Making a liquid electrophotographic (LEP) paste

Patent metadata

Field	Value
Publication number	US-9857714-B2
Application number	US-201615087929-A
Country	US
Kind code	B2
Filing date	Mar 31, 2016
Priority date	May 31, 2012
Publication date	Jan 2, 2018
Grant date	Jan 2, 2018

Abstract

A method of making a liquid electrophotographic (LEP) paste is disclosed herein. A base paste is made by forming a dispersion of a pigment and a non-polar carrier, adding a transparent resin dispersion to the pigment dispersion to form a dispersion mixture, and homogenizing the dispersion mixture. The transparent resin dispersion includes a polymer dispersed in a non-aqueous carrier. The homogenizing may be accomplished by agitating the dispersion mixture at a frequency of less than 1 kHz, thereby forming the paste.

First claim

What is claimed is:

1. A method of making a liquid electrophotographic (LEP) paste, comprising:
forming a pigment dispersion of a non-polar carrier and a pigment chosen from i) a pigment having a silver appearance or ii) a combination of the pigment having the silver appearance and an other pigment having a pearlescent optical property;
adding a transparent resin dispersion to the pigment dispersion to form a dispersion mixture, the transparent resin dispersion including a polymer dispersed in a non-aqueous carrier; and
then homogenizing the dispersion mixture, the homogenizing being accomplished by agitating the dispersion mixture at a frequency ranging from 1 Hz to 1 kHz, thereby forming the paste, wherein the pigment having the silver appearance maintains its original morphology in the paste after processing.

2. The method as defined in claim 1 wherein the agitating is accomplished by pivotal shaking, orbital shaking, rotational shaking, pneumatic shaking, or combinations thereof, and wherein the agitating alone accomplishes formation of the paste.

3. The method as defined in claim 1 wherein the pigment is self-dispersible in the non-polar carrier.

4. The method as defined in claim 1 wherein the pigment is non-self-dispersible in the non-polar carrier, and wherein the forming of the pigment dispersion is accomplished by:
adding the pigment and a dispersant to a liquid medium to form a pigment dispersion; and then
combining the pigment dispersion and the non-polar carrier.

5. The method as defined in claim 1 wherein the agitating of the dispersion mixture is performed at a temperature ranging from about 22° C. to about 25° C.

6. The method as defined in claim 1 wherein the agitating of the dispersion mixture involves a non-impact process.

7. The method as defined in claim 1 wherein the pigment having the silver appearance is chosen from aluminum pigment particles, encapsulated aluminum pigment particles, aluminum pigment flakes, aluminum pigment powders, silver pigments, chromium pigments, platinum pigments, and titanium alloys.

8. The method as defined in claim 1 wherein the polymer of the transparent resin dispersion is chosen from ethyl vinyl acetate copolymers, ethylene copolymers having a carboxylic acid functionality, polybutyl terephthalate, and ethylene ethyl acrylate.

9. The method as defined in claim 1 wherein the pigment having the silver appearance maintains a particle size distribution, a particle thickness distribution, or combinations thereof after homogenizing.

10. The method as defined in claim 1 wherein:
an amount of the pigment having the silver appearance in the pigment dispersion ranges from about 20 wt % to about 60 wt %; and
an amount of the polymer in the transparent resin dispersion ranges from about 15 wt % to about 40 wt % of the transparent resin dispersion.

11. The method as defined in claim 1 wherein:
an amount of the pigment having the silver appearance ranges from about 20 wt % to about 60 wt % of the pigment dispersion, and the amount of the other pigment having the pearlescent optical property ranges from about 5 wt % to about 30 wt % of the pigment dispersion; and
an amount of the polymer in the transparent resin dispersion ranges from about 15 wt % to about 40 wt % of the transparent resin dispersion.

12. The method as defined in claim 1 wherein the frequency is about 10 Hz.

Assignees

• Hewlett Packard Development Co Lp

Inventors

• Chun Doris Pik-Yiu

Classifications

• C09B67/009

  polymeric dispersing agent · CPC title

• C09B67/0088

  cationic dispersing agents · CPC title

• C09B67/0098

  Organic pigments exhibiting interference colours, e.g. nacrous pigments · CPC title

• G03G9/125

  characterised by the liquid · CPC title

• C09D11/033

  characterised by the solvent · CPC title