Reaction device for preparing light olefins from methanol and/or dimethyl ether

Patent metadata

Field	Value
Publication number	US-9827544-B2
Application number	US-201315039471-A
Country	US
Kind code	B2
Filing date	Dec 3, 2013
Priority date	Dec 3, 2013
Publication date	Nov 28, 2017
Grant date	Nov 28, 2017

Abstract

A reaction device for preparing light olefins from methanol and/or dimethyl ether, and more specifically relates to a reaction device for preparing light olefins from methanol and/or dimethyl ether, which mainly comprises a dense phase fluidized bed reactor ( 2 ), a cyclone separator ( 3 ), a stripper ( 5 ), a lift pipe ( 7 ), a dense phase fluidized bed regenerator ( 10 ), a cyclone separator ( 11 ), a stripper ( 13 ), and a lift pipe ( 15 ), wherein the dense phase fluidized bed reactor ( 2 ) is separated into n (n≧2) secondary reaction zones by a material flow controller ( 17 ), and the dense phase fluidized bed regenerator ( 10 ) is separated into m (m≧2) secondary regeneration zones by the material flow controller ( 17 ).

First claim

What is claimed is:

1. A reaction device for preparing light olefins from methanol and/or dimethyl ether comprising a dense phase fluidized bed reactor, a cyclone separator, a stripper, a lift pipe, a dense phase fluidized bed regenerator, a cyclone separator, a stripper, and a lift pipe; wherein a feeding line for reactor is connected to the bottom of the dense phase fluidized bed reactor; a part of the stripper is in the dense phase fluidized bed reactor, and the remaining part thereof is below the dense phase fluidized bed reactor; the bottom of the lift pipe is connected to the bottom of the stripper, and the top of the lift pipe is connected to the dense phase fluidized bed regenerator; a feeding line for regenerator is connected to the bottom of the dense phase fluidized bed regenerator; a part of the stripper is in the dense phase fluidized bed regenerator, and the remaining part thereof is below the dense phase fluidized bed regenerator; the bottom of the lift pipe is connected to the bottom of the stripper, and the top of the lift pipe is connected to the dense phase fluidized bed reactor, wherein a material flow controller is provided in the dense phase fluidized bed reactor and/or the dense phase fluidized bed regenerator, and the dense phase fluidized bed reactor is separated into n secondary reaction zones by the material flow controller and the 1 st to the n th secondary reaction zones are sequentially connected; the dense phase fluidized bed regenerator is separated into m secondary regeneration zones by the material flow controller and the 1 st to the m th secondary regeneration zones are sequentially connected; and wherein n≧2, and m≧2.

2. The reaction device according to claim 1 , wherein the top of the lift pipe is connected to the 1 st secondary reaction zone, the n th secondary reaction zone is connected to a material overflow port on the upper part of the stripper; and the cyclone separator is provided on the upper part of the dense phase fluidized bed reactor, a top outlet of the cyclone separator is connected to a product material line, and the bottom of the cyclone separator is connected to the n th secondary reaction zone.

3. The reaction device according to claim 2 , wherein the material flow controller is composed of a partition plate, an orifice, a material downward flow pipe, a bottom baffle, and a heat extraction member; and the orifice is located below the partition plate and is connected to the bottom of the material downward flow pipe, the bottom baffle is located at the bottom of the material downward flow pipe and the orifice, and the heat extraction member is fixed on the partition plate.

4. The reaction device according to claim 3 , wherein the bottom baffle is a porous plate or a nonporous plate.

5. The reaction device according to claim 1 , wherein top of the lift pipe is connected to the 1 st secondary regeneration zone, the m th secondary regeneration zone is connected to a material overflow port on the upper part of the stripper; and the cyclone separator is provided on the upper part of the dense phase fluidized bed regenerator, a top outlet of the cyclone separator is connected to an exhaust gas line, and the bottom of the cyclone separator is connected to the m th secondary regeneration zone.

6. The reaction device according to claim 5 , wherein the material flow controller is composed of a partition plate, an orifice, a material downward flow pipe, a bottom baffle, and a heat extraction member; and the orifice is located below the partition plate and is connected to the bottom of the material downward flow pipe, the bottom baffle is located at the bottom of the material downward flow pipe and the orifice, and the heat extraction member is fixed on the partition plate.

7. The reaction device according to claim 6 , wherein the bottom baffle is a porous plate or a nonporous plate.

8. The reaction device according to claim 1 , wherein 8≧n≧3.

9. The reaction device according to claim 8 , wherein the material flow controller is composed of a partition plate, an orifice, a material downward flow pipe, a bottom baffle, and a heat extraction member; and the orifice is located below the partition plate and is connected to the bottom of the material downward flow pipe, the bottom baffle is located at the bottom of the material downward flow pipe and the orifice, and the heat extraction member is fixed on the partition plate.

10. The reaction device according to claim 9 , wherein the bottom baffle is a porous plate or a nonporous plate.

11. The reaction device according to claim 1 , wherein 8≧m≧3.

12. The reaction device according to claim 11 , wherein the material flow controller is composed of a partition plate, an orifice, a material downward flow pipe, a bottom baffle, and a heat extraction member; and the orifice is located below the partition plate and is connected to the bottom of the material downward flow pipe, the bottom baffle is located at the bottom of the material downward flow pipe and the orifice, and the heat extraction member is fixed on the partition plate.

13. The reaction device according to claim 1 , wherein the material flow controller is composed of a partition plate, an orifice, a material downward flow pipe, a bottom baffle, and a heat extraction member; and the orifice is located below the partition plate and is connected to the bottom of the material downward flow pipe, the bottom baffle is located at the bottom of the material downward flow pipe and the orifice, and the heat extraction member is fixed on the partition plate.

14. The reaction device according to claim 13 , wherein the bottom baffle is a porous plate or a nonporous plate.

15. The reaction device according to claim 14 , wherein the bottom baffle is a porous plate or a nonporous plate.

Assignees

• Dalian Inst Chem & Physics Cas

Inventors

• Zhang Tao
• Ye Mao
• Liu Zhongmin

Classifications

• B01J8/1827

  the fluidising gas being a reactant · CPC title

• C07C11/06

  Propene · CPC title

• B01J8/1872

  Details of the fluidised bed reactor (B01J8/1836 takes precedence) · CPC title

• C07C1/20

  starting from organic compounds containing only oxygen atoms as heteroatoms · CPC title

• B01J2208/00902

  Nozzle-type feeding elements · CPC title