and annealing; and
(7) coating an insulation layer.

2. The manufacturing method of common oriented silicon steel having high magnetic induction according to claim 1 , wherein in the step (2), the hot-rolling begins at a temperature of 1180° C. or below, and ends at a temperature of 860° C. or above, and then a coiling after the hot-rolling is performed at a temperature of below 650° C.

3. The manufacturing method of common oriented silicon steel having high magnetic induction according to claim 2 , wherein in said step (3), a cold-rolling reduction ratio is not less than 80%.

4. The manufacturing method of common oriented silicon steel having high magnetic induction according to claim 3 , wherein in the step (4), a heating rate is 15-35° C./s, a decarbonizing temperature is 800-860° C., and a decarbonizing dew point is 60-70° C.

5. The manufacturing method of common oriented silicon steel having high magnetic induction according to claim 4 , wherein in the step (4), a protective atmosphere is 75% H 2 +25% N 2 .

6. The manufacturing method of common oriented silicon steel having high magnetic induction according to claim 1 , wherein in the step (5), the nitriding is performed by NH 3 with a volume fraction of 0.5-4.0%, at a temperature of 760-860° C., within a time of 20-50 s, and in an oxidation degree P H2O /P H2 of 0.045-0.200.

Assignees

• Baoshan Iron & Steel

Inventors

• Shen Kanyi
• Li Guobao
• Chu Shuangjie
• Sun Yezhong
• Zhang Huabing
• Yang Yongjie
• Hu Zhuochao
• Zhao Bin
• Xu Qi
• Huang Jie
• Zhang Peili

Classifications

• C21D6/008

  containing Si · CPC title

• C21D8/1277

  involving a particular surface treatment (C21D8/1294 takes precedence) · CPC title

• C22C38/008

  containing tin · CPC title

• H01F1/18

  with insulating coating · CPC title

• C22C38/02

  containing silicon · CPC title