Method for producing hydrophobic silica granules
US-2019375942-A1 · Dec 12, 2019 · US
US9834475B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9834475-B2 |
| Application number | US-201514643562-A |
| Country | US |
| Kind code | B2 |
| Filing date | Mar 10, 2015 |
| Priority date | Apr 24, 2014 |
| Publication date | Dec 5, 2017 |
| Grant date | Dec 5, 2017 |
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The method is for use with a substrate having a plurality of parallel channels extending therethrough. In the method, the steps comprise: filling a selected plurality of the channels with a granular material; and consolidating the granular material through heat. The selected plurality of channels is selected to produce a wall that separates the substrate into: a first portion having a first plurality of the parallel channels extending therethrough; and a second portion having a second plurality of the parallel channels extending therethrough.
Opening claim text (preview).
What is claimed is: 1. A method of forming a substrate having a plurality of parallel channels extending there through, the method comprising the steps of: mixing from about 65 to 85% by weight of fly-ash with from about 15 to 35% by weight of a heat sensitive binder to form a granular material; filling a selected plurality of the channels with the granular material; and consolidating the granular material through heat, the selected plurality being selected to produce a wall that separates the substrate into: a first portion having a first plurality of the parallel channels extending there through; and a second portion having a second plurality of the parallel channels extending there through. 2. A method according to claim 1 , wherein the granular material is sintered to produce the wall. 3. A method according to claim 1 , wherein the granular material consists essentially of: from 65 to 85% by weight of fly-ash comprising cenospheres, from 15 to 35% by weight of a heat sensitive binder selected from the group consisting of boric acid and anhydrous boron oxide. 4. A method according to claim 1 , wherein the granular material consists essentially of: from about 80% by weight of said fly ash; about 20% by weight of said heat sensitive binder. 5. The method according to claim 1 , wherein the binder is boric acid. 6. The method according to claim 1 , wherein the granular material has a density of from 25 to 30 lb/ft 3 . 7. The method according to claim 1 , wherein the granular material has a median particle size of approximately 50 microns and a particle size ranging from 10 to 160 microns. 8. The method according to claim 1 , wherein the filling step involves pouring the granular material into the selected plurality of the cells. 9. The method of claim 1 , wherein said granular material is heated to between about 300° C. and 750° C. before filling the selected plurality of channels and fired to above about 850° C. after filling said selected plurality of channels. 10. The method of claim 9 , wherein said firing is above 900° C. 11. The method of claim 10 , wherein said firing is for at least 12 hours. 12. The method of claim 1 , wherein said substrate comprises a catalytic converter.
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