High-throughput sorting of small objects via oil and/or moisture content using low-field nuclear magnetic resonance

Patent metadata

Field	Value
Publication number	US-9880116-B2
Application number	US-201615371871-A
Country	US
Kind code	B2
Filing date	Dec 7, 2016
Priority date	Mar 15, 2013
Publication date	Jan 30, 2018
Grant date	Jan 30, 2018

Abstract

The current disclosure describes an automated high-throughput seed sorting system for separating seed via oil and/or moisture content using novel nuclear magnetic resonance (NMR) systems and methods. The disclosed systems and methods for measuring the oil and/or moisture content of a single seed in a low-field time domain NMR instrument are superior in sample throughput and signal-to-noise ratio to conventional NMR systems and methods (free induction decay or spin echo) for single seed oil/moisture measurement.

First claim

What is claimed is:

1. A high throughput dynamic seed sorting system, said system comprising:
a conveyor assembly including a seed conveyor belt having a plurality of seed cups attached thereto, the conveyor assembly structured and operable to continuously move the conveyor belt at a selected constant rate of speed during operation of the system;
a seed feeder assembly structured and operable to singulate seeds from a plurality of seeds and deposit each singulated seed into a respective one of the seed cups as the conveyor belt continuously moves at the selected constant rate of speed;
a nuclear magnetic resonance (NMR) assembly having the conveyor belt operably extending therethrough, the NMR assembly structured and operable to generate oil mass data for each seed as each seed moves through the NMR assembly at the selected constant rate of speed; and
a computer based central control system structured and operable to:
receive the oil mass data from the NMR assembly for each seed, and execute oil content software to:
store the oil mass data for each seed and associate the oil mass data received for each seed with the respective seed, and
based on the oil mass, compute an oil content value for each respective seed within a time period dictated by the selected constant rate of speed of the conveyor belt.

2. The system of claim 1 further comprising a microwave resonance cavity structured and operable to receive and have pass therethrough, without pause, each seed after each respective seed has been conveyed through the NMR assembly and to obtain total seed mass data for each respective seed.

3. The system of claim 2 , further comprising a diverter assembly structured and operable to receive the seeds from the microwave resonance cavity and, via commands from the central control system, separate the seeds based on the computed oil/moisture content of each respective seed.

4. The system of claim 2 , wherein the NMR assembly comprises:
an NMR rexlameter structured and operable to exert a magnetic force on each seed passing through the NMR assembly; and
a radio frequency (RF) probe structured and operable to generate a plurality of pulses and receive an echo from each pulse from which the at least one of oil and moisture mass data is generated.

5. The system of claim 4 , wherein the number of pulses generated each millisecond is such that noise generated by each pulse cancels the noise of subsequent pulses, thereby increasing the signal-to-noise ratio of NMR measurement during determination of the at least one of oil and moisture mass data.

6. The system of claim 5 , wherein the number of pulses generated each millisecond is approximately five pulses per millisecond.

7. The system of claim 1 , wherein each seed cup comprises a reservoir into which each respective seed is deposited by the seed feeder assembly and a plurality of serrations through a body of seed cup, the reservoir and serrations structured and operable to center and reduce vibration of each seed within the respective seed cup and retain each seed in a stable orientation within the respective seed cup as each seed is conveyed through the NMR assembly.

8. The system of claim 1 , wherein the selected rate of speed is approximately one meter per second.

9. The system of claim 1 further comprising a stray seed removal assembly structured and operable to remove stray seeds that are not retained within a seed cup from the conveyor belt.

10. A high throughput seed sorting system, said system comprising:
a conveyor assembly including a conveyor belt having a plurality of seed cups attached thereto, the conveyor assembly structured and operable to continuously move the conveyor belt at a selected constant rate of speed during operation of the system;
a seed feeder assembly structured and operable to singulate seeds from a plurality of seeds and deposit each singulated seed into a respective one of the seed cups as the conveyor belt continuously moves at the selected constant rate of speed;
a nuclear magnetic resonance (NMR) assembly having the conveyor belt operably extending therethrough, the NMR assembly structured and operable to generate at least one of oil and moisture mass data for each seed as each seed moves through the NMR assembly at the selected constant rate of speed;
a computer based central control system structured and operable to:
receive the at least one of oil and moisture mass data from the NMR assembly for each seed, and
execute oil/moisture content software to store the at least one of oil and moisture mass data for each seed and associate the at least one of oil and moisture mass data received for each seed with the respective seed; and

a diverter assembly structured and operable to receive the seeds and, via commands from the central control system, separate the seeds based on the at least one of oil and moisture mass data of each respective seed.

11. A method for high throughput seed sorting, said method comprising:
continuously moving a conveyor belt at a selected constant rate of speed, the conveyor belt included in a conveyor assembly of a high throughput seed sorting system and having a plurality of seed cups attached thereto;
singulating seeds from a plurality of seeds and depositing each singulated seed into a respective one of the seed cups as the conveyor belt continuously moves at the selected constant rate of speed;
generating at least one of oil and moisture mass data for each seed as each seed moves through a nuclear magnetic resonance (NMR) assembly at the selected constant rate of speed; and
separating the seeds into at least two subsets based on the at least one of oil and moisture mass data of each respective seed.

Assignees

• Monsanto Technology Llc

Inventors

• Dai Bin
• Macisaac Susan
• Deppermann Kevin L
• Ehrhardt Mark
• White Brad
• Brown Wayne
• Krasucki Paul
• Mcdonald Jemmi C

Classifications

• G01R33/307

  specially adapted for moving the sample relative to the MR system, e.g. spinning mechanisms, flow cells or means for positioning the sample inside a spectrometer · CPC title

• G01R33/561

  by reduction of the scanning time, i.e. fast acquiring systems, e.g. using echo-planar pulse sequences · CPC title

• A01C1/00

  Apparatus, or methods of use thereof, for testing or treating seed, roots, or the like, prior to sowing or planting · CPC title

• G01R33/445

  MR involving a non-standard magnetic field B0, e.g. of low magnitude as in the earth's magnetic field or in nanoTesla spectroscopy, comprising a polarizing magnetic field for pre-polarisation, B0 with a temporal variation of its magnitude or direction such as field cycling of B0 or rotation of the direction of B0, or spatially inhomogeneous B0 like in fringe-field MR or in stray-field imaging · CPC title

• G01N24/08 Primary

  by using nuclear magnetic resonance (G01N24/12 takes precedence) · CPC title