Multi-additive delivery system

Patent metadata

Field	Value
Publication number	US-9821288-B2
Application number	US-201314385792-A
Country	US
Kind code	B2
Filing date	Apr 19, 2013
Priority date	May 10, 2012
Publication date	Nov 21, 2017
Grant date	Nov 21, 2017

Abstract

An apparatus and method for delivery of additives(s), e.g., catalyst, co-catalyst, scavengers, and/or other reaction- or product-modifying agents, to a reaction or mixing site, such as a reaction vessel, offers the capability for multi-additive delivery and customization of additive selection, flow and flow rate, and if desired, mixing thereof, without production train shutdowns. The invention includes at least two additive sources that are detachably connected, with conduit, to the reaction or mixing site, and a process control means, preferably automated, that is capable of initiating, terminating, and determining the rate of flow from the additive sources.

First claim

What is claimed is:

1. An apparatus for delivery of at least one additive to at least one polyolefin polymerization reaction site or polyolefin compounding site, comprising:
(a) at least one means of ingress detachably connected to the at least one polyolefin polymerization reaction site or polyolefin compounding site,
(b) at least one delivery components comprising a first additive source connected intermittently or continuously in series to a second additive source via at least one detachable means for connection, wherein the second additive source is connected to the at least one means of ingress via the at least one detachable means for connection, and wherein the second additive source is capable of providing continuous flow of the at least one additive into the at least one polyolefin polymerization reaction site or polyolefin compounding site via the at least one means for ingress, and
(c) a process control means connected at least to the second additive source, wherein the process control means controls flow of the at least one additive from the second additive source to the at least one means of ingress, wherein controlling flow includes initiation, cessation, and rate of flow of the at least one additive.

2. The apparatus of claim 1 wherein the first and second additive sources are selected from the group consisting of canisters, iso containers, cylinders, and combinations thereof.

3. The apparatus of claim 1 , wherein the process control means comprises automated means that send or receive electrical signals to or from at least one device selected from the group consisting of pumps, valves, meters, conduits, and combinations thereof.

4. A method for delivery of at least one additive, comprising
selecting an apparatus for delivery of the at least one additive according to claim 1 ,
controlling flow of the at least one additive to the polyolefin polymerization reaction site or polyolefin compounding site via the apparatus under conditions such that the at least one additive is continuously delivered to the polyolefin polymerization reaction site or polyolefin compounding site at a pre-selected time, for a pre-selected duration, and at a pre-selected rate, wherein controlling flow includes initiation, cessation, and rate of flow.

5. The method of claim 4 , further comprising transitioning between a plurality of the at least one the additive during the controlling.

6. The method of claim 5 , wherein the transitioning is swung on the fly between the plurality of the at least one additive without shutting down flow.

Assignees

• Dow Global Technologies Llc

Inventors

• Cerk Frank J
• Jain Jr Pradeep
• Dirk Michelle D
• Boone Harold W

Classifications

• B01J2219/00164

  controlling the flow · CPC title

• Y10T137/0318

  Processes · CPC title

• B01J4/02 Primary

  for feeding measured {, i.e. prescribed} quantities of reagents · CPC title

• B01J19/0006 Primary

  Controlling or regulating processes (controlling or regulating in general G05) · CPC title

• B01J2204/002

  the feeding side being of particular interest · CPC title