System and method for ceramic doping of carbon fiber composite structures

Patent metadata

Field	Value
Publication number	US-9822834-B2
Application number	US-201414527457-A
Country	US
Kind code	B2
Filing date	Oct 29, 2014
Priority date	Oct 29, 2014
Publication date	Nov 21, 2017
Grant date	Nov 21, 2017

Abstract

A system and method for ceramic doping of carbon fiber materials is disclosed. A carbon fiber preform may be made of carbonized oxidized PAN fibers and may be placed in contact with a nanoparticle suspension having nanoparticles and a dispersion medium. The nanoparticles may impregnate the carbon fiber preform, causing it to become a doped carbon fiber preform. The doped carbon fiber preform may be densified. The doped carbon fiber preform may be densified by conventional CVI processing techniques. The doped carbon fiber preform may be densified by thermal gradient CVI.

First claim

What is claimed is:

1. A method of processing a carbon fiber preform comprising:
carbonizing a fibrous preform comprising oxidized PAN fibers to form the carbon fiber preform;
placing the carbon fiber preform in a vacuum chamber;
exposing the carbon fiber preform to a nanoparticle dispersion comprising a nanoparticle and a dispersion medium, wherein the nanoparticle comprises aluminum oxide nanoparticles;
drawing an at least partial vacuum within the vacuum chamber by a vacuum source for a first duration of time and at a first vacuum pressure to facilitate impregnating the nanoparticle into the carbon fiber preform, whereby the carbon fiber preform is converted into a doped carbon fiber preform; and
drying the doped carbon fiber preform at a first temperature whereby the dispersion medium is at least one of substantially removed or completely removed from the doped carbon fiber preform.

2. The method according to claim 1 , wherein the first temperature comprises about 260° C. to 316° C.

3. The method according to claim 1 , further comprising densifying the doped carbon fiber preform.

4. The method according to claim 3 , wherein the impregnating occurs prior to the densifying.

5. The method according to claim 3 , wherein the densifying comprises chemical vapor infiltration (“CVI”).

6. The method of processing a carbon fiber preform according to claim 1 , wherein the first duration of time comprises about 30 minutes.

7. The method of processing a carbon fiber preform according to claim 1 , wherein the first vacuum pressure comprises about 15 mmHg.

8. The method of processing a carbon fiber preform according to claim 3 , wherein the densifying comprises thermal gradient CVI.

Assignees

• Goodrich Corp

Inventors

• Perea Paul

Classifications

• F16D2200/0082

  Production methods therefor · CPC title

• C04B2235/3217

  Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina · CPC title

• C04B35/83

  Carbon fibres in a carbon matrix · CPC title

• F16D2250/0053

  Hardening · CPC title

• C23C16/56

  After-treatment · CPC title