Process for making a conditioning gel phase

Patent metadata

Field	Value
Publication number	US-9889079-B2
Application number	US-201314416173-A
Country	US
Kind code	B2
Filing date	Jul 24, 2013
Priority date	Jul 27, 2012
Publication date	Feb 13, 2018
Grant date	Feb 13, 2018

Abstract

Process for making a conditioning gel phase comprising: i) forming an aqueous dispersion of fatty alcohol and amidoamine; ii) adding a cationic surfactant to the aqueous dispersion and mixing; and iii) neutralizing the amidoamine, wherein the temperature of the mixture of cationic surfactant in the aqueous dispersion is maintained at from 56° C. to 67° C.

First claim

The invention claimed is:

1. Process for making a conditioning gel phase comprising:
i) forming an aqueous dispersion of fatty alcohol and amidoamine, wherein the temperature of the aqueous dispersion is maintained at least 5° C. above the melting point of the fatty alcohol;
ii) adding a cationic surfactant to the aqueous dispersion and mixing, and
iii) neutralising the amidoamine by the addition of acid,
wherein:
the amidoamine is of the general formula:
R 1 CONH(CH 2 ) m N(R 2 )R 3 ,

wherein R 1 is a hydrocarbyl residue having from about 11 to about 24 carbon atoms, R 2 and R 3 are independently methyl or ethyl groups and m is 2 or 3,
the fatty alcohol is C16 to C22 fatty alcohol, and
the cationic surfactant is selected from the group of: cetyltrimethylammonium chloride, behenyltrimethylammonium chloride, cetylpyridinium chloride, tetramethylammonium chloride, tetraethylammonium chloride, octyltrimethylammonium chloride, dodecyltriethylammonium chloride, hexadecyltrimethylammonium chloride, octyldimethylbenzylammonium chloride, decyldimethylbenzylammonium chloride, stearyldimethylbenzylammonium chloride, didodecyldimethylammonium chloride, dioctadecyldimethylammonium chloride, PEG-2-oleammonium chloride, and mixtures of any of the foregoing,

wherein the temperature of the mixture of cationic surfactant in the aqueous dispersion of the fatty alcohol and amidoamine is maintained at from 56° C. to 67° C., and above the melting point of the fatty alcohol, for from 20 to 60 minutes, after which time the acid is added.

2. The process according to claim 1 in which the aqueous dispersion comprises from 4 to 20 wt % of the dispersion fatty alcohol.

3. The process according to claim 1 in which the aqueous dispersion comprises from 1 to 5 wt % of the dispersion amidoamine surfactant.

4. The process according to claim 1 in which the mixture of cationic surfactant and fatty alcohol and amidoamine comprises from 0.5 to 5 wt % cationic surfactant.

5. The process according, to claim 1 in which the cationic surfactant is behenyltrimethylammonium chloride.

6. The process according to claim 1 in which the amidoamine surfactant is stearylamidopropyl dimethylamine.

7. The process according to claim 1 in which the fatty alcohol is a C16 to C18 fatty alcohol.

8. The process according to claim 1 comprising passing the resulting conditioning gel phase through a mixer with rotor tip speed of 10-34 ms−1.

9. The process according to claim 1 wherein one or more additional ingredients selected from the group consisting of fragrances, silicones, fibre actives and other benefit agents are added after the conditioning gel phase is formed to produce a conditioning composition for hair treatment.

10. The process according to claim 1 wherein the temperature of the mixture of cationic surfactant in the aqueous dispersion of the fatty alcohol and amidoamine is maintained at from 58° C. to 85° C., and above the melting point of the fatty alcohol, for from 20 to 60 minutes, after which time the acid is added.

11. The process according to claim 9 comprising passing the conditioning composition through a mixer with rotor tip speed of 10-30 ms−1.

12. The process according to claim 1 wherein the cationic surfactant is cetyltrimethylammonium chloride and/or behenyltrimethylammonium chloride and the amidoamine is selected from the group consisting of stearamidopropyldimethylamine stearamidopropyldiethylamine, stearamidoethyldiethylamine, stearamidoethyldimethylamine, palmitamidopropyldimethylamine, palmitamidoethyldimethylamine, behenamidopropyldimethylamine, behenamidopropyldiethylamine, behenamidoethyldiethylamine, behenamidoethyldimethylamine, arachidamidopropyldimethylamine, arachidamidopropyldiethylamine, arachidamidoethyldiethylamine, arachidamidoethyldimethylamine, and mixtures thereof.

13. The process according to claim 1 wherein the cationic surfactant is cetyltrimethylammonium chloride and/or behenyltrimethylammonium chloride.

14. The process according to claim 13 wherein the fatty alcohol is C16 to C18 fatty alcohol and the amidoamine is stearamidopropyldimethylamine.

Assignees

• Conopco Inc

Inventors

• Casugbo Christia
• Flanagan Mark
• Hough John Alan
• Naughton John Michael
• Serridge David

Classifications

• A61K8/416

  Quaternary ammonium compounds (A61K8/35 takes precedence) · CPC title

• A61K8/042

  Gels · CPC title

• A61K8/04

  Dispersions; Emulsions · CPC title

• A61K8/42 Primary

  Amides · CPC title

• A61Q5/12

  Preparations containing hair conditioners · CPC title