Stabilizer composition of co-attrited microcrystalline cellulose and carboxymethylcellulose, method for making, and uses
US-9055757-B2 · Jun 16, 2015 · US
US9828493B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9828493-B2 |
| Application number | US-201214362652-A |
| Country | US |
| Kind code | B2 |
| Filing date | Nov 30, 2012 |
| Priority date | Dec 9, 2011 |
| Publication date | Nov 28, 2017 |
| Grant date | Nov 28, 2017 |
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The present invention is directed to a co-attrited stabilizer composition comprising: a) microcrystalline cellulose in an amount of from 20%-90% by weight of the composition; b) a hydrocolloid in an amount of from 5%-50% by weight of the composition, wherein the hydrocolloid is selected from at least one member of the group consisting of carboxymethyl cellulose having a degree of substitution of at least 0.95, pectin, alginate, carrageenan, xanthan gum, agar gum, wellan gum, or gellan gum; and c) a starch in an amount of from 5%-50% by weight of the composition, wherein the stabilizer composition has a gel strength (G′) of at least 25 Pa when measured after 24 hours in a 2.6% solids water dispersion at 20° C. The composition is useful as a stabilizer, particularly in food and beverage products.
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What is claimed is: 1. A co-attrited stabilizer composition comprising: a) microcrystalline cellulose in an amount of from 20%-90% by weight of the composition; b) a hydrocolloid in an amount of from 5%-50% by weight of the composition, wherein the hydrocolloid is selected from at least one member of the group consisting of carboxymethyl cellulose having a degree of substitution of from 0.95 to 1.5, pectin, alginate, carrageenan, xanthan gum, agar gum, wellan gum, or gelian gum; and c) a starch in an amount of from 5%-50% by weight of the composition; wherein the stabilizer composition has a gel strength (G′) of at least 25 Pa when measurement is made using a TA-Instruments rheometer (ARES-RFS3) with oscillatory strain sweep at 1 Hz and at 20° C., with gap size at 1.8 mm measured after 24 hours in a 2.6% solids in de-ionized water dispersion at 20° C. 2. The stabilizer of claim 1 , wherein said gel strength (G′) is at least 42 Pa. 3. The stabilizer composition of claim 1 , wherein said hydrocolloid is present in an amount of from 5%-30% and said gel strength (G′) is at least 50 Pa. 4. The stabilizer composition of claim 1 , wherein the microcrystalline cellulose is present in an amount of from 45 to 70% by weight of the composition, the hydrocolloid is present in an amount of from 10-30% by weight of the composition, and the starch is present in an amount of from 20-50% by weight of the composition. 5. The stabilizer composition of claim 1 , wherein the hydrocolloid is carboxymethyl cellulose present in an amount of 5% to 20% by weight of the composition. 6. The stabilizer composition of claim 1 , wherein the carboxymethyl cellulose is present in an amount of from 5%-30%. 7. The stabilizer composition of claim 1 , wherein the carboxymethyl cellulose has a degree of substitution of from 1.15 to 1.5 and is present in an amount of from 5%-30%. 8. The stabilizer composition of claim 1 , wherein the hydrocolloid is at least one carrageenan comprising kappa carrageenan, kappa-2 carrageenan, iota carrageenan, or lambda carrageenan, and mixtures thereof. 9. The stabilizer composition of claim 1 , wherein the starch is selected from at least one member of the group consisting of wheat, corn, oat, rice, tapioca, or potato. 10. The stabilizer composition of claim 1 , wherein the starch comprises a tapioca starch. 11. The stabilizer composition of claim 1 , wherein said composition does not contain a co-attriting agent. 12. A method for making the stabilizer composition of claim 1 comprising: a) admixing the microcrystalline cellulose, hydrocolloid, and starch; b) co-attriting the admixture of step a) to obtain an extrudent; and c) drying the extrudent of step b). 13. The method of claim 12 , wherein the drying of step c) is spray drying. 14. The method of claim 12 , wherein said co-attriting is co-extruding. 15. The method of claim 12 , wherein step b) is performed without the use of a co-attriting salt. 16. A food comprising the stabilizer composition of claim 1 . 17. The food of claim 16 , wherein the food is a beverage. 18. The food of claim 17 , wherein the beverage has a pH of from 2-7. 19. The food of claim 17 , wherein the beverage comprises milk. 20. The food of claim 12 , wherein the stabilizer composition is present in an amount of from 0.05 to 3.5% by total weight of the food. 21. A suspension comprising the stabilizer composition of claim 1 suitable for use in pharmaceutical products, nutraceutical products, cosmetic products, personal care products, or agricultural products. 22. A stabilizer composition of claim 1 prepared by a process comprising the steps: a) admixing the microcrystalline cellulose, hydrocolloid, and starch; b) co-attriting the admixture of step a) to obtain an extrudent; and c) drying the extrudent of step b).
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