Porous silica particle, method for producing the same, and cleansing cosmetic containing the same

Patent metadata

Field	Value
Publication number	US-9889072-B2
Application number	US-201515512985-A
Country	US
Kind code	B2
Filing date	Oct 2, 2015
Priority date	Oct 2, 2014
Publication date	Feb 13, 2018
Grant date	Feb 13, 2018

Abstract

A porous silica particle with the small specific surface area and large pore volume, which is contained as the scrubbing agent in the cleansing cosmetics is provided. The porous silica particle has high collapsibility, and therefore the damage of the skin can be prevented. A porous silica particle according to the present invention has: an average circularity of 0.1 to 0.5; a pore volume of 0.1≦Pv<1.0 ml/g; a specific surface area of 5 to 60 m 2 /cm 3 ; a median size of 100 to 1000 μm; a ratio of a maximum particle diameter to the median size, of 3.0 or less; and a median size of 5 to 40 μm and a maximum particle diameter of 15 to 200 μm, after rubbing for 30 seconds with a load of 1.0 to 1.4 KPa.

First claim

The invention claimed is:

1. A porous silica particle comprising:
an average circularity of 0.1 to 0.5;
a pore volume of 0.1≦Pv<1.0 ml/g;
a specific surface area of 5 to 60 m 2 /cm 3 ;
a median size of 100 to 1000 μm;
a ratio of a maximum particle diameter to the median size, of 3.0 or less; and
a median size of 5 to 40 μm and a maximum particle diameter of 15 to 200 μm, after rubbing for 30 seconds with a load of 1.0 to 1.4 KPa.

2. The porous silica particle according to claim 1 , wherein when a compressive force of 0.5 gf is applied to the porous silica particle, a displacement of 0.5 to 3 μm occurs.

3. The porous silica particle according to claim 1 , wherein when the compressive force that is increased up to 2.5 gf at a proportion of 0.21 gf/sec is applied to the porous silica particle, five or more displacements in a stepwise shape occur, each displacement ranging from 0.01 to 1.0 μm.

4. The porous silica particle according to claim 3 , wherein when an amount of displacement at a compressive force f 2 of 2.5 gf is expressed by a displacement d 2 (μm), a tilt of compression displacement (f 2 /d 2 ) is in the range of 0.5 to 2.5.

5. The porous silica particle according to claim 1 , wherein when the compressive force that is increased at a proportion of 0.21 gf/sec is applied to the porous silica particle, a plurality of displacements in a stepwise shape occurs and a compressive force f 3 at which the displacement of 10 μm or more occurs first is in the range of 5 to 40 gf.

6. The porous silica particle according to claim 5 , wherein when an amount of compression displacement before the compression displacement of 10 μm or more at the compressive force f 3 (gf) occurs is expressed by a displacement d 3 (μm), a tilt of compression displacement (f 3 /d 3 ) is in the range of 0.3 to 1.25.

7. A cleansing cosmetic comprising the porous silica particle according to claim 1 , and a cleansing cosmetic component.

8. The porous silica particle according to claim 2 , wherein when the compressive force that is increased up to 2.5 gf at a proportion of 0.21 gf/sec is applied to the porous silica particle, five or more displacements in a stepwise shape occur, each displacement ranging from 0.01 to 1.0 μm.

9. The porous silica particle according to claim 2 , wherein when the compressive force that is increased at a proportion of 0.21 gf/sec is applied to the porous silica particle, a plurality of displacements in a stepwise shape occurs and a compressive force at which the displacement of 10 μm or more occurs first is in the range of 5 to 40 gf.

10. The porous silica particle according to claim 3 , wherein when the compressive force that is increased at a proportion of 0.21 gf/sec is applied to the porous silica particle, a plurality of displacements in a stepwise shape occurs and a compressive force at which the displacement of 10 μm or more occurs first is in the range of 5 to 40 gf.

11. The porous silica particle according to claim 4 , wherein when the compressive force that is increased at a proportion of 0.21 gf/sec is applied to the porous silica particle, a plurality of displacements in a stepwise shape occurs and a compressive force at which the displacement of 10 μm or more occurs first is in the range of 5 to 40 gf.

Assignees

• Jgc Catalysts & Chemicals Ltd

Inventors

• Watanabe Satoshi
• Enomoto Naoyuki
• Miyoshi Yasutaka

Classifications

• C01P2006/12

  Surface area · CPC title

• A61K2800/60

  Particulates further characterized by their structure or composition · CPC title

• A61Q19/10

  Washing or bathing preparations · CPC title

• A61K8/345

  containing more than one hydroxy group · CPC title

• A61K8/19

  containing inorganic ingredients · CPC title