Saccharified solution production method and saccharified solution production apparatus that use cellulosic biomass as starting material

Patent metadata

Field	Value
Publication number	US-9850551-B2
Application number	US-201214655485-A
Country	US
Kind code	B2
Filing date	Dec 25, 2012
Priority date	Dec 25, 2012
Publication date	Dec 26, 2017
Grant date	Dec 26, 2017

Abstract

A saccharified solution production method includes: a saccharifying step of saccharifying hemicellulose or cellulose contained in cellulosic biomass to C5 or C6 saccharides by subjecting a slurry of cellulosic biomass to a hot water treatment in a supercritical state or subcritical state; a washing step of successively washing a solid in the slurry with washing water after the saccharifying step, by using multiple stages of thickeners for washing arranged in series so that the direction of movement of the solid in the slurry and the direction of movement of overflow water are opposite to each other; and a concentration step of removing a solid residue from the washing water recovered in the washing step by using a thickener for still standing that is different from the thickeners for washing, and then concentrating a supernatant of the thickener for still standing by using a concentration device to give a saccharified solution.

First claim

The invention claimed is:

1. A saccharified solution production method that uses cellulosic biomass as a starting material having all the limitations claimed as whole, comprising:
a saccharifying step of saccharifying hemicellulose or cellulose contained in the cellulosic biomass to C5 saccharides or C6 saccharides by subjecting a slurry of the cellulosic biomass to a hot water treatment in a supercritical state or subcritical state;
a washing step of successively washing a solid in the slurry with washing water after the saccharifying step, by using multiple stages of thickeners for washing arranged in series so that the direction of movement of the solid in the slurry and the direction of movement of an overflow washing water are opposite to each other; and
a concentration step of removing a solid residue from overflow washing water recovered in the washing step by using a thickener that is different from the thickeners for washing, and then concentrating a supernatant of the different thickener by using a concentration device to give a saccharified solution.

2. The saccharified solution production method according to claim 1 , wherein the number of stages of the thickeners for washing is more than or equal to 3 and less than or equal to 6.

3. The saccharified solution production method according to claim 1 , further comprising:
a grinding step of grinding the cellulosic biomass to have a 50% mean particle size ranging from 100 μm or more and 500 μm or less, before the saccharifying step.

4. The saccharified solution production method according to claim 1 , further comprising:
a flush step of flush evaporating the slurry after the saccharifying step,
wherein flush vapor is recovered in the flush step, and is used for preheating the slurry before the saccharifying step.

5. A saccharified solution production apparatus that uses cellulosic biomass as a starting material apparatus as having all the limitations claimed as whole, comprising:
a saccharifying device for saccharifying hemicellulose or cellulose contained in the cellulosic biomass to C5 saccharides or C6 saccharides by subjecting a slurry of the cellulosic biomass to a hot water treatment in a supercritical state or subcritical state;
a flush tank for flush evaporating slurry taken from the saccharifying device;
a heat recovery means that recovers flush vapor and uses it for preheating slurry to be fed to the saccharifying device;
multiple stages of thickeners for washing successively arranged in series so that the direction of movement of a solid in slurry taken from the flush tank and the direction of movement of an overflow washing water are opposite to each other;
a thickener for removing a solid residue from overflow washing water taken from the thickeners for washing; and
a concentration device for concentrating a supernatant of the thickener for removing a solid residue from the overflow washing water taken from the thickeners for washing.

Assignees

• Kawasaki Heavy Ind Ltd

Inventors

• Kusuda Hiromasa
• Izumi Noriaki
• Tajiri Hironori
• Tsujita Shoji
• Taniyama Noriyuki

Classifications

• C12P7/10

  substrate containing cellulosic material · CPC title

• C13K1/02 Primary

  obtained by saccharification of cellulosic materials (manufacture of fodder A23K10/32) · CPC title

• C13K1/04 Primary

  Purifying · CPC title

• Y02P20/544

  Cross-Sectional Technologies · mapped topic

• Y02E50/16

  Cross-Sectional Technologies · mapped topic