Process for preparing catalysts
US-9221034-B2 · Dec 29, 2015 · US
US9873108B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9873108-B2 |
| Application number | US-201314765283-A |
| Country | US |
| Kind code | B2 |
| Filing date | Dec 2, 2013 |
| Priority date | Jan 31, 2013 |
| Publication date | Jan 23, 2018 |
| Grant date | Jan 23, 2018 |
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Various metal oxide mesocrystals can be synthesized in a simple manner by a method for producing a metal oxide mesocrystal, the method comprising the step of annealing an aqueous precursor solution comprising one or more metal oxide precursors, an ammonium salt, a surfactant, and water at 300 to 600° C. Composite mesocrystals consisting of a plurality of metal oxides or an alloy oxide can also be provided.
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We claim: 1. A method for producing a metal oxide mesocrystal, the method comprising the step of maintaining an aqueous precursor solution comprising one or more metal oxide precursors, an ammonium salt, a surfactant, and water at 300 to 600° C. 2. The method according to claim 1 , wherein the one or more metal oxide precursors are a metal nitrate and/or a metal fluoride salt. 3. The method according to claim 1 , wherein the ammonium salt is NH 4 NO 3 . 4. The method according to claim 1 , wherein the surfactant is at least one member selected from the group consisting of anionic surfactants, cationic surfactants, amphoteric surfactants, and nonionic surfactants. 5. The method according to claim 1 , wherein, in the aqueous precursor solution, the molar ratio of metal oxide precursor to surfactant is 1 to 1000:1, and the molar ratio of ammonium salt to surfactant is 1 to 1000:1.
Nanoparticles · CPC title
Scanning electron microscopy; Transmission electron microscopy · CPC title
Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties · CPC title
X-ray diffraction · CPC title
characterised by their crystalline properties, e.g. semi-crystalline (catalysts comprising carbon B01J21/18; molecular sieves B01J29/00) · CPC title
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