Contact and separation column and tray

Patent metadata

Field	Value
Publication number	US-9895629-B2
Application number	US-201214365288-A
Country	US
Kind code	B2
Filing date	Dec 14, 2012
Priority date	Dec 16, 2011
Publication date	Feb 20, 2018
Grant date	Feb 20, 2018

Abstract

A contact and separation column ( 1 ) encasing a stack of one or more contact and separation cells ( 3 ). Each cell comprises: —a tray ( 4 ) with gas flow openings ( 6 ) opening into contact and separation units ( 7 ); —a downcomer ( 16 ) defining a liquid discharge; and —a liquid supply ( 17 ). Each contact and separation unit ( 7 ) comprises an upstream contact zone ( 8, 9 ) with liquid inlets ( 12 ), and one or more downstream separation zones ( 10 ) provided with a swirler ( 13 ) and a top end with a gas outlet ( 14 ). The swirler ( 13 ) is located at a distance from the gas inlet of from 50 to 90 % of the total length of the contact and separation zone. Process for treating a gas with such a column.

First claim

That which is claimed is:

1. A contact and separation column comprising a column wall encasing a stack of one or more contact and separation cells, wherein each contact and separation cell comprises:
a liquid supply for supplying liquid to the contact and separation cell;
a downcomer defining a liquid discharge;
a tray with a number of gas flow openings opening into one or more contact and separation units positioned on an upper side of the tray, the tray being adapted to hold a layer of the liquid,
wherein each contact and separation unit comprises an upstream contact zone defined by vertical plates connected to the tray and positioned to receive gas flowing through the gas flow openings, wherein the vertical plates have liquid inlets located near the tray and wherein the liquid inlets provide for liquid flow from the layer of the liquid into the upstream contact zone, and
one or more downstream separation zones each defined by a body and which are connected to upper ends of the vertical plates of the upstream contact zone to be in fluid communication with the upstream contact zone, wherein each body has a lower end provided with a swirler and a top end defining a gas outlet,
the swirler being located at a distance from the tray of from 50 to 90% of the total length of the contact and separation cell,
the contact zone of each contact and separation unit having a larger cross-sectional area than the corresponding one or more separation zones.

2. The contact and separation column according to claim 1 , wherein the upstream contact zone defined by the vertical plates has a contact zone volume, wherein each downstream separation zone defined by its body has a separation zone volume, wherein the contact zone volume is at least 50% larger than the sum of the separation zone& volumes of the downstream separation zones associated with the upstream contact zone.

3. The contact and separation column according to claim 1 , wherein the cross-section of the contact zone is a square or rectangle.

4. The contact and separation column according to claim 1 , wherein a contact and separation unit comprises a single contact zone and a plurality of separation zones.

5. The contact and separation column according to claim 1 , wherein at least part of the contact zones is filled with a packing material.

6. The contact and separation column according to claim 1 , wherein the downcomers in adjacent cells are offset relative to each other and wherein the liquid discharge of an upper contact and separation cell forms the liquid supply of a lower contact and separation cell.

7. The contact and separation column according to claim 1 , wherein at an edge of the tray downcomers comprise a weir, wherein the weir and column wall define a liquid discharge.

8. The contact and separation column according to claim 1 , wherein the contact and separation units comprise a box shaped contact zone opening into one or more tubular separation zones.

9. The contact and separation column according to claim 1 , wherein the gas outlet is bordered by a liquid flow deflector.

10. The contact and separation column according to claim 9 , wherein the liquid flow deflector comprises a return skirt having a U-shaped radial cross section with an open side arranged over a top edge of the separation zone.

11. A process of treating gas with a liquid which process comprises introducing the gas at the gas inlet and liquid at the liquid inlet in a lower contact and separation cell of a contact and separation column according to claim 1 .

12. The process of claim 11 wherein the flow velocity of the gas in the contact zone is lower than the flow velocity in the separation zone.

13. The process of claim 12 wherein the gas is natural gas.

Assignees

• Shell Int Research
• Shell Oil Co

Inventors

• Koeppen Jannes
• Vos Eric Johannes
• Wilkinson Peter Mervyn

Classifications

• B01D3/20 Primary

  Bubble caps; Risers for vapour; Discharge pipes for liquid · CPC title

• B01D2257/504

  Carbon dioxide · CPC title

• B01D53/185

  Liquid distributors · CPC title

• B01D2252/20484

  with one hydroxyl group · CPC title

• B01D53/1462

  Removing mixtures of hydrogen sulfide and carbon dioxide · CPC title