Method and apparatus for adding steam for a steam explosion pretreatment process

Patent metadata

Field	Value
Publication number	US-9856601-B2
Application number	US-201314428182-A
Country	US
Kind code	B2
Filing date	Sep 18, 2013
Priority date	Sep 19, 2012
Publication date	Jan 2, 2018
Grant date	Jan 2, 2018

Abstract

A method for treating cellulosic biomass feed stock including: feeding the feed stock to an upper inlet of a vertical reactor vessel, wherein the feed stock is deposited on a pile of feed stock within the vertical reactor vessel; adding heat energy to heat the feed stock by injecting steam to an upper region of the vertical reactor vessel; propelling the feed stock through an outlet in a lower region of the vertical reactor vessel by injecting steam into the biomass at, near or after the bottom outlet of the vertical reactor vessel, and moving the propelled feed stock through an expansion device, such as a steam explosion device, to subject the feed stock to a steam explosion process.

First claim

What is claimed is:

1. A method for treating biomass comprising:
feeding a biomass feed stock through a pressure isolation device and to an upper inlet of a vertical reactor vessel-system, wherein the biomass feed stock is deposited on a pile of biomass within a vertical reactor vessel, and wherein the feeding of the biomass feed stock to the upper inlet is continuous;
adding heat energy to heat and pressurize the biomass feed stock by injecting a first steam volume into an upper region of the vertical reactor vessel;
propelling a heated biomass from the pile of biomass through an outlet disposed at a lower region of the vertical reactor vessel by injecting at least a second steam volume into the lower region of the vertical reactor vessel at, near, or after the outlet of the vertical reactor vessel to define a propelled heated biomass, wherein the injection of the first steam volume and the injection of the at least the second steam volume are vertically separated by at least a portion of the pile of biomass;
moving the propelled heated biomass to and through an expansion device to subject the propelled heated biomass to a steam explosion process;
measuring a differential pressure between a vapor space above the pile of biomass in the vertical reactor vessel and a vapor space within or above the expansion device; and
controlling a flow of the at least the second steam volume into the lower region of the vertical reactor vessel at, near, or after the outlet of the vertical reactor vessel to regulate the moving of the propelled heated biomass to and through the expansion device based on the differential pressure.

2. The method of claim 1 further comprising adding propelling steam after the outlet of the vertical reactor vessel directly into a conduit for the propelled heated biomass, the conduit extending from the outlet of the vertical reactor vessel to the expansion device.

3. The method of claim 1 further comprising injecting additional steam into the vertical reactor vessel at a middle region between the upper and lower regions.

4. A method for treating biomass comprising:
adding a biomass through a pressure isolation device and into an upper inlet of a vertically oriented reactor vessel, wherein the biomass falls through a vapor phase within the vertically oriented reactor vessel and lands on a pile of biomass in the vertically oriented reactor vessel, and wherein the adding of the biomass into the upper inlet is continuous;
injecting a first heated and pressurized gas or vapor to an upper region of the vertically oriented reactor vessel;
injecting at least a second pressurized gas or vapor through nozzles after a lower region of the vertically oriented reactor vessel, wherein a vertical distance and at least a portion of the pile of biomass separates the injection of the first heated and pressurized gas or vapor and the injection of the at least the second pressurized gas or vapor, wherein the at least the second pressurized gas or vapor is injected into a conduit to propel the biomass to a steam expansion device, and wherein the conduit extends from the outlet of the vertically oriented reactor vessel to the expansion device,
rapidly reducing the pressure on the biomass in the expansion device to burst cellular structures in the biomass;
measuring a differential pressure between a vapor space above the pile of biomass in the vertically oriented reactor vessel and a vapor space within or above the expansion device; and
using a control system to control a flow of the at least the second pressurized gas or vapor through nozzles after a lower region of the vertically oriented reactor vessel based on the differential pressure to thereby regulate a flow of the biomass to and through the expansion device.

5. The method of claim 4 , wherein the heated and pressurized gas or vapor is selected from the group consisting of: steam, air, nitrogen, oxygen, argon and other inert gas.

6. The method of claim 4 , wherein the at least the second pressurized gas or vapor is selected from the group consisting of: steam, air, nitrogen, oxygen, argon and other inert gas.

7. The method of claim 4 further comprising injecting additional steam into the vertically oriented reactor vessel at a middle region between the upper and lower regions.

8. An assembly for treating biomass comprising:
a vertical reactor vessel including an upper biomass inlet and an upper steam inlet at an upper region of the vertical reactor vessel, wherein the vertical reactor vessel is configured to receive a biomass continuously;
an outlet in the lower region of the vertical reactor vessel;
a propelling steam inlet at the lower region of the vertical reactor vessel, wherein the upper steam inlet and the propelling steam inlet are vertically separated-by a height of biomass;
an expansion device configured for receiving a heated biomass from the vertical reactor vessel, and
a conduit extending from the outlet to the expansion device;
sensors configured to detect a differential pressure between a vapor space above a pile of biomass in the vertical reactor vessel and a vapor space within or above the expansion device; and
a control system configured to control the flow of the propelling steam based on the differential pressure.

9. The assembly of claim 8 further comprising a one-dimensional convergence section of the vertical reactor vessel at, near, or above the propelling steam inlet.

10. The assembly of claim 8 , wherein the propelling steam inlet is at a location after the outlet of the vertical reactor vessel at the conduit extending from the outlet to the expansion device.

11. The assembly of claim 8 further comprising an additional steam inlet on or in the vertical reactor vessel at a middle elevation between the upper and lower regions.

12. The assembly of claim 8 wherein the expansion device is a steam explosion device.

13. The assembly of claim 8 further comprising a source of steam for the upper steam inlet and a source of steam for the propelling steam inlet.

14. The assembly of claim 13 , wherein the source of steam for the upper steam inlet and a source of steam for the propelling steam inlet is the same source.

15. The method of claim 1 , wherein the propelling of the heated biomass through the steam expansion device is continuous.

16. The method of claim 4 , wherein rapidly reducing the pressure on the biomass in the expansion device to burst cellular structures in the biomass occurs continuously.

17. The assembly of claim 8 , wherein the control system is further configured to discharge the biomass from the steam expansion device continuously.

18. A method for treating biomass comprising:
feeding a biomass feed stock through a pressure isolation device and to an upper inlet of a vertical reactor vessel-system, wherein the biomass feed stock is deposited on a pile of biomass within a vertical reactor vessel, and wherein the feeding of the biomass feed stock to the upper inlet is continuous;
adding heat energy to heat and pressurize the biomass feed stock by injecting a first steam volume into an upper region of the vertical reactor vessel;
propelling a heated biomass from the pile of biomass through an outlet disposed at a lower region of the vertical reactor vessel by injecting at least a second steam volume into the lower region of the vertical reactor vessel at, near, or after the outlet of the vertical reactor vessel to define a propelled heated biomass, wherein the injection of the first steam volume and the injection of the at least the second steam volume are ve

Assignees

• Andritz Inc

Inventors

• Stromberg Bertil

Classifications

• C08H8/00

  Macromolecular compounds derived from lignocellulosic materials {(pretreatment thereof B27N)} · CPC title

• D21B1/36 Primary

  Explosive disintegration by sudden pressure reduction · CPC title

• Y02P30/20

  using bio-feedstock · CPC title

• C12M45/20

  Heating; Cooling (heating or cooling apparatus for laboratory uses B01L7/00) · CPC title

• D21C1/02

  with water or steam · CPC title